KR102580934B1 - Anti-inflammation and antioxidant cosmetic composition using raw materials from Jeju - Google Patents
Anti-inflammation and antioxidant cosmetic composition using raw materials from Jeju Download PDFInfo
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/00—Cosmetics or similar toiletry preparations
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Abstract
Description
본 발명은 제주산 원물을 활용한 항염 항산화 화장료 조성물에 관한 것으로, 상세하게는 제주산 원물을 활용하여 미백, 보습, 항산화, 항염 효과를 나타내는 화장료 조성물에 관한 것이다.The present invention relates to an anti-inflammatory antioxidant cosmetic composition using ingredients from Jeju Island, and more specifically, to a cosmetic composition that exhibits whitening, moisturizing, antioxidant, and anti-inflammatory effects using ingredients from Jeju Island.
생체에서 표면적이 가장 큰 기관인 피부 내에 존재하는 멜라닌은 피부의 색상을 변화시키는 주요한 생물학적 색소로서 작용한다. 피부 기저층에는 존재하는 멜라노사이트에서 멜라노좀과 멜라닌이 생성되는데 멜라닌은 멜라노좀이라는 새포에 의해 만들어진다. 피부의 멜라닌 생합성에는 다양한 기전들이 연관되어 있는데 그 중에서도 자외선에 의한 자극으로 p53유전자가 만들어 내는 알파-멜라노사이트-조절호르몬에 의한 조절과, 이 호르몬에 의해 증가된 마이크로프탈미아 연합 전이 요소(MITF)가 멜라노좀 안에 존재하는 타이로시네이즈의 활성화를 촉진하고, 활성화된 타이로시네이즈에 의해 DOPA의 하이드록실레이션 과정이 개시되며, 타이로시네이즈 하위 단백질들인 TRP1과 TRP2에 의해 멜라닌 생합성을 촉진 및 조절하게 된다. 최종 산물인 멜라닌은 표피 세포 안으로 들어가 자외선과 같은 피부 자극 물질로부터 피부세포를 보호하는 역할을 수행하게 된다. 그러나 멜라닌 합성의 과다 촉진은 피부에 과색소 침착과 염증성 침착과 같은 기전을 일으키게 된다. Melanin present in the skin, the organ with the largest surface area in the living body, acts as a major biological pigment that changes the color of the skin. Melanosomes and melanin are produced from melanocytes present in the basal layer of the skin, and melanin is produced by cells called melanosomes. Various mechanisms are involved in melanin biosynthesis in the skin. Among them, regulation by alpha-melanocyte-regulating hormone produced by the p53 gene upon stimulation by ultraviolet rays, and microphthalmia-associated transposable element (MITF) increased by this hormone. It promotes the activation of tyrosinase present in melanosomes, the hydroxylation process of DOPA is initiated by the activated tyrosinase, and melanin biosynthesis is promoted by the tyrosinase sub-proteins TRP1 and TRP2. and is adjusted. The final product, melanin, enters the epidermal cells and plays the role of protecting skin cells from skin irritants such as ultraviolet rays. However, excessive promotion of melanin synthesis causes mechanisms such as hyperpigmentation and inflammatory deposition in the skin.
현재 피부 미백에 대해 알부틴(Arbutin)과 누룩산(Kojic acid)이 효과적으로 알려져 있는 대표적인 물질이다. 그러나 알부틴은 하이드로퀴논(Hydroquinone)기로 인해 멜라노사이트에 대한 독성이 있는 것으로 알려져 있고 누룩산(Kojic acid)의 경우 2.5%의 농도에서 피부염을 유발시키는 것으로 밝혀졌으며(Nakagawa Met, 1995), 1%의 농도에서도 색소접촉 피부염을 발생시킨다는 논문이 발표되었다(Juan Garcia-Gavin et, 2010). 이러한 피부 독성과 부작용으로 인해 미백효과를 기대하는 물질들은 사용이 어려운 경우가 많다. 따라서, 최근에는 피부에 자극을 최소화하면서 우수한 미백효과를 기대할 수 있는 연구가 천연물에서 유래한 추출물 또는 정제된 미백물질을 중심으로 이루어지고 있다.Currently, arbutin and kojic acid are representative substances known to be effective for skin whitening. However, arbutin is known to be toxic to melanocytes due to its hydroquinone group, and kojic acid was found to cause dermatitis at a concentration of 2.5% (Nakagawa Met, 1995), and 1%. A paper was published showing that pigment contact dermatitis occurs even at high concentrations (Juan Garcia-Gavin et, 2010). Due to these skin toxicity and side effects, it is often difficult to use substances expected to have a whitening effect. Therefore, in recent years, research that can be expected to provide excellent whitening effects while minimizing skin irritation has been focused on extracts or purified whitening substances derived from natural products.
피부는 외부 환경으로부터 몸을 보호하여 체내 항상성을 유지하는데 중요한 역할을 한다. 그러나 끊임없는 외부의 여러 자극과 자체 대사과정 등에서 생기는 불필요한 대사산물(metabolite)에 의해 피부 기능은 저하되고 노화 현상이 촉진된다. 주름생성에 대한 원인으로 여러 가지가 보고되고 있는데, 우선 피부가 과다한 자외선에 노출되면 피부 구성성분인 콜라겐(collahen)분해가 촉진되어 피부가 탄력을 읽고 주름이 생성될 수 있다. 피부 내 콜라겐은 피부 섬유아세포에서 생성되는 구조 단백질로 노화에 의한 생성 감소 및 해당 구조의 변화는 피부의 주름 형성과 관련이 있다고 알려져 있다.그러므로 피부 내 콜라겐 생성, 멜라닌 색소 억제, 각질 줄기세포 생장에 관련된 체내 항상성은 피부의 건강 및 미용에 영향을 주는 밀접한 인자로써 이에 대한 기능과 유효 소재 발굴을 위한 연구는 여전히 활발히 진행되고 있으나, 표면에 도포하는 외용적 처치 소재의 유효성은 표피 및 진피를 통과해야 하는 기술적 어려움으로 인해 많은 노력이 요구된다.The skin plays an important role in maintaining body homeostasis by protecting the body from the external environment. However, skin function deteriorates and aging phenomenon is accelerated due to unnecessary metabolites generated from constant external stimulation and internal metabolic processes. There are several reported causes of wrinkles. First, when the skin is exposed to excessive ultraviolet rays, the breakdown of collagen, a skin component, is accelerated, which can cause the skin to lose elasticity and wrinkles to form. Collagen in the skin is a structural protein produced by skin fibroblasts, and it is known that the decrease in production and changes in the structure due to aging are related to the formation of wrinkles in the skin. Therefore, it is important for the production of collagen in the skin, suppression of melanin pigment, and growth of keratin stem cells. Homeostasis in the body is a close factor that affects the health and beauty of the skin, and research on its function and discovery of effective materials is still actively underway. However, the effectiveness of external treatment materials applied to the surface must pass through the epidermis and dermis. A lot of effort is required due to technical difficulties.
본 발명은 상기와 같은 문제점을 해결하기 위해 안출된 것으로서, 본 발명의 목적은 미백, 보습, 항산화, 항염 효과를 나타내는 화장료 조성물을 제공하는 것이다.The present invention was devised to solve the above problems, and the purpose of the present invention is to provide a cosmetic composition that exhibits whitening, moisturizing, antioxidant, and anti-inflammatory effects.
본 발명의 과제는 이상에서 언급한 과제들로 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업자에게 명확하게 이해될 수 있을 것이다.The object of the present invention is not limited to the problems mentioned above, and other problems not mentioned will be clearly understood by those skilled in the art from the description below.
상기 목적을 달성하기 위하여 본 발명은In order to achieve the above object, the present invention
제주산 원물 추출물을 함유하는 화장료 조성물을 제공한다.A cosmetic composition containing a Jeju raw material extract is provided.
