KR20010108487A - 현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 - Google Patents
현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 Download PDFInfo
- Publication number
- KR20010108487A KR20010108487A KR1020017012918A KR20017012918A KR20010108487A KR 20010108487 A KR20010108487 A KR 20010108487A KR 1020017012918 A KR1020017012918 A KR 1020017012918A KR 20017012918 A KR20017012918 A KR 20017012918A KR 20010108487 A KR20010108487 A KR 20010108487A
- Authority
- KR
- South Korea
- Prior art keywords
- vacuum
- mass spectrometer
- sample
- pump
- carrier gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000004458 analytical method Methods 0.000 title claims description 17
- 239000000126 substance Substances 0.000 title claims description 6
- 238000004817 gas chromatography Methods 0.000 title description 2
- 239000007789 gas Substances 0.000 claims description 28
- 239000012159 carrier gas Substances 0.000 claims description 26
- 108010083687 Ion Pumps Proteins 0.000 claims description 7
- 238000012546 transfer Methods 0.000 claims description 7
- 238000002347 injection Methods 0.000 claims description 6
- 239000007924 injection Substances 0.000 claims description 6
- 239000011521 glass Substances 0.000 claims description 2
- 238000011179 visual inspection Methods 0.000 claims description 2
- 238000011065 in-situ storage Methods 0.000 claims 1
- 238000012423 maintenance Methods 0.000 abstract description 2
- 238000004445 quantitative analysis Methods 0.000 abstract description 2
- 238000004451 qualitative analysis Methods 0.000 abstract 1
- 239000000523 sample Substances 0.000 description 18
- 150000001875 compounds Chemical class 0.000 description 8
- 238000010926 purge Methods 0.000 description 6
- 238000003965 capillary gas chromatography Methods 0.000 description 5
- 238000013461 design Methods 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000010453 quartz Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000004587 chromatography analysis Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 102000006391 Ion Pumps Human genes 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 238000003339 best practice Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000001010 compromised effect Effects 0.000 description 1
- 239000012468 concentrated sample Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000011491 glass wool Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
- G01N30/7206—Mass spectrometers interfaced to gas chromatograph
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/0022—Portable spectrometers, e.g. devices comprising independent power supply, constructional details relating to portability
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N2030/0095—Separation specially adapted for use outside laboratory, e.g. field sampling, portable equipments
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8881—Modular construction, specially adapted therefor
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Electron Tubes For Measurement (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/289,755 | 1999-04-12 | ||
| US09/289,755 US6351983B1 (en) | 1999-04-12 | 1999-04-12 | Portable gas chromatograph mass spectrometer for on-site chemical analyses |
| PCT/US2000/009624 WO2000062054A2 (en) | 1999-04-12 | 2000-04-11 | Portable gas chromatograph mass spectrometer for on-site chemical analyses |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020067026791A Division KR100821954B1 (ko) | 1999-04-12 | 2000-04-11 | 현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20010108487A true KR20010108487A (ko) | 2001-12-07 |
