KR102610677B1 - (메트)아크릴산 에스테르를 정제하기 위한 방법 - Google Patents

(메트)아크릴산 에스테르를 정제하기 위한 방법 Download PDF

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Publication number
KR102610677B1
KR102610677B1 KR1020197035333A KR20197035333A KR102610677B1 KR 102610677 B1 KR102610677 B1 KR 102610677B1 KR 1020197035333 A KR1020197035333 A KR 1020197035333A KR 20197035333 A KR20197035333 A KR 20197035333A KR 102610677 B1 KR102610677 B1 KR 102610677B1
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column
section
meth
acrylic acid
purified
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Korean (ko)
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KR20200033797A (ko
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로이 롤레스
세르게 트레티악
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아르끄마 프랑스
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10—Separation; Purification; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
KR1020197035333A 2017-07-25 2018-07-03 (메트)아크릴산 에스테르를 정제하기 위한 방법 Active KR102610677B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1757038A FR3069538B1 (fr) 2017-07-25 2017-07-25 Procede de purification d'esters (meth)acryliques.
FR1757038 2017-07-25
PCT/FR2018/051645 WO2019020889A1 (fr) 2017-07-25 2018-07-03 Procede de purification d'esters (meth)acryliques

Publications (2)

Publication Number Publication Date
KR20200033797A KR20200033797A (ko) 2020-03-30
KR102610677B1 true KR102610677B1 (ko) 2023-12-05

Family

ID=60138503

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020197035333A Active KR102610677B1 (ko) 2017-07-25 2018-07-03 (메트)아크릴산 에스테르를 정제하기 위한 방법

Country Status (8)

Country Link
US (1) US11261150B2 (enExample)
EP (1) EP3658249B1 (enExample)
JP (1) JP7079272B2 (enExample)
KR (1) KR102610677B1 (enExample)
CN (1) CN110709149A (enExample)
FR (1) FR3069538B1 (enExample)
SA (1) SA519410648B1 (enExample)
WO (1) WO2019020889A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116323537B (zh) * 2021-09-14 2025-07-22 株式会社Lg化学 多组分混合物分离系统
AU2024209766A1 (en) * 2023-01-20 2025-07-31 Kemira Oyj Surfactant compositions derived from waste streams, and methods

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015504084A (ja) * 2012-01-23 2015-02-05 アルケマ フランス エステル交換による２−オクチルアクリレートの生成のための方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5035214A (en) * 1990-02-16 1991-07-30 Siemens Automotive L.P. Engine throttle blade sealing
JPH0613462B2 (ja) * 1990-09-25 1994-02-23 東亞合成化学工業株式会社 ジメチルアミノエチルアクリレートの貯蔵方法
FR2777561B1 (fr) 1998-04-21 2000-06-02 Atochem Elf Sa Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle
DE10127938A1 (de) 2001-06-08 2002-07-25 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
DE10127939A1 (de) 2001-06-08 2002-05-29 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
US6930206B1 (en) * 2001-07-05 2005-08-16 Catalytic Distillation Technologies Process and apparatus for catalytic distillations
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
US20090139852A1 (en) * 2007-12-04 2009-06-04 Vannuland Marco L Separation Method And Apparatus
AU2010326267B2 (en) * 2009-12-01 2015-07-16 Exxonmobil Research And Engineering Company Two stage hydroprocessing with divided wall column fractionator
SG190284A1 (en) * 2010-11-22 2013-06-28 Rohm & Haas Acrylate production process
KR101496488B1 (ko) * 2010-12-29 2015-02-26 주식회사 엘지화학 고순도 2-에틸헥실-아크릴레이트 생산을 위한 분리벽형 증류탑 및 이를 이용한 제조방법
FR2999572B1 (fr) 2012-12-17 2014-11-28 Arkema France Procede de production d'acrylate d'alkyle.
KR101583145B1 (ko) * 2013-07-18 2016-01-07 주식회사 엘지화학 증류 장치
CN203494195U (zh) * 2013-09-24 2014-03-26 中国石油化工股份有限公司 用于共沸精馏的分壁精馏塔
CN106861353A (zh) * 2015-12-14 2017-06-20 财团法人工业技术研究院 分离装置
CN106748758A (zh) * 2016-12-21 2017-05-31 常州大学 热泵分隔壁反应精馏塔制备乙酸异丙酯的装置

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015504084A (ja) * 2012-01-23 2015-02-05 アルケマ フランス エステル交換による２−オクチルアクリレートの生成のための方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
- Chemical Engineering and Processing 49 (2010) 139-146. 1부.*

Also Published As

Publication number Publication date
EP3658249A1 (fr) 2020-06-03
FR3069538B1 (fr) 2020-05-15
BR112019024485A2 (pt) 2020-06-16
US11261150B2 (en) 2022-03-01
CN110709149A (zh) 2020-01-17
KR20200033797A (ko) 2020-03-30
FR3069538A1 (fr) 2019-02-01
JP7079272B2 (ja) 2022-06-01
US20210300857A1 (en) 2021-09-30
SA519410648B1 (ar) 2023-01-10
JP2020528398A (ja) 2020-09-24
EP3658249B1 (fr) 2021-10-27
WO2019020889A1 (fr) 2019-01-31

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