또한, 상기 화장료 조성물은 영귤추출물, 진귤추출물, 하귤추출물, 당귤추출물, 금귤추출물, 만다린추출물, 유자추출물 및 레몬추출물을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 과일 추출물 3-7 중량부, 우뭇가사리추출물, 비단망사추출물, 감태추출물, 알쏭이모자반추출물, 괭생이추출물, 지충이추출물, 넓패추출물, 다시마추출물, 미역추출물, 김추출물, 꼬시래기추출물 및 개우무추출물을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 해조류 추출물 3-7 중량부, 녹차추출물, 백서향추출물, 울금추출물, 조릿대추출물, 상사화추출물, 이질풀추출물, 진득찰추출물, 케일추출물, 순비기추출물, 산야초추출물, 닥나무추출물 및 주박추출물 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 식물 추출물 3-7 중량부, 화산재추출물 및 화산토추출물을 1:1의 중량비율로 포함하는 화산추출물 1-5 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 포함한다.In addition, the cosmetic composition includes young tangerine extract, real tangerine extract, red tangerine extract, tangerine extract, kumquat extract, mandarin extract, citron extract, and lemon extract in a weight ratio of 1:1:1:1:1:1:1:1. 3-7 parts by weight of fruit extract from Jeju, agar agar extract, silk net extract, Ecklonia cava extract, Algeria snail extract, hoe extract, earthworm extract, seaweed extract, kelp extract, seaweed extract, seaweed extract, seaweed extract, and seaweed extract. 3-7 parts by weight of seaweed extract from Jeju containing agar extract at a weight ratio of 1:1:1:1:1:1:1:1:1:1:1:1, green tea extract, white persimmon extract, and turmeric extract. , Japanese bamboo extract, Moringa extract, Elephant chinensis extract, Jindeukchal extract, kale extract, Sunbigi extract, wild wild herb extract, mulberry extract and Sourdough extract 1:1:1:1:1:1:1:1:1:1:1: 3-7 parts by weight of Jeju plant extract containing a weight ratio of 1, 1-5 parts by weight of a volcanic extract containing volcanic ash extract and volcanic soil extract in a weight ratio of 1:1, 4-8 parts by weight of hyaluronic acid, and 0.5 adenosine. -4 parts by weight, niacinamide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, ascorbyl glucoside 0.3 -3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, polyglyceryl-6 stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05-0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05-0.2 parts by weight, histidine 0.05-0.2 parts by weight, sodium hyaluronate 0.05- It contains 0.2 parts by weight, hyaluronic acid 0.5-4 parts by weight, dextrin 0.5-4 parts by weight, linalool 0.5-4 parts by weight, limonene 0.5-4 parts by weight, and broccoli water 42-46 parts by weight.
또한, 본 발명은In addition, the present invention
영귤, 진귤, 하귤, 당귤, 금귤, 만다린, 유자 및 레몬을 세척하고, 적절한 크기로 자른 뒤 동결건조시키고, 분쇄하여 영귤분말, 진귤분말, 하귤분말, 당귤분말, 금귤분말, 만다린분말, 유자분말 및 레몬분말을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주과일혼합물을 준비하는 단계; 상기 제주과일혼합물 및 물을 혼합하고, 교반을 수행하며 95-105℃의 온도에서 9-15시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제1 혼합추출물을 제조하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하고, 125-135℃의 온도에서 6-12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제2 혼합추출물을 제조하는 단계; 및 상기 제1 혼합추출물 및 제2 혼합추출물을 혼합하는 단계;를 포함하는 제주산 과일 추출물을 제조하는 단계;Wash young tangerines, real tangerines, red tangerines, tangerines, kumquats, mandarins, citrons, and lemons, cut them into appropriate sizes, freeze-dry them, and grind them to make young tangerine powder, real tangerine powder, red tangerine powder, tangerine powder, kumquat powder, mandarin powder, and citron powder. and preparing a Jeju fruit mixture containing lemon powder in a weight ratio of 1:1:1:1:1:1:1:1; Mixing the Jeju fruit mixture and water, stirring, and performing primary hot water extraction at a temperature of 95-105°C for 9-15 hours; After performing the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After performing the first hot water extraction, filtering through filter paper, mixing the remaining solids with water again, and performing the second hot water extraction at a temperature of 125-135°C for 6-12 hours; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a second mixed extract; and mixing the first mixed extract and the second mixed extract; preparing a Jeju fruit extract comprising a;
우뭇가사리, 비단망사, 감태, 알쏭이모자반, 괭생이, 지충이, 넓패, 다시마, 미역, 김, 꼬시래기 및 개우무를 세척하고 동결건조한 후 분쇄하여 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 제조하는 단계; 제조된 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말 20 g을 물 200 ml와 혼합하고, 교반하면서 80℃의 온도에서 8시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 1차 혼합추출물을 제조하는 단계; 1차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 교반하면서 120℃의 온도에서 12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 2차 혼합추출물을 제조하는 단계; 2차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 여기에 [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis trifluoromethylsulfonyl)imide)를 1-2 g 첨가한 후 교반하면서 100℃의 온도에서 8시간 동안 3차 열수추출을 수행하는 단계; 3차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 3차 혼합추출물을 제조하는 단계; 및 상기 1차 혼합추출물, 2차 혼합추출물 및 3차 혼합추출물을 혼합하는 단계;를 포함하는 제주산 해조류 추출물을 제조하는 단계;Agar agar, silk mesh, gamtae, Japanese radish, ash, worms, sea kelp, kelp, seaweed, seaweed, sea radish, and radish are washed, freeze-dried, and crushed to produce agar agar powder, silk mesh powder, gamtae powder, and radish agaric. Preparing powder, hoe powder, vermicompost powder, shell powder, kelp powder, seaweed powder, seaweed powder, seaweed powder, and radish powder; Manufactured agar powder, silk mesh powder, Ecklonia cava powder, Red-eared cap powder, hoe powder, earthworm powder, shell powder, kelp powder, seaweed powder, seaweed powder, sea snail powder, and radish radish powder in a ratio of 1:1:1: 20 g of the mixed powder mixed at a weight ratio of 1:1:1:1:1:1:1:1:1 was mixed with 200 ml of water and subjected to primary hot water extraction at a temperature of 80°C for 8 hours while stirring. Steps to perform; After the first hot water extraction, filtering with filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After the first hot water extraction, filter through filter paper and mix the remaining solids with water again so that the mixing ratio of solids and water is 0.1 g/ml, and perform the second hot water extraction at a temperature of 120°C for 12 hours while stirring. steps; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary mixed extract; After secondary hot water extraction and filtering with filter paper, the remaining solids are mixed with water again so that the mixing ratio of solids and water is 0.1 g/ml, and then mixed with [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis) Adding 1-2 g of trifluoromethylsulfonyl)imide) and performing third hot water extraction at a temperature of 100°C for 8 hours while stirring; After the third hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a third mixed extract; And mixing the first mixed extract, second mixed extract, and third mixed extract; preparing a Jeju seaweed extract comprising a;
녹차, 백서향, 울금, 조릿대, 상사화, 이질풀, 진득찰, 케일, 순비기, 산야초, 닥나무 및 주박을 세척하고 동결건조한 후 분쇄하여 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 준비하는 단계; 준비된 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말을 에탄올 및 헥산을 1:1의 부피비로 혼합한 혼합 용매와 1:9의 중량비율로 혼합하고, 28-32℃의 온도에서 22-26시간 동안 추출하여 추출액을 제조하는 단계; 및 상기 추출액을 여과지로 여과하고, 여과된 여과액을 영하 50℃에서 감압농축 및 동결건조하는 단계;를 포함하는 제주산 식물 추출물을 제조하는 단계;Green tea, white paper incense, turmeric, Chinese bamboo, silkworm, cranesbill, chinensis root, kale, sunbeam, wild grass, paper mulberry, and pumpkin are washed, freeze-dried, and crushed to make green tea powder, white paper scented powder, turmeric powder, Chinese bamboo powder, silkworm powder, cranesbill powder, Preparing Jindeukchal powder, kale powder, Sunbigi powder, Sanyacho powder, mulberry tree powder, and pumpkin powder; Prepared green tea powder, white paper incense powder, turmeric powder, bamboo shoot powder, silkworm powder, dysentery powder, jadeukchal powder, kale powder, pure beige powder, Sanya herb powder, paper mulberry powder and cucurbit powder in 1:1:1:1:1:1: The mixed powder mixed at a weight ratio of 1:1:1:1:1:1 is mixed with a mixed solvent of ethanol and hexane at a volume ratio of 1:1 and mixed at a weight ratio of 1:9, and stored at 28-32°C. Preparing an extract by extracting at temperature for 22-26 hours; and filtering the extract through filter paper, concentrating and freeze-drying the filtered filtrate at -50°C under reduced pressure. Preparing a plant extract from Jeju Island, including:
화산재 및 화산토를 분쇄하여 화산재 분말 및 화산토 분말을 준비하는 단계; 준비된 화산재 분말 50 중량부, 화산토 분말 50 중량부 및 물 280-320 중량부를 혼합하여 화산혼합물을 제조하는 단계; 상기 화산혼합물을 98-102℃의 온도에서 5-7시간 동안 열수추출하는 단계; 및 열수추출 후 여과하여 여과액을 얻는 단계;를 포함하는 화산추출물을 제조하는 단계; 및Preparing volcanic ash powder and volcanic soil powder by pulverizing volcanic ash and volcanic soil; Preparing a volcanic mixture by mixing 50 parts by weight of prepared volcanic ash powder, 50 parts by weight of volcanic soil powder, and 280-320 parts by weight of water; Hydrothermal extraction of the volcanic mixture at a temperature of 98-102°C for 5-7 hours; And obtaining a filtrate by filtering after hot water extraction; Preparing a volcanic extract including; and
상기 제주산 과일 추출물 3-7 중량부, 상기 제주산 해조류 추출물 3-7 중량부, 상기 제주산 식물 추출물 3-7 중량부, 상기 화산추출물 1-5 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 혼합하는 단계;를 포함하는 화장료 조성물의 제조방법을 제공한다.3-7 parts by weight of the Jeju fruit extract, 3-7 parts by weight of the Jeju seaweed extract, 3-7 parts by weight of the Jeju plant extract, 1-5 parts by weight of the volcanic extract, 4-8 parts by weight of hyaluronic acid, Adenosine 0.5-4 parts by weight, niacinamide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, Ascorbyl Glucoside 0.3-3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, polyglyceryl-6 stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05 -0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05-0.2 parts by weight, histidine 0.05-0.2 parts by weight, sodium hyaluronate Mixing 0.05-0.2 parts by weight, 0.5-4 parts by weight of hyaluronic acid, 0.5-4 parts by weight of dextrin, 0.5-4 parts by weight of linalool, 0.5-4 parts by weight of limonene, and 42-46 parts by weight of broccoli water; It provides a method for producing a cosmetic composition comprising.