Family
ID=23112943
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020017012918A Ceased KR20010108487A (ko) | 1999-04-12 | 2000-04-11 | 현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 |
| KR1020067026791A Expired - Fee Related KR100821954B1 (ko) | 1999-04-12 | 2000-04-11 | 현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020067026791A Expired - Fee Related KR100821954B1 (ko) | 1999-04-12 | 2000-04-11 | 현장에서의 화학 분석을 위한 휴대용 가스 크로마토그래프질량 분석계 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6351983B1 (enExample) |
| JP (1) | JP2003527563A (enExample) |
| KR (2) | KR20010108487A (enExample) |
| CN (1) | CN1242265C (enExample) |
| AU (1) | AU4229100A (enExample) |
| WO (1) | WO2000062054A2 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101143080B1 (ko) * | 2006-07-31 | 2012-05-08 | 어플라이드 머티어리얼스, 인코포레이티드 | 전자 장치 제조 시스템에서 가스들의 인시튜 분석을 위한 방법 및 장치 |
| KR101345759B1 (ko) * | 2009-10-28 | 2014-01-03 | (주)바이오니아 | 실시간 휘발성 유기 화합물 모니터링을 위한 휴대형 gcms |
Families Citing this family (51)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JP4671462B2 (ja) * | 2000-02-22 | 2011-04-20 | パナソニック株式会社 | ニッケル水素二次電池の気密検査方法 |
| DE10013561A1 (de) * | 2000-03-20 | 2001-09-27 | Abb Research Ltd | Meß- und Auswerteeinrichtung |
| CA2358243C (en) * | 2000-10-04 | 2010-07-27 | University Of South Florida | Portable underwater mass spectrometer |
| FR2815074B1 (fr) * | 2000-10-10 | 2002-12-06 | Inst Francais Du Petrole | Methode d'analyse et de mesures chimique et isotopique sur des constituants transportes par un fluide de forage |
| US7210342B1 (en) * | 2001-06-02 | 2007-05-01 | Fluid Inclusion Technologies, Inc. | Method and apparatus for determining gas content of subsurface fluids for oil and gas exploration |
| JP2003254285A (ja) * | 2002-02-28 | 2003-09-10 | Boc Edwards Technologies Ltd | ポンプ装置 |
| JP3537425B2 (ja) * | 2002-03-29 | 2004-06-14 | 日本パステック株式会社 | 複合分析装置 |
| US6837096B2 (en) * | 2003-01-23 | 2005-01-04 | Midwest Research Institute, Inc. | Low-power gas chromatograph |
| DE10319130B3 (de) * | 2003-04-28 | 2004-09-09 | Siemens Ag | Gaschromatograph mit nachgeordnetem Massenspektrometer und Verfahren zur gaschromatographisch-massenspektrometrischen Analyse eines Stoffgemischs |
| DE112005001385T5 (de) * | 2004-06-15 | 2007-05-10 | Griffin analytical Technologies Inc., West Lafayette | Analyseinstrumente, -baugruppen und -verfahren |
| GB2439261B (en) | 2005-04-25 | 2011-02-23 | Griffin Analytical Technologies Llc | Analytical apparatuses and methods |
| US7635005B2 (en) * | 2006-05-16 | 2009-12-22 | Alliant Techsystems Inc. | Very small high pressure regulator |
| US7524363B2 (en) * | 2006-05-16 | 2009-04-28 | Alliant Techsystems Inc. | Gas chromatograph column assembly |
| US7735352B2 (en) * | 2006-05-16 | 2010-06-15 | Alliant Techsystems Inc. | Multi-dimensional portable gas chromatograph system |
| US7485176B2 (en) * | 2006-05-16 | 2009-02-03 | Alliant Techsystems Inc. | Compact thermal conductivity detector |
| US20070274841A1 (en) * | 2006-05-24 | 2007-11-29 | Ghantasala Muralidhar K | Passive adsorption microvacuum pump and microsystem containing the same |
| US7992424B1 (en) | 2006-09-14 | 2011-08-09 | Griffin Analytical Technologies, L.L.C. | Analytical instrumentation and sample analysis methods |
| US8288719B1 (en) | 2006-12-29 | 2012-10-16 | Griffin Analytical Technologies, Llc | Analytical instruments, assemblies, and methods |
