FR3069538B1 - Procede de purification d'esters (meth)acryliques. - Google Patents

Procede de purification d'esters (meth)acryliques. Download PDF

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Publication number
FR3069538B1
FR3069538B1 FR1757038A FR1757038A FR3069538B1 FR 3069538 B1 FR3069538 B1 FR 3069538B1 FR 1757038 A FR1757038 A FR 1757038A FR 1757038 A FR1757038 A FR 1757038A FR 3069538 B1 FR3069538 B1 FR 3069538B1
Authority
FR
France
Prior art keywords
column
meth
purification
acrylic esters
contiguous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1757038A
Other languages
English (en)
French (fr)
Other versions
FR3069538A1 (fr
Inventor
Serge Tretjak
Eloi Rolez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1757038A priority Critical patent/FR3069538B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to KR1020197035333A priority patent/KR102610677B1/ko
Priority to US16/616,528 priority patent/US11261150B2/en
Priority to CN201880035815.XA priority patent/CN110709149A/zh
Priority to PCT/FR2018/051645 priority patent/WO2019020889A1/fr
Priority to JP2019563593A priority patent/JP7079272B2/ja
Priority to BR112019024485-9A priority patent/BR112019024485B1/pt
Priority to EP18749024.8A priority patent/EP3658249B1/fr
Publication of FR3069538A1 publication Critical patent/FR3069538A1/fr
Priority to SA519410648A priority patent/SA519410648B1/ar
Application granted granted Critical
Publication of FR3069538B1 publication Critical patent/FR3069538B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
FR1757038A 2017-07-25 2017-07-25 Procede de purification d'esters (meth)acryliques. Active FR3069538B1 (fr)

Priority Applications (9)

Application Number Priority Date Filing Date Title
FR1757038A FR3069538B1 (fr) 2017-07-25 2017-07-25 Procede de purification d'esters (meth)acryliques.
US16/616,528 US11261150B2 (en) 2017-07-25 2018-07-03 Method for purifying (meth)acrylic esters
CN201880035815.XA CN110709149A (zh) 2017-07-25 2018-07-03 纯化(甲基)丙烯酸酯的方法
PCT/FR2018/051645 WO2019020889A1 (fr) 2017-07-25 2018-07-03 Procede de purification d'esters (meth)acryliques
KR1020197035333A KR102610677B1 (ko) 2017-07-25 2018-07-03 (메트)아크릴산 에스테르를 정제하기 위한 방법
JP2019563593A JP7079272B2 (ja) 2017-07-25 2018-07-03 （メタ）アクリル酸エステルの精製方法
BR112019024485-9A BR112019024485B1 (pt) 2017-07-25 2018-07-03 Processo de purificação de ésteres metacrílicos
EP18749024.8A EP3658249B1 (fr) 2017-07-25 2018-07-03 Procede de purification d'esters (meth)acryliques
SA519410648A SA519410648B1 (ar) 2017-07-25 2019-11-27 طريقة لتنقية استرات (ميث) أكريليك

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1757038A FR3069538B1 (fr) 2017-07-25 2017-07-25 Procede de purification d'esters (meth)acryliques.
FR1757038 2017-07-25

Publications (2)

Publication Number Publication Date
FR3069538A1 FR3069538A1 (fr) 2019-02-01
FR3069538B1 true FR3069538B1 (fr) 2020-05-15

Family

ID=60138503

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1757038A Active FR3069538B1 (fr) 2017-07-25 2017-07-25 Procede de purification d'esters (meth)acryliques.

Country Status (8)

Country Link
US (1) US11261150B2 (enExample)
EP (1) EP3658249B1 (enExample)
JP (1) JP7079272B2 (enExample)
KR (1) KR102610677B1 (enExample)
CN (1) CN110709149A (enExample)
FR (1) FR3069538B1 (enExample)
SA (1) SA519410648B1 (enExample)
WO (1) WO2019020889A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116323537B (zh) * 2021-09-14 2025-07-22 株式会社Lg化学 多组分混合物分离系统
AU2024209766A1 (en) * 2023-01-20 2025-07-31 Kemira Oyj Surfactant compositions derived from waste streams, and methods

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5035214A (en) * 1990-02-16 1991-07-30 Siemens Automotive L.P. Engine throttle blade sealing
JPH0613462B2 (ja) * 1990-09-25 1994-02-23 東亞合成化学工業株式会社 ジメチルアミノエチルアクリレートの貯蔵方法
FR2777561B1 (fr) 1998-04-21 2000-06-02 Atochem Elf Sa Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle
DE10127938A1 (de) 2001-06-08 2002-07-25 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
DE10127939A1 (de) 2001-06-08 2002-05-29 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
US6930206B1 (en) * 2001-07-05 2005-08-16 Catalytic Distillation Technologies Process and apparatus for catalytic distillations
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
US20090139852A1 (en) * 2007-12-04 2009-06-04 Vannuland Marco L Separation Method And Apparatus
AU2010326267B2 (en) * 2009-12-01 2015-07-16 Exxonmobil Research And Engineering Company Two stage hydroprocessing with divided wall column fractionator
SG190284A1 (en) * 2010-11-22 2013-06-28 Rohm & Haas Acrylate production process
KR101496488B1 (ko) * 2010-12-29 2015-02-26 주식회사 엘지화학 고순도 2-에틸헥실-아크릴레이트 생산을 위한 분리벽형 증류탑 및 이를 이용한 제조방법
FR2985999B1 (fr) 2012-01-23 2014-01-31 Arkema France Procede de production d'acrylate de 2-octyle par transesterification
FR2999572B1 (fr) 2012-12-17 2014-11-28 Arkema France Procede de production d'acrylate d'alkyle.
KR101583145B1 (ko) * 2013-07-18 2016-01-07 주식회사 엘지화학 증류 장치
CN203494195U (zh) * 2013-09-24 2014-03-26 中国石油化工股份有限公司 用于共沸精馏的分壁精馏塔
CN106861353A (zh) * 2015-12-14 2017-06-20 财团法人工业技术研究院 分离装置
CN106748758A (zh) * 2016-12-21 2017-05-31 常州大学 热泵分隔壁反应精馏塔制备乙酸异丙酯的装置

Also Published As

Publication number Publication date
EP3658249A1 (fr) 2020-06-03
BR112019024485A2 (pt) 2020-06-16
US11261150B2 (en) 2022-03-01
CN110709149A (zh) 2020-01-17
KR20200033797A (ko) 2020-03-30
KR102610677B1 (ko) 2023-12-05
FR3069538A1 (fr) 2019-02-01
JP7079272B2 (ja) 2022-06-01
US20210300857A1 (en) 2021-09-30
SA519410648B1 (ar) 2023-01-10
JP2020528398A (ja) 2020-09-24
EP3658249B1 (fr) 2021-10-27
WO2019020889A1 (fr) 2019-01-31

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