본 발명에 따른 화장료 조성물은 제주산 원물을 활용하여 제조된 것으로, 미백, 보습, 항산화, 항염 효과를 나타낸다.The cosmetic composition according to the present invention is manufactured using raw materials from Jeju Island, and exhibits whitening, moisturizing, antioxidant, and anti-inflammatory effects.
이하에서는 첨부된 다양한 실시예를 보다 상세하게 설명한다. 본 명세서에 기재된 실시예는 다양하게 변형될 수 있다. 특정한 실시예가 상세한 설명에서 자세하게 설명될 수 있다. 그러나 개시된 특정한 실시 예는 다양한 실시예를 쉽게 이해하도록 하기 위한 것일 뿐이다. 따라서 개시된 특정 실시예에 의해 기술적 사상이 제한되는 것은 아니며, 발명의 사상 및 기술 범위에 포함되는 모든 균등물 또는 대체물을 포함하는 것으로 이해되어야 한다.Hereinafter, various attached embodiments will be described in more detail. The embodiments described herein may be modified in various ways. Specific embodiments may be described in detail in the detailed description. However, the specific embodiments disclosed are only intended to facilitate understanding of the various embodiments. Accordingly, the technical idea is not limited to the specific embodiments disclosed, and should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.
1차, 2차, 제1, 제2 등과 같이 서수를 포함하는 용어는 다양한 구성요소들을 설명하는데 사용될 수 있지만, 이러한 구성요소들은 상술한 용어에 의해 한정되지는 않는다. 상술한 용어는 하나의 구성요소를 다른 구성요소로부터 구별하는 목적으로만 사용된다.Terms containing ordinal numbers, such as primary, secondary, first, second, etc., may be used to describe various components, but these components are not limited by the above-mentioned terms. The above-mentioned terms are used only for the purpose of distinguishing one component from another.
본 명세서에서, '포함한다' 또는 '가지다' 등의 용어는 명세서상에 기재된 특징, 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것이 존재함을 지정하려는 것이지, 하나 또는 그 이상의 다른 특징들이나 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것들의 존재 또는 부가 가능성을 미리 배제하지 않는 것으로 이해되어야 한다. 어떤 구성요소가 다른 구성요소에 '연결되어' 있다거나 '접속되어' 있다고 언급된 때에는, 그 다른 구성요소에 직접적으로 연결되어 있거나 또는 접속되어 있을 수도 있지만, 중간에 다른 구성요소가 존재할 수도 있다고 이해되어야 할 것이다. 반면에, 어떤 구성요소가 다른 구성요소에 '직접 연결되어' 있다거나 '직접 접속되어' 있다고 언급된 때에는, 중간에 다른 구성요소가 존재하지 않는 것으로 이해되어야 할 것이다.In this specification, terms such as 'include' or 'have' are intended to designate the presence of features, numbers, steps, operations, components, parts, or combinations thereof described in the specification, but are not intended to indicate the presence of one or more other features. It should be understood that this does not exclude in advance the possibility of the existence or addition of elements, numbers, steps, operations, components, parts, or combinations thereof. When a component is said to be 'connected' or 'connected' to another component, it is understood that it may be directly connected or connected to the other component, but that other components may exist in between. It should be. On the other hand, when a component is mentioned as being 'directly connected' or 'directly connected' to another component, it should be understood that there are no other components in between.
그 밖에도, 본 발명을 설명함에 있어서, 관련된 공지 기능 혹은 구성에 대한 구체적인 설명이 본 발명의 요지를 불필요하게 흐릴 수 있다고 판단되는 경우, 그에 대한 상세한 설명은 축약하거나 생략한다.In addition, when describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the gist of the present invention, the detailed description thereof is abbreviated or omitted.
본 발명은This invention
제주산 원물 추출물을 함유하는 화장료 조성물을 제공한다.A cosmetic composition containing a Jeju raw material extract is provided.
상기 제주산 원물은 영귤, 진귤, 하귤, 오렌지(당귤), 둥근금감(금귤), 만다린, 유자(댕유지), 레몬 등의 과일을 포함한다.The raw materials from Jeju include fruits such as young tangerines, real tangerines, red tangerines, oranges, kumquats, mandarins, yuzu, and lemons.
상기 제주산 원물은 우뭇가사리, 비단망사, 감태, 알쏭이모자반(사가숨), 괭생이, 지충이, 넓패, 다시마, 미역, 김, 우뭇가사리, 꼬시래기, 개우무 등의 해조류를 포함한다.The raw materials from Jeju include seaweeds such as agar, silk net, gamtae, sagebrush (Sagasum), snail, earthworm, seaweed, kelp, seaweed, seaweed, agar, agar, radish, and radish.
상기 제주산 원물은 녹차, 백서향(천리향), 울금, 조릿대, 상사화, 이질풀(허브로버트), 진득찰, 케일, 순비기, 산야초, 닥나무, 주박 등 의 식물을 포함한다.The raw materials from Jeju include plants such as green tea, Baekseohyang (Cheonrihyang), turmeric, bamboo shoots, silkworm, dysentery (Herb Robert), Jindeukchal, kale, Sunbigi, wild wild grass, mulberry, and pumpkin.
상기 제주산 원물은 화산재, 화산토 등을 포함한다.The raw materials from Jeju include volcanic ash, volcanic soil, etc.
상기 제주산 원물과 제주의 물을 이용하여 제조된 정제수를 혼합하고, 초음파를 가하여 초음파 추출물을 추출한다.The Jeju raw material and purified water prepared using Jeju water are mixed, and ultrasonic waves are applied to extract the ultrasonic extract.
또한, 환류공정, 디핑공정 등의 공정과, 추출온도, 추출첨가제 등을 통해 추출물의 유효성분을 극대화시킬 수 있다.In addition, the active ingredients of the extract can be maximized through processes such as reflux process and dipping process, extraction temperature, and extraction additives.
또한, 초음파추출물에 첨가제를 넣고 추출할 수 있다.Additionally, additives can be added to the ultrasonic extract and extracted.
본 발명에 따른 제주산 원물 추출물을 함유하는 화장료 조성물은 미백, 보습, 항산화, 항염 효과를 나타낸다.The cosmetic composition containing the Jeju raw material extract according to the present invention exhibits whitening, moisturizing, antioxidant, and anti-inflammatory effects.