| EP2112678B1 (en) * | 2007-02-16 | 2021-03-31 | National Institute of Information and Communications Technology | Vacuum conveyance system |
| US20080296491A1 (en) * | 2007-02-26 | 2008-12-04 | Arkansas State University Research And Development Institute | Method and apparatus to detect chemical vapors |
| JP5221903B2 (ja) * | 2007-06-27 | 2013-06-26 | 株式会社島津製作所 | 質量分析装置 |
| US7564029B2 (en) * | 2007-08-15 | 2009-07-21 | Varian, Inc. | Sample ionization at above-vacuum pressures |
| JP4915623B2 (ja) * | 2008-08-19 | 2012-04-11 | 西川計測株式会社 | 化学剤検出・定量方法 |
| US20100096544A1 (en) * | 2008-10-16 | 2010-04-22 | Battelle Memorial Institute | Surface Sampling Probe for Field Portable Surface Sampling Mass Spectrometer |
| KR101193988B1 (ko) | 2010-11-11 | 2012-10-24 | 한국수력원자력 주식회사 | 복합 환경에서의 재료 기상 반응 분석 장치 |
| US20120118144A1 (en) * | 2010-11-12 | 2012-05-17 | Meadoworks, Inc. | Vacuum Chromatography Gas Detector |
| JP5285735B2 (ja) | 2011-03-31 | 2013-09-11 | 株式会社日立ハイテクノロジーズ | 質量分析装置 |
| JP2013011556A (ja) * | 2011-06-30 | 2013-01-17 | Md Innovations Kk | 隔膜気圧計 |
| JP5682506B2 (ja) * | 2011-08-24 | 2015-03-11 | 株式会社島津製作所 | ガスクロマトグラフ装置 |
| KR101168199B1 (ko) | 2011-11-04 | 2012-07-25 | 국방과학연구소 | 특정화학물질의 신속 현장 검증 방법 및 그 장치 |
| CN104797932B (zh) * | 2012-06-04 | 2016-12-28 | 分析中心 | 一种用于含有易燃物质的流体的分析仪和相应的方法 |
| US10229824B2 (en) | 2013-03-11 | 2019-03-12 | 1St Detect Corporation | Chemical analysis instrument with multi-purpose pump |
| US9373492B2 (en) | 2013-03-14 | 2016-06-21 | The University Of North Carolina At Chapel Hill | Microscale mass spectrometry systems, devices and related methods |
| US10012623B2 (en) | 2014-11-24 | 2018-07-03 | Marco CISTERNI | Apparatus and method for mitigation of alterations in mass spectrometry in the presence of hydrogen |
| US10088464B2 (en) * | 2015-06-16 | 2018-10-02 | Lunatech, Llc | Systems and methods for analyzing pharmaceuticals |
| US20160370337A1 (en) * | 2015-06-16 | 2016-12-22 | Lunatech, Llc | Analysis System For Biological Compounds, And Method Of Operation |
| US9874546B2 (en) * | 2015-07-24 | 2018-01-23 | Thermo Finnigan Llc | Systems and methods for conserving carrier gas |
| US20170067863A1 (en) * | 2015-09-03 | 2017-03-09 | Ranjith Kunnath Narayanan | Portable spectroscopic analysis tool |
| US10502664B2 (en) | 2016-03-08 | 2019-12-10 | Entech Instruments Inc. | Vacuum-assisted sample extraction device and method |
| US10849600B2 (en) | 2016-03-08 | 2020-12-01 | Entech Instruments Inc. | Breath condensate and saliva analysis using oral rinse |
| USD834433S1 (en) | 2017-06-13 | 2018-11-27 | Flir Detection, Inc. | Trace analysis instrument |
| JP6753366B2 (ja) * | 2017-06-23 | 2020-09-09 | 株式会社島津製作所 | 分析装置 |
| KR102444774B1 (ko) * | 2017-12-27 | 2022-09-19 | 오씨아이 주식회사 | 카본 블랙의 표면 관능기의 정량 및 정성 분석 시스템 및 방법 |
| WO2019173501A1 (en) | 2018-03-06 | 2019-09-12 | Entech Instruments Inc. | Ventilator-coupled sampling device and method |
| EP3769333A4 (en) * | 2018-03-23 | 2022-04-13 | Adaptas Solutions Pty Ltd | PARTICLE DETECTOR WITH IMPROVED PERFORMANCE AND LIFESPAN |
| GB201810828D0 (en) * | 2018-06-01 | 2018-08-15 | Micromass Ltd | A GC/MS arrangement and mass spectrometer |
| WO2020028441A1 (en) | 2018-07-31 | 2020-02-06 | Entech Instruments Inc. | Hybrid capillary/packed trap and method of use |
| GB2576169B (en) * | 2018-08-07 | 2022-03-09 | Applied Science & Tech Solutions Ltd | Mass spectrometry system |
| CN112816436B (zh) * | 2019-11-15 | 2022-05-17 | 武汉米字能源科技有限公司 | 一种光谱-质谱联用装置及检测方法 |
| EP4115440B1 (en) * | 2020-03-05 | 2024-02-28 | Smart Sensors Holdings B.V. | Instrument comprising a vacuum chamber |
