KR102599853B1 - 재생 루프 세정 - Google Patents

재생 루프 세정 Download PDF

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KR102599853B1
KR102599853B1 KR1020177003647A KR20177003647A KR102599853B1 KR 102599853 B1 KR102599853 B1 KR 102599853B1 KR 1020177003647 A KR1020177003647 A KR 1020177003647A KR 20177003647 A KR20177003647 A KR 20177003647A KR 102599853 B1 KR102599853 B1 KR 102599853B1
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contaminants
regeneration gas
particulate adsorbent
adsorbent bed
adsorbent
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KR1020177003647A
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Korean (ko)
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KR20170035934A (ko
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윌리엄 돌란
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바스프 코포레이션
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0423—Beds in columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0462—Temperature swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/04—Ethylene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/06—Propene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/08—Alkenes with four carbon atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/104—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/30—Physical properties of adsorbents
    • B01D2253/302—Dimensions
    • B01D2253/304—Linear dimensions, e.g. particle shape, diameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/24—Hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/30—Sulfur compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/30—Sulfur compounds
    • B01D2257/306—Organic sulfur compounds, e.g. mercaptans
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40083—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption
    • B01D2259/40086—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by using a purge gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40083—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption
    • B01D2259/40088—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating
    • B01D2259/4009—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating using hot gas
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/40—Ethylene production

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
KR1020177003647A 2014-07-16 2015-07-15 재생 루프 세정 Active KR102599853B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US14/332,485 2014-07-16
US14/332,485 US9517983B2 (en) 2014-07-16 2014-07-16 Regeneration loop clean-up
PCT/US2015/040602 WO2016011171A1 (en) 2014-07-16 2015-07-15 Regeneration loop clean-up

Publications (2)

Publication Number Publication Date
KR20170035934A KR20170035934A (ko) 2017-03-31
KR102599853B1 true KR102599853B1 (ko) 2023-11-09

Family

ID=55073989

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Application Number Title Priority Date Filing Date
KR1020177003647A Active KR102599853B1 (ko) 2014-07-16 2015-07-15 재생 루프 세정

Country Status (11)

Country Link
US (2) US9517983B2 (enExample)
EP (1) EP3169656B1 (enExample)
JP (1) JP6682499B2 (enExample)
KR (1) KR102599853B1 (enExample)
CN (1) CN107074690A (enExample)
CA (1) CA2955189C (enExample)
ES (1) ES2797025T3 (enExample)
HU (1) HUE048800T2 (enExample)
PL (1) PL3169656T3 (enExample)
SG (1) SG11201700293TA (enExample)
WO (1) WO2016011171A1 (enExample)

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CN109922872A (zh) 2016-09-01 2019-06-21 埃克森美孚上游研究公司 使用3a沸石结构移除水的变化吸附处理
JP7021227B2 (ja) 2016-12-21 2022-02-16 エクソンモービル アップストリーム リサーチ カンパニー 活性材料を有する自己支持構造
US10744492B2 (en) * 2017-11-03 2020-08-18 Uop Llc Adsorbent for contaminant removal from C4 hydrocarbons
US11097219B2 (en) 2018-03-31 2021-08-24 Uop Llc Thermal swing adsorption process with purification
US11318410B2 (en) 2018-12-21 2022-05-03 Exxonmobil Upstream Research Company Flow modulation systems, apparatus, and methods for cyclical swing adsorption
EP3962641A1 (en) 2019-04-30 2022-03-09 Exxonmobil Upstream Research Company (EMHC-N1-4A-607) Rapid cycle adsorbent bed
ES2984328T3 (es) * 2019-05-14 2024-10-29 Evonik Oxeno Gmbh & Co Kg Procedimiento para la purificación de una corriente de hidrocarburos con buteno residual
WO2021071755A1 (en) 2019-10-07 2021-04-15 Exxonmobil Upstream Research Company Adsorption processes and systems utilizing step lift control of hydraulically actuated poppet valves
US11433346B2 (en) 2019-10-16 2022-09-06 Exxonmobil Upstream Research Company Dehydration processes utilizing cationic zeolite RHO
JP7588468B2 (ja) * 2020-03-19 2024-11-22 三井化学株式会社 重合用α－オレフィンの製造方法
US11565986B2 (en) * 2020-08-31 2023-01-31 Chevron U.S.A. Inc. Ethylene separations using small pore zeolites containing double-six rings and cages
WO2022087265A1 (en) * 2020-10-22 2022-04-28 Basf Corporation Adsorbent material for removing nitrogen oxides from indoor or cabin air
KR102588214B1 (ko) * 2021-03-22 2023-10-12 한국화학연구원 올레핀 복분해 반응용 원료 정제를 위한 금속 입자 혼합물의 재생방법
JP7650767B2 (ja) * 2021-09-22 2025-03-25 大阪瓦斯株式会社 二酸化炭素回収装置及び二酸化炭素回収方法
CN115491223A (zh) * 2022-10-21 2022-12-20 中国石油化工股份有限公司 一种用于脱除异构烷烃中含氧化合物吸附剂的再生方法

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US3176445A (en) 1960-09-16 1965-04-06 Union Carbide Corp Method of separating gas mixtures by adsorption
US4484933A (en) 1983-06-14 1984-11-27 Union Carbide Corporation Process for drying gas streams
US4971606A (en) 1989-11-06 1990-11-20 Air Products And Chemicals, Inc. Closed-loop thermal regeneration of adsorbents containing reactive adsorbates
JP2011230103A (ja) * 2010-04-30 2011-11-17 Jx Nippon Oil & Energy Corp 固体成型吸着剤及び炭化水素の精製方法

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US3176445A (en) 1960-09-16 1965-04-06 Union Carbide Corp Method of separating gas mixtures by adsorption
US4484933A (en) 1983-06-14 1984-11-27 Union Carbide Corporation Process for drying gas streams
US4971606A (en) 1989-11-06 1990-11-20 Air Products And Chemicals, Inc. Closed-loop thermal regeneration of adsorbents containing reactive adsorbates
JP2011230103A (ja) * 2010-04-30 2011-11-17 Jx Nippon Oil & Energy Corp 固体成型吸着剤及び炭化水素の精製方法

Also Published As

Publication number Publication date
CN107074690A (zh) 2017-08-18
US20160016865A1 (en) 2016-01-21
US20170050903A1 (en) 2017-02-23
EP3169656B1 (en) 2020-03-18
ES2797025T3 (es) 2020-12-01
US9517983B2 (en) 2016-12-13
WO2016011171A1 (en) 2016-01-21
PL3169656T3 (pl) 2020-08-10
JP6682499B2 (ja) 2020-04-15
KR20170035934A (ko) 2017-03-31
US9994500B2 (en) 2018-06-12
EP3169656A1 (en) 2017-05-24
HUE048800T2 (hu) 2020-08-28
JP2017521450A (ja) 2017-08-03
CA2955189C (en) 2023-08-29
SG11201700293TA (en) 2017-02-27
EP3169656A4 (en) 2018-04-04
CA2955189A1 (en) 2016-01-21

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