또한, 본 발명은In addition, the present invention
영귤추출물, 진귤추출물, 하귤추출물, 당귤추출물, 금귤추출물, 만다린추출물, 유자추출물 및 레몬추출물을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 과일 추출물 3-7 중량부, 우뭇가사리추출물, 비단망사추출물, 감태추출물, 알쏭이모자반추출물, 괭생이추출물, 지충이추출물, 넓패추출물, 다시마추출물, 미역추출물, 김추출물, 꼬시래기추출물 및 개우무추출물을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 해조류 추출물 3-7 중량부, 녹차추출물, 백서향추출물, 울금추출물, 조릿대추출물, 상사화추출물, 이질풀추출물, 진득찰추출물, 케일추출물, 순비기추출물, 산야초추출물, 닥나무추출물 및 주박추출물 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 식물 추출물 3-7 중량부, 화산재추출물 및 화산토추출물을 1:1의 중량비율로 포함하는 화산추출물 1-5 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 포함하는 화장료 조성물을 제공한다.Jeju fruit extract 3 containing young tangerine extract, real tangerine extract, red tangerine extract, tangerine extract, kumquat extract, mandarin extract, citron extract, and lemon extract in a weight ratio of 1:1:1:1:1:1:1:1 -7 parts by weight, 1:1 agar agar extract, silk mesh extract, Ecklonia cava extract, Korean radish extract, hoe extract, earthworm extract, seaweed extract, kelp extract, seaweed extract, seaweed extract, seaweed extract, and radish extract. :1:1:1:1:1:1:1:1:1:1, containing 3-7 parts by weight of seaweed extract from Jeju, green tea extract, white persimmon extract, turmeric extract, bamboo shoot extract, and cypress extract. , Dysentery extract, Jindeukchal extract, kale extract, Sunbigi extract, Sanya herb extract, mulberry extract, and Sourdough extract are included in a weight ratio of 1:1:1:1:1:1:1:1:1:1:1:1. 3-7 parts by weight of Jeju plant extract, 1-5 parts by weight of volcanic extract containing volcanic ash extract and volcanic soil extract at a weight ratio of 1:1, 4-8 parts by weight of hyaluronic acid, 0.5-4 parts by weight of adenosine, niacin Amide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, ascorbyl glucoside 0.3-3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, polyglyceryl-6 stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05-0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05-0.2 parts by weight, histidine 0.05-0.2 parts by weight, sodium hyaluronate 0.05-0.2 parts by weight, hyaluronic acid Provided is a cosmetic composition comprising 0.5-4 parts by weight of ronic acid, 0.5-4 parts by weight of dextrin, 0.5-4 parts by weight of linalool, 0.5-4 parts by weight of limonene, and 42-46 parts by weight of broccoli water.
상기 화장료 조성물은 상기 화장료 조성물은 영귤추출물, 진귤추출물, 하귤추출물, 당귤추출물, 금귤추출물, 만다린추출물, 유자추출물 및 레몬추출물을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 과일 추출물 4-6 중량부, 우뭇가사리추출물, 비단망사추출물, 감태추출물, 알쏭이모자반추출물, 괭생이추출물, 지충이추출물, 넓패추출물, 다시마추출물, 미역추출물, 김추출물, 꼬시래기추출물 및 개우무추출물을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 해조류 추출물 4-6 중량부, 녹차추출물, 백서향추출물, 울금추출물, 조릿대추출물, 상사화추출물, 이질풀추출물, 진득찰추출물, 케일추출물, 순비기추출물, 산야초추출물, 닥나무추출물 및 주박추출물 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 식물 추출물 4-6 중량부, 화산재추출물 및 화산토추출물을 1:1의 중량비율로 포함하는 화산추출물 2-4 중량부, 히알루론산 5-7 중량부, 아데노신 1-3 중량부, 나이아신아마이드 1-3 중량부, 부틸렌글리콜 4-6 중량부, 글리세린 2-4 중량부, 변성알코올 2-4 중량부, 다이프로필렌글리콜 2-4 중량부, 아스코빌글루코사이드 0.5-1.5 중량부, 스쿠알란 3-5 중량부, 아스파틱애씨드 0.08-0.12 중량부, 글루타믹애씨드 0.08-0.12 중량부, 폴리글리세릴-6스테아레이트 0.08-0.12 중량부, 스테아릴알코올 0.08-0.12 중량부, 이소퀘르시트린 0.08-0.12 중량부, 글리세릴스테아레이트 0.08-0.12 중량부, 발린 0.08-0.12 중량부, 트레오닌 0.08-0.12 중량부, 히스티딘 0.08-0.12 중량부, 소듐하이알루로네이트 0.08-0.12 중량부, 하이알루로닉애씨드 1-3 중량부, 덱스트린 1-3 중량부, 리날룰 1-3 중량부, 리모넨 1-3 중량부 및 브로콜리수 43-45 중량부를 포함하는 것이 더욱 바람직하다.The cosmetic composition includes young tangerine extract, real tangerine extract, red tangerine extract, tangerine extract, kumquat extract, mandarin extract, citron extract, and lemon extract in a weight ratio of 1:1:1:1:1:1:1:1. 4-6 parts by weight of fruit extract from Jeju Island, including agar agar extract, silk net extract, Ecklonia cava extract, Ecklonia sagebrush extract, blacktail extract, earthworm extract, seaweed extract, kelp extract, seaweed extract, seaweed extract, and seaweed extract. and 4-6 parts by weight of seaweed extract from Jeju containing radish extract in a weight ratio of 1:1:1:1:1:1:1:1:1:1:1:1, green tea extract, white paper fragrant extract, Turmeric extract, Chinese bamboo extract, Moringa extract, scalene extract, Jindeukchal extract, kale extract, Sunbigi extract, wild wildflower extract, mulberry extract and Sourdough extract 1:1:1:1:1:1:1:1:1:1: 4-6 parts by weight of Jeju plant extract containing a weight ratio of 1:1, 2-4 parts by weight of a volcanic extract containing volcanic ash extract and volcanic soil extract in a weight ratio of 1:1, 5-7 parts by weight of hyaluronic acid, Adenosine 1-3 parts by weight, niacinamide 1-3 parts by weight, butylene glycol 4-6 parts by weight, glycerin 2-4 parts by weight, denatured alcohol 2-4 parts by weight, dipropylene glycol 2-4 parts by weight, ascorbyl Glucoside 0.5-1.5 parts by weight, squalane 3-5 parts by weight, aspartic acid 0.08-0.12 parts by weight, glutamic acid 0.08-0.12 parts by weight, polyglyceryl-6 stearate 0.08-0.12 parts by weight, stearyl alcohol 0.08 -0.12 parts by weight, isoquercitrin 0.08-0.12 parts by weight, glyceryl stearate 0.08-0.12 parts by weight, valine 0.08-0.12 parts by weight, threonine 0.08-0.12 parts by weight, histidine 0.08-0.12 parts by weight, sodium hyaluronate It is further recommended to contain 0.08-0.12 parts by weight, 1-3 parts by weight of hyaluronic acid, 1-3 parts by weight of dextrin, 1-3 parts by weight of linalool, 1-3 parts by weight of limonene, and 43-45 parts by weight of broccoli water. desirable.
또한, 본 발명은In addition, the present invention
영귤, 진귤, 하귤, 당귤, 금귤, 만다린, 유자 및 레몬을 세척하고, 적절한 크기로 자른 뒤 동결건조시키고, 분쇄하여 영귤분말, 진귤분말, 하귤분말, 당귤분말, 금귤분말, 만다린분말, 유자분말 및 레몬분말을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주과일혼합물을 준비하는 단계; 상기 제주과일혼합물 및 물을 혼합하고, 교반을 수행하며 95-105℃의 온도에서 9-15시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제1 혼합추출물을 제조하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하고, 125-135℃의 온도에서 6-12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제2 혼합추출물을 제조하는 단계; 및 상기 제1 혼합추출물 및 제2 혼합추출물을 혼합하는 단계;를 포함하는 제주산 과일 추출물을 제조하는 단계;Wash young tangerines, real tangerines, red tangerines, tangerines, kumquats, mandarins, citrons, and lemons, cut them into appropriate sizes, freeze-dry them, and grind them to make young tangerine powder, real tangerine powder, red tangerine powder, tangerine powder, kumquat powder, mandarin powder, and citron powder. and preparing a Jeju fruit mixture containing lemon powder in a weight ratio of 1:1:1:1:1:1:1:1; Mixing the Jeju fruit mixture and water, stirring, and performing primary hot water extraction at a temperature of 95-105°C for 9-15 hours; After performing the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After performing the first hot water extraction, filtering through filter paper, mixing the remaining solids with water again, and performing the second hot water extraction at a temperature of 125-135°C for 6-12 hours; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a second mixed extract; and mixing the first mixed extract and the second mixed extract; preparing a Jeju fruit extract comprising a;
우뭇가사리, 비단망사, 감태, 알쏭이모자반, 괭생이, 지충이, 넓패, 다시마, 미역, 김, 꼬시래기 및 개우무를 세척하고 동결건조한 후 분쇄하여 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 제조하는 단계; 제조된 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말 20 g을 물 200 ml와 혼합하고, 교반하면서 80℃의 온도에서 8시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 1차 혼합추출물을 제조하는 단계; 1차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 교반하면서 120℃의 온도에서 12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 2차 혼합추출물을 제조하는 단계; 2차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 여기에 [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis trifluoromethylsulfonyl)imide)를 1-2 g 첨가한 후 교반하면서 100℃의 온도에서 8시간 동안 3차 열수추출을 수행하는 단계; 3차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 3차 혼합추출물을 제조하는 단계; 및 상기 1차 혼합추출물, 2차 혼합추출물 및 3차 혼합추출물을 혼합하는 단계;를 포함하는 제주산 해조류 추출물을 제조하는 단계;Agar agar, silk mesh, gamtae, Japanese radish, ash, worms, sea kelp, kelp, seaweed, seaweed, sea radish, and radish are washed, freeze-dried, and crushed to produce agar agar powder, silk mesh powder, gamtae powder, and radish agaric. Preparing powder, hoe powder, vermicompost powder, shell powder, kelp powder, seaweed powder, seaweed powder, seaweed powder, and radish powder; Manufactured agar powder, silk mesh powder, Ecklonia cava powder, Red-eared cap powder, hoe powder, earthworm powder, shell powder, kelp powder, seaweed powder, seaweed powder, sea snail powder, and radish radish powder in a ratio of 1:1:1: 20 g of the mixed powder mixed at a weight ratio of 1:1:1:1:1:1:1:1:1 was mixed with 200 ml of water and subjected to primary hot water extraction at a temperature of 80°C for 8 hours while stirring. Steps to perform; After the first hot water extraction, filtering with filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After the first hot water extraction, filter through filter paper and mix the remaining solids with water again so that the mixing ratio of solids and water is 0.1 g/ml, and perform the second hot water extraction at a temperature of 120°C for 12 hours while stirring. steps; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary mixed extract; After secondary hot water extraction and filtering with filter paper, the remaining solids are mixed with water again so that the mixing ratio of solids and water is 0.1 g/ml, and then mixed with [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis) Adding 1-2 g of trifluoromethylsulfonyl)imide) and performing third hot water extraction at a temperature of 100°C for 8 hours while stirring; After the third hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a third mixed extract; And mixing the first mixed extract, second mixed extract, and third mixed extract; preparing a Jeju seaweed extract comprising a;
녹차, 백서향, 울금, 조릿대, 상사화, 이질풀, 진득찰, 케일, 순비기, 산야초, 닥나무 및 주박을 세척하고 동결건조한 후 분쇄하여 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 준비하는 단계; 준비된 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말을 에탄올 및 헥산을 1:1의 부피비로 혼합한 혼합 용매와 1:9의 중량비율로 혼합하고, 28-32℃의 온도에서 22-26시간 동안 추출하여 추출액을 제조하는 단계; 및 상기 추출액을 여과지로 여과하고, 여과된 여과액을 영하 50℃에서 감압농축 및 동결건조하는 단계;를 포함하는 제주산 식물 추출물을 제조하는 단계;Green tea, white paper incense, turmeric, Chinese bamboo, silkworm, cranesbill, chinensis root, kale, sunbeam, wild grass, paper mulberry, and pumpkin are washed, freeze-dried, and crushed to make green tea powder, white paper scented powder, turmeric powder, Chinese bamboo powder, silkworm powder, cranesbill powder, Preparing Jindeukchal powder, kale powder, Sunbigi powder, Sanyacho powder, mulberry tree powder, and pumpkin powder; Prepared green tea powder, white paper incense powder, turmeric powder, bamboo shoot powder, silkworm powder, dysentery powder, jadeukchal powder, kale powder, pure beige powder, Sanya herb powder, paper mulberry powder and cucurbit powder in 1:1:1:1:1:1: The mixed powder mixed at a weight ratio of 1:1:1:1:1:1 is mixed with a mixed solvent of ethanol and hexane at a volume ratio of 1:1 and mixed at a weight ratio of 1:9, and stored at 28-32°C. Preparing an extract by extracting at temperature for 22-26 hours; and filtering the extract through filter paper, concentrating and freeze-drying the filtered filtrate at -50°C under reduced pressure. Preparing a plant extract from Jeju Island, including:
화산재 및 화산토를 분쇄하여 화산재 분말 및 화산토 분말을 준비하는 단계; 준비된 화산재 분말 50 중량부, 화산토 분말 50 중량부 및 물 280-320 중량부를 혼합하여 화산혼합물을 제조하는 단계; 상기 화산혼합물을 98-102℃의 온도에서 5-7시간 동안 열수추출하는 단계; 및 열수추출 후 여과하여 여과액을 얻는 단계;를 포함하는 화산추출물을 제조하는 단계; 및Preparing volcanic ash powder and volcanic soil powder by pulverizing volcanic ash and volcanic soil; Preparing a volcanic mixture by mixing 50 parts by weight of prepared volcanic ash powder, 50 parts by weight of volcanic soil powder, and 280-320 parts by weight of water; Hydrothermal extraction of the volcanic mixture at a temperature of 98-102°C for 5-7 hours; And obtaining a filtrate by filtering after hot water extraction; Preparing a volcanic extract including; and
상기 제주산 과일 추출물 3-7 중량부, 상기 제주산 해조류 추출물 3-7 중량부, 상기 제주산 식물 추출물 3-7 중량부, 상기 화산추출물 1-5 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 혼합하는 단계;를 포함하는 화장료 조성물의 제조방법을 제공한다.3-7 parts by weight of the Jeju fruit extract, 3-7 parts by weight of the Jeju seaweed extract, 3-7 parts by weight of the Jeju plant extract, 1-5 parts by weight of the volcanic extract, 4-8 parts by weight of hyaluronic acid, Adenosine 0.5-4 parts by weight, niacinamide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1-5 parts by weight, dipropylene glycol 1-5 parts by weight, Ascorbyl Glucoside 0.3-3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, polyglyceryl-6 stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05 -0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05-0.2 parts by weight, histidine 0.05-0.2 parts by weight, sodium hyaluronate Mixing 0.05-0.2 parts by weight, 0.5-4 parts by weight of hyaluronic acid, 0.5-4 parts by weight of dextrin, 0.5-4 parts by weight of linalool, 0.5-4 parts by weight of limonene, and 42-46 parts by weight of broccoli water; It provides a method for producing a cosmetic composition comprising.
이하, 본 발명에 따른 화장료 조성물의 제조방법에 대하여 각 단계별로 상세히 설명한다.Hereinafter, the manufacturing method of the cosmetic composition according to the present invention will be described in detail for each step.
먼저, 본 발명에 따른 화장료 조성물의 제조방법은 제주산 과일 추출물을 제조하는 단계를 포함한다. 상기 제주산 과일 추출물을 제조하는 단계는, 영귤, 진귤, 하귤, 당귤, 금귤, 만다린, 유자 및 레몬을 세척하고, 적절한 크기로 자른 뒤 동결건조시키고, 분쇄하여 영귤분말, 진귤분말, 하귤분말, 당귤분말, 금귤분말, 만다린분말, 유자분말 및 레몬분말을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주과일혼합물을 준비하는 단계; 상기 제주과일혼합물 및 물을 혼합하고, 교반을 수행하며 95-105℃의 온도에서 9-15시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제1 혼합추출물을 제조하는 단계; 1차 열수추출을 수행하고난 후, 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하고, 125-135℃의 온도에서 6-12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 제2 혼합추출물을 제조하는 단계; 및 상기 제1 혼합추출물 및 제2 혼합추출물을 혼합하는 단계;를 포함한다.First, the method for producing a cosmetic composition according to the present invention includes preparing a Jeju fruit extract. In the step of preparing the fruit extract from Jeju, young tangerines, real tangerines, red tangerines, tangerines, kumquats, mandarins, citrons, and lemons are washed, cut into appropriate sizes, freeze-dried, and pulverized to produce young tangerine powder, real tangerine powder, and red tangerine powder; Preparing a Jeju fruit mixture containing tangerine powder, kumquat powder, mandarin powder, citron powder, and lemon powder in a weight ratio of 1:1:1:1:1:1:1:1; Mixing the Jeju fruit mixture and water, stirring, and performing primary hot water extraction at a temperature of 95-105°C for 9-15 hours; After performing the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After performing the first hot water extraction, filtering through filter paper, mixing the remaining solids with water again, and performing the second hot water extraction at a temperature of 125-135°C for 6-12 hours; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a second mixed extract; And mixing the first mixed extract and the second mixed extract.
상기와 같은 공정을 통해 제조되는 제주산 과일 추출물은 항산화, 항염 성분을 다량 포함한다.Jeju fruit extract produced through the above process contains a large amount of antioxidant and anti-inflammatory ingredients.
다음으로, 본 발명에 따른 화장료 조성물의 제조방법은 제주산 해조류 추출물을 제조하는 단계를 포함한다. 상기 제주산 해조류 추출물을 제조하는 단계는, 우뭇가사리, 비단망사, 감태, 알쏭이모자반, 괭생이, 지충이, 넓패, 다시마, 미역, 김, 꼬시래기 및 개우무를 세척하고 동결건조한 후 분쇄하여 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 제조하는 단계; 제조된 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말 20 g을 물 200 ml와 혼합하고, 교반하면서 80℃의 온도에서 8시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 1차 혼합추출물을 제조하는 단계; 1차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 교반하면서 120℃의 온도에서 12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 2차 혼합추출물을 제조하는 단계; 2차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 여기에 [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis trifluoromethylsulfonyl)imide)를 1-2 g 첨가한 후 교반하면서 100℃의 온도에서 8시간 동안 3차 열수추출을 수행하는 단계; 3차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 3차 혼합추출물을 제조하는 단계; 및 상기 1차 혼합추출물, 2차 혼합추출물 및 3차 혼합추출물을 혼합하는 단계;를 포함한다.Next, the method for producing a cosmetic composition according to the present invention includes preparing a seaweed extract from Jeju Island. In the step of preparing the seaweed extract from Jeju, agar agar, silk net, Ecklonia cava, Agar agar, Agar agar, agar, worm, sea kelp, kelp, seaweed, seaweed, sea radish, and Agar radish are washed, freeze-dried, and pulverized into agar agar powder. , manufacturing silk mesh powder, Ecklonia cava powder, Halibut powder, hoe powder, earthworm powder, seaweed powder, kelp powder, seaweed powder, seaweed powder, seaweed powder, and radish radish powder; Manufactured agar powder, silk mesh powder, Ecklonia cava powder, Red-eared cap powder, hoe powder, earthworm powder, shell powder, kelp powder, seaweed powder, seaweed powder, sea snail powder, and radish radish powder in a ratio of 1:1:1: 20 g of the mixed powder mixed at a weight ratio of 1:1:1:1:1:1:1:1:1 was mixed with 200 ml of water and subjected to primary hot water extraction at a temperature of 80°C for 8 hours while stirring. Steps to perform; After the first hot water extraction, filtering with filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After the first hot water extraction, filter through filter paper and mix the remaining solids with water again so that the mixing ratio of solids and water is 0.1 g/ml, and perform the second hot water extraction at a temperature of 120°C for 12 hours while stirring. steps; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary mixed extract; After secondary hot water extraction and filtering with filter paper, the remaining solids are mixed with water again so that the mixing ratio of solids and water is 0.1 g/ml, and then mixed with [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis) Adding 1-2 g of trifluoromethylsulfonyl)imide) and performing third hot water extraction at a temperature of 100°C for 8 hours while stirring; After the third hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a third mixed extract; And mixing the first mixed extract, second mixed extract, and third mixed extract.
상기와 같은 공정을 통해 제조되는 제주산 해조류 추출물은 항산화, 항염 성분을 다량 포함한다.Jeju seaweed extract produced through the above process contains a large amount of antioxidant and anti-inflammatory ingredients.
다음으로, 본 발명에 따른 화장료 조성물의 제조방법은 제주산 식물 추출물을 제조하는 단계를 포함한다. 상기 제주산 식물 추출물을 제조하는 단계는, 녹차, 백서향, 울금, 조릿대, 상사화, 이질풀, 진득찰, 케일, 순비기, 산야초, 닥나무 및 주박을 세척하고 동결건조한 후 분쇄하여 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 준비하는 단계; 준비된 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말을 에탄올 및 헥산을 1:1의 부피비로 혼합한 혼합 용매와 1:9의 중량비율로 혼합하고, 28-32℃의 온도에서 22-26시간 동안 추출하여 추출액을 제조하는 단계; 및 상기 추출액을 여과지로 여과하고, 여과된 여과액을 영하 50℃에서 감압농축 및 동결건조하는 단계;를 포함한다.Next, the method for producing a cosmetic composition according to the present invention includes preparing a Jeju plant extract. In the step of preparing the Jeju plant extract, green tea, white paper incense, turmeric, bamboo shoots, silkworms, cranesbill, jadeukchal, kale, sunbigi, mountain grass, paper mulberry and pumpkin are washed, freeze-dried, and then ground to produce green tea powder, white paper incense powder, and turmeric. Preparing powder, bamboo shoot powder, silkworm powder, dysentery powder, Jindeukchal powder, kale powder, Sunbigi powder, Sanyacho powder, paper mulberry powder, and pumpkin powder; Prepared green tea powder, white paper incense powder, turmeric powder, bamboo shoot powder, silkworm powder, dysentery powder, jadeukchal powder, kale powder, pure beige powder, Sanya herb powder, paper mulberry powder and cucurbit powder in 1:1:1:1:1:1: The mixed powder mixed at a weight ratio of 1:1:1:1:1:1 is mixed with a mixed solvent of ethanol and hexane at a volume ratio of 1:1 and mixed at a weight ratio of 1:9, and stored at 28-32°C. Preparing an extract by extracting at temperature for 22-26 hours; And filtering the extract with filter paper, concentrating the filtered filtrate under reduced pressure at -50°C and freeze-drying it.
상기와 같은 공정을 통해 제조되는 제주산 식물 추출물은 항산화, 항염 성분을 다량 포함한다.Jeju plant extract produced through the above process contains a large amount of antioxidant and anti-inflammatory ingredients.
다음으로, 본 발명에 따른 화장료 조성물의 제조방법은 화산추출물을 제조하는 단계를 포함한다. 상기 화산추출물을 제조하는 단계는, 화산재 및 화산토를 분쇄하여 화산재 분말 및 화산토 분말을 준비하는 단계; 준비된 화산재 분말 50 중량부, 화산토 분말 50 중량부 및 물 280-320 중량부를 혼합하여 화산혼합물을 제조하는 단계; 상기 화산혼합물을 98-102℃의 온도에서 5-7시간 동안 열수추출하는 단계; 및 열수추출 후 여과하여 여과액을 얻는 단계;를 포함한다.Next, the method for producing a cosmetic composition according to the present invention includes the step of preparing a volcanic extract. The step of preparing the volcanic extract includes pulverizing volcanic ash and volcanic soil to prepare volcanic ash powder and volcanic soil powder; Preparing a volcanic mixture by mixing 50 parts by weight of prepared volcanic ash powder, 50 parts by weight of volcanic soil powder, and 280-320 parts by weight of water; Hydrothermal extraction of the volcanic mixture at a temperature of 98-102°C for 5-7 hours; and obtaining a filtrate by filtration after hot water extraction.
다음으로, 본 발명에 따른 화장료 조성물의 제조방법은 상기 제주산 과일 추출물 3-7 중량부, 상기 제주산 해조류 추출물 3-7 중량부, 상기 제주산 식물 추출물 3-7 중량부, 상기 화산추출물 1-5 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 혼합하는 단계를 포함한다.Next, the method for producing the cosmetic composition according to the present invention is 3-7 parts by weight of the fruit extract from Jeju, 3-7 parts by weight of the seaweed extract from Jeju, 3-7 parts by weight of the plant extract from Jeju, and 1 part by weight of the volcanic extract. -5 parts by weight, hyaluronic acid 4-8 parts by weight, adenosine 0.5-4 parts by weight, niacinamide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1-5 parts by weight parts, dipropylene glycol 1-5 parts by weight, ascorbyl glucoside 0.3-3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, polyglyceryl- 6Stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05-0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05-0.2 parts by weight , histidine 0.05-0.2 parts by weight, sodium hyaluronate 0.05-0.2 parts by weight, hyaluronic acid 0.5-4 parts by weight, dextrin 0.5-4 parts by weight, linalool 0.5-4 parts by weight, limonene 0.5-4 parts by weight and mixing 42-46 parts by weight of broccoli water.
상기 혼합은 제주산 과일 추출물 4-6 중량부, 상기 제주산 해조류 추출물 4-6 중량부, 상기 제주산 식물 추출물 4-6 중량부, 상기 화산추출물 2-4 중량부, 히알루론산 5-7 중량부, 아데노신 1-3 중량부, 나이아신아마이드 1-3 중량부, 부틸렌글리콜 4-6 중량부, 글리세린 2-4 중량부, 변성알코올 2-4 중량부, 다이프로필렌글리콜 2-4 중량부, 아스코빌글루코사이드 0.5-1.5 중량부, 스쿠알란 3-5 중량부, 아스파틱애씨드 0.08-0.12 중량부, 글루타믹애씨드 0.08-0.12 중량부, 폴리글리세릴-6스테아레이트 0.08-0.12 중량부, 스테아릴알코올 0.08-0.12 중량부, 이소퀘르시트린 0.08-0.12 중량부, 글리세릴스테아레이트 0.08-0.12 중량부, 발린 0.08-0.12 중량부, 트레오닌 0.08-0.12 중량부, 히스티딘 0.08-0.12 중량부, 소듐하이알루로네이트 0.08-0.12 중량부, 하이알루로닉애씨드 1-3 중량부, 덱스트린 1-3 중량부, 리날룰 1-3 중량부, 리모넨 1-3 중량부 및 브로콜리수 43-45 중량부를 사용하여 수행하는 것이 더욱 바람직하다.The mixture includes 4-6 parts by weight of fruit extract from Jeju, 4-6 parts by weight of seaweed extract from Jeju, 4-6 parts by weight of plant extract from Jeju, 2-4 parts by weight of volcanic extract, and 5-7 parts by weight of hyaluronic acid. parts, adenosine 1-3 parts by weight, niacinamide 1-3 parts by weight, butylene glycol 4-6 parts by weight, glycerin 2-4 parts by weight, denatured alcohol 2-4 parts by weight, dipropylene glycol 2-4 parts by weight, Ascorbyl glucoside 0.5-1.5 parts by weight, squalane 3-5 parts by weight, aspartic acid 0.08-0.12 parts by weight, glutamic acid 0.08-0.12 parts by weight, polyglyceryl-6 stearate 0.08-0.12 parts by weight, stearyl Alcohol 0.08-0.12 parts by weight, isoquercitrin 0.08-0.12 parts by weight, glyceryl stearate 0.08-0.12 parts by weight, valine 0.08-0.12 parts by weight, threonine 0.08-0.12 parts by weight, histidine 0.08-0.12 parts by weight, sodium hyaluronate Using 0.08-0.12 parts by weight of Ronate, 1-3 parts by weight of Hyaluronic Acid, 1-3 parts by weight of Dextrin, 1-3 parts by weight of Linalool, 1-3 parts by weight of Limonene, and 43-45 parts by weight of broccoli water. It is more desirable to carry out
또한, 상기 화장료 조성물은 오미자씨 발효추출물 및 메밀씨 발효추출물을 0.3-3 중량부 포함하는 것이 더욱 바람직하다.In addition, it is more preferable that the cosmetic composition contains 0.3-3 parts by weight of fermented Schisandra chinensis seed extract and fermented buckwheat seed extract.
상기 오미자씨 발효추출물 및 메밀씨 발효추출물은, 오미자씨 및 메밀씨를 끓인 물로 세척하고, 분쇄하여 오미자씨분말 및 메밀씨분말을 준비하는 단계; 오미자씨분말 18-22 중량부, 메밀씨분말 18-22 중량부 및 물 58-62 중량부를 혼합하여 혼합물을 제조하고, 혼합물에 효모균으로 사카로미케스 케레비시아이(Saccharomyces cerevisiae) 1 중량부를 첨가한 후 38-42℃의 온도에서 34-38시간 동안 발효시키는 단계; 발효된 혼합물 및 부틸렌글리콜을 혼합하고, 28-32℃의 온도에서 4-6일 동안 교반하여 추출물을 제조하는 단계; 및 상기 추출물을 여과 및 감압농축한 후 동결건조하는 단계;를 수행하여 제조되는 것을 사용한다.The fermented Schisandra seed extract and the fermented buckwheat seed extract include the steps of washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; and filtering and concentrating the extract under reduced pressure and then freeze-drying the extract.
이하, 본 발명을 하기의 실시예에 의해 보다 상세하게 설명한다.Hereinafter, the present invention will be explained in more detail by the following examples.
단, 하기 실시예는 본 발명의 내용을 예시하는 것일 뿐 발명의 범위가 실시예 및 실험예에 의해 한정되는 것은 아니다.However, the following examples only illustrate the content of the present invention and the scope of the invention is not limited by the examples and experimental examples.
<실시예 1> 화장료 조성물의 제조-1<Example 1> Preparation of cosmetic composition-1
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영귤추출물, 진귤추출물, 하귤추출물, 당귤추출물, 금귤추출물, 만다린추출물, 유자추출물 및 레몬추출물을 1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 과일 추출물 5 중량부, 우뭇가사리추출물, 비단망사추출물, 감태추출물, 알쏭이모자반추출물, 괭생이추출물, 지충이추출물, 넓패추출물, 다시마추출물, 미역추출물, 김추출물, 꼬시래기추출물 및 개우무추출물을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 해조류 추출물 5 중량부, 녹차추출물, 백서향추출물, 울금추출물, 조릿대추출물, 상사화추출물, 이질풀추출물, 진득찰추출물, 케일추출물, 순비기추출물, 산야초추출물, 닥나무추출물 및 주박추출물 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 포함하는 제주산 식물 추출물 5 중량부, 화산재추출물 및 화산토추출물을 1:1의 중량비율로 포함하는 화산추출물 3 중량부, 히알루론산 6 중량부, 아데노신 2 중량부, 나이아신아마이드 2 중량부, 부틸렌글리콜 5 중량부, 글리세린 3 중량부, 변성알코올 3 중량부, 다이프로필렌글리콜 3 중량부, 아스코빌글루코사이드 1 중량부, 스쿠알란 4 중량부, 아스파틱애씨드 0.1 중량부, 글루타믹애씨드 0.1 중량부, 폴리글리세릴-6스테아레이트 0.1 중량부, 스테아릴알코올 0.1 중량부, 이소퀘르시트린 0.1 중량부, 글리세릴스테아레이트 0.1 중량부, 발린 0.1 중량부, 트레오닌 0.1 중량부, 히스티딘 0.1 중량부, 소듐하이알루로네이트 0.1 중량부, 하이알루로닉애씨드 2 중량부, 덱스트린 2 중량부, 리날룰 2 중량부, 리모넨 2 중량부 및 브로콜리수 44 중량부를 혼합하여 화장료 조성물을 제조하였다.Jeju fruit extract 5 containing young tangerine extract, real tangerine extract, red tangerine extract, tangerine extract, kumquat extract, mandarin extract, citron extract, and lemon extract in a weight ratio of 1:1:1:1:1:1:1:1 1:1:1 by weight: agar agar extract, silk mesh extract, Ecklonia cava extract, snail extract, hoe extract, earthworm extract, seaweed extract, kelp extract, seaweed extract, seaweed extract, sea radish extract, and radish extract. :1:1:1:1:1:1:1:1:1: 5 parts by weight of marine algae extract from Jeju, green tea extract, white persimmon extract, turmeric extract, bamboo shoot extract, Euphorbia extract, E. coli extract, Plants produced in Jeju, including glutinous rice extract, kale extract, sunbeam extract, wild wildflower extract, mulberry extract, and pumpkin extract in a weight ratio of 1:1:1:1:1:1:1:1:1:1:1:1:1 5 parts by weight of extract, 3 parts by weight of volcanic extract containing volcanic ash extract and volcanic soil extract in a weight ratio of 1:1, 6 parts by weight of hyaluronic acid, 2 parts by weight of adenosine, 2 parts by weight of niacinamide, 5 parts by weight of butylene glycol, 3 parts by weight of glycerin, 3 parts by weight of denatured alcohol, 3 parts by weight of dipropylene glycol, 1 part by weight of ascorbyl glucoside, 4 parts by weight of squalane, 0.1 part by weight of aspartic acid, 0.1 part by weight of glutamic acid, polyglyceryl-6 0.1 part by weight of stearate, 0.1 part by weight of stearyl alcohol, 0.1 part by weight of isoquercitrin, 0.1 part by weight of glyceryl stearate, 0.1 part by weight of valine, 0.1 part by weight of threonine, 0.1 part by weight of histidine, 0.1 part by weight of sodium hyaluronate. A cosmetic composition was prepared by mixing 2 parts by weight of hyaluronic acid, 2 parts by weight of dextrin, 2 parts by weight of linalool, 2 parts by weight of limonene, and 44 parts by weight of broccoli water.
<실시예 2> 화장료 조성물의 제조-2<Example 2> Preparation of cosmetic composition-2
상기 실시예 1에서 혼합 시 오미자씨 발효추출물 및 메밀씨 발효추출물을 1 중량부 더 첨가하여 혼합한 것을 제외하고 상기 실시예 1과 동일하게 수행하여 화장료 조성물을 제조하였다.A cosmetic composition was prepared in the same manner as in Example 1, except that 1 part by weight of fermented Schisandra seed extract and fermented buckwheat seed extract were added and mixed in Example 1.
<실험예 1> <Experimental Example 1>
1. 피부 주름 개선 효과1. Skin wrinkle improvement effect
상기 실시예 1 및 실시예 2에서 제조된 화장료 조성물의 피부 주름 개선 효과를 확인하기 위하여 다음과 같은 실험을 수행하였다. 구체적으로, 연령이 40-50대인 피시험자 30명 각각은 아침과 저녁으로 매일 2회에 걸쳐 약 3-4 g의 화장료 조성물을 얼굴에 고루 펴서 바르는 식으로 35일간 시험을 실시하였다. 35일의 시험 종료 후에 주름 개선의 정도를 관찰자의 육안을 이용하여 평가하였다. 주름 개선의 정도는 아래와 같이 1-4번 항목으로 평가하였고, 그 결과를 하기 표 1에 나타내었다.The following experiment was performed to confirm the skin wrinkle improvement effect of the cosmetic composition prepared in Examples 1 and 2 above. Specifically, each of 30 test subjects in their 40s and 50s was tested for 35 days by spreading about 3-4 g of the cosmetic composition evenly on the face twice a day, morning and evening. After completion of the 35-day test, the degree of wrinkle improvement was evaluated using the observer's naked eye. The degree of wrinkle improvement was evaluated using items 1 to 4 as follows, and the results are shown in Table 1 below.
1번 : 주름 개선이 전혀 나타나지 않음No. 1: No improvement in wrinkles appears at all
2번 : 주름 개선이 이루어지기는 하였으나, 크게 변화를 못느낌No. 2: Wrinkles were improved, but no significant change was felt.
3번 : 주름 개선 효과가 우수하며, 변화를 느낌No. 3: Excellent wrinkle improvement effect, feel the change
4번 : 주름 개선 효과가 확연히 우수함No. 4: The wrinkle improvement effect is clearly excellent.
상기 표 1에 나타낸 바와 같이, 주름 개선 효과가 우수함을 확인할 수 있었다.As shown in Table 1 above, it was confirmed that the wrinkle improvement effect was excellent.
2. 보습 효과2. Moisturizing effect
상기 실시예 1 및 실시예 2에서 제조된 화장료 조성물의 보습 효과를 확인하기 위하여 다음과 같은 실험을 수행하였다. 설문 조사를 통하여 피부가 건조하다고 느끼는 건강한 성인남녀 100명을 무작위로 선정하여 실시예 1 및 실시예 2의 화장료 조성물을 각각 1일 2회씩 8주간 안면에 도포한 후 물로 씻어 냈다. 보습 효과는 실사용 시험 시작 후부터 매 1주간, 그리고 종료 후의 개선 효과를 수분 함유량 측정기기인 corneometer CM 820(Corage +Khazaka, Germany)를 이용하여 평가하였다. 보습 효과 측정 결과를 하기 표 2에 나타내었다.The following experiment was performed to confirm the moisturizing effect of the cosmetic compositions prepared in Examples 1 and 2. Through a survey, 100 healthy adult men and women who felt that their skin was dry were randomly selected and the cosmetic compositions of Examples 1 and 2 were applied to their faces twice a day for 8 weeks, respectively, and then washed off with water. The moisturizing effect was evaluated every week from the start of the actual use test, and the improvement effect after the end was evaluated using corneometer CM 820 (Corage + Khazaka, Germany), a moisture content measuring device. The moisturizing effect measurement results are shown in Table 2 below.
상기 표 2에 나타낸 바와 같이, 보습 효과가 우수함을 확인할 수 있었다.As shown in Table 2 above, it was confirmed that the moisturizing effect was excellent.
3. 미백 효과3. Whitening effect
상기 실시예 1 및 실시예 2에서 제조된 화장료 조성물의 미백 효과를 확인하기 위하여 30명의 건강한 30-40세 여성을 무작위로 3개 군으로 나누어 실시예 1 및 실시예 2의 피부 미백용 화장료 조성물을 매일 아침, 저녁 2회씩 세안 후 안면 좌측 부위와 안면 우측 부위에 적당량을 2개월간 연속적으로 도포하게 하였다.In order to confirm the whitening effect of the cosmetic composition prepared in Example 1 and Example 2, 30 healthy women aged 30 to 40 were randomly divided into three groups and treated with the cosmetic composition for skin whitening of Example 1 and Example 2. After washing the face twice every morning and evening, an appropriate amount was applied to the left and right sides of the face continuously for two months.
피부 미백 효과는 실험 개시 1개월 후 및 실험 종료 후의 안면의 개선 정도를 관찰하여 효과가 나타난 실험 대상자의 인원수로써 개선 효과를 평가하였다. 상기 실험 결과는 하기 표 3에 나타내었다.The skin whitening effect was evaluated by observing the degree of facial improvement one month after the start of the experiment and after the end of the experiment, and measuring the number of test subjects who showed the effect. The experimental results are shown in Table 3 below.
(명)available
(number of people)
(명)slightly valid
(number of people)
(명)invalidity
(number of people)
(%)effective rate
(%)
상기 표 3에 나타낸 바와 같이, 미백 효과가 우수함을 확인할 수 있었다.As shown in Table 3 above, it was confirmed that the whitening effect was excellent.
Claims (2)
우뭇가사리, 비단망사, 감태, 알쏭이모자반, 괭생이, 지충이, 넓패, 다시마, 미역, 김, 꼬시래기 및 개우무를 세척하고 동결건조한 후 분쇄하여 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 제조하는 단계; 제조된 우뭇가사리분말, 비단망사분말, 감태분말, 알쏭이모자반분말, 괭생이분말, 지충이분말, 넓패분말, 다시마분말, 미역분말, 김분말, 꼬시래기분말 및 개우무분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말 20 g을 물 200 ml와 혼합하고, 교반하면서 80℃의 온도에서 8시간 동안 1차 열수추출을 수행하는 단계; 1차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 1차 혼합추출물을 제조하는 단계; 1차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 교반하면서 120℃의 온도에서 12시간 동안 2차 열수추출을 수행하는 단계; 2차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 2차 혼합추출물을 제조하는 단계; 2차 열수추출 후 여과지로 여과한 다음 남은 고형물을 다시 물과 혼합하되, 고형물 및 물의 혼합비율이 0.1 g/ml가 되도록 혼합하고, 여기에 [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis trifluoromethylsulfonyl)imide)를 1-2 g 첨가한 후 교반하면서 100℃의 온도에서 8시간 동안 3차 열수추출을 수행하는 단계; 3차 열수추출 후, 여과지로 여과한 다음 그 여액을 동결건조하여 3차 혼합추출물을 제조하는 단계; 및 상기 1차 혼합추출물, 2차 혼합추출물 및 3차 혼합추출물을 혼합하는 단계;를 포함하는 제주산 해조류 추출물을 제조하는 단계;
녹차, 백서향, 울금, 조릿대, 