| US11867682B2 (en) | 2020-09-21 | 2024-01-09 | Baker Hughes Oilfield Operations Llc | System and method for determining natural hydrocarbon concentration utilizing isotope data |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US5313061A (en) * | 1989-06-06 | 1994-05-17 | Viking Instrument | Miniaturized mass spectrometer system |
| US5051557A (en) * | 1989-06-07 | 1991-09-24 | The United States Of America As Represented By The Secretary Of The Department Of Health And Human Services | Microwave induced plasma torch with tantalum injector probe |
| US5083450A (en) * | 1990-05-18 | 1992-01-28 | Martin Marietta Energy Systems, Inc. | Gas chromatograph-mass spectrometer (gc/ms) system for quantitative analysis of reactive chemical compounds |
| US5155357A (en) * | 1990-07-23 | 1992-10-13 | Massachusetts Institute Of Technology | Portable mass spectrometer |
| US5360976A (en) * | 1992-08-25 | 1994-11-01 | Southwest Research Institute | Time of flight mass spectrometer, ion source, and methods of preparing a sample for mass analysis and of mass analyzing a sample |
| US5472670A (en) * | 1993-03-05 | 1995-12-05 | Ohio University | Gas chromatography sample injector and apparatus using same |
| US5426300A (en) * | 1993-09-17 | 1995-06-20 | Leybold Inficon, Inc. | Portable GCMS system using getter pump |
| US5611846A (en) * | 1994-01-14 | 1997-03-18 | Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College | Portable gas chromatograph |
| US5525799A (en) * | 1994-04-08 | 1996-06-11 | The United States Of America As Represented By The United States Department Of Energy | Portable gas chromatograph-mass spectrometer |
| US5451781A (en) | 1994-10-28 | 1995-09-19 | Regents Of The University Of California | Mini ion trap mass spectrometer |
| US5521381A (en) * | 1994-12-12 | 1996-05-28 | The Regents Of The University Of California | Contamination analysis unit |
| JP3128053B2 (ja) * | 1995-05-30 | 2001-01-29 | 株式会社島津製作所 | ガスクロマトグラフ質量分析装置 |
| JP3473280B2 (ja) * | 1996-06-27 | 2003-12-02 | 株式会社島津製作所 | ガスクロマトグラフ質量分析装置 |
| WO1998015813A1 (en) * | 1996-10-09 | 1998-04-16 | Symyx Technologies | Infrared spectroscopy and imaging of libraries |
-
1999
- 1999-04-12 US US09/289,755 patent/US6351983B1/en not_active Expired - Lifetime
-
2000
- 2000-04-11 CN CNB008073252A patent/CN1242265C/zh not_active Expired - Fee Related
- 2000-04-11 KR KR1020017012918A patent/KR20010108487A/ko not_active Ceased
- 2000-04-11 AU AU42291/00A patent/AU4229100A/en not_active Abandoned
- 2000-04-11 WO PCT/US2000/009624 patent/WO2000062054A2/en not_active Ceased
- 2000-04-11 JP JP2000611067A patent/JP2003527563A/ja active Pending
- 2000-04-11 KR KR1020067026791A patent/KR100821954B1/ko not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101143080B1 (ko) * | 2006-07-31 | 2012-05-08 | 어플라이드 머티어리얼스, 인코포레이티드 | 전자 장치 제조 시스템에서 가스들의 인시튜 분석을 위한 방법 및 장치 |
| US8813538B2 (en) | 2006-07-31 | 2014-08-26 | Applied Materials, Inc. | Methods and apparatus for insitu analysis of gases in electronic device fabrication systems |
| KR101345759B1 (ko) * | 2009-10-28 | 2014-01-03 | (주)바이오니아 | 실시간 휘발성 유기 화합물 모니터링을 위한 휴대형 gcms |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1242265C (zh) | 2006-02-15 |
| US6351983B1 (en) | 2002-03-05 |
| CN1367874A (zh) | 2002-09-04 |
| WO2000062054A2 (en) | 2000-10-19 |
| KR100821954B1 (ko) | 2008-04-15 |
| WO2000062054A3 (en) | 2001-02-01 |
| AU4229100A (en) | 2000-11-14 |
| KR20070009743A (ko) | 2007-01-18 |
| JP2003527563A (ja) | 2003-09-16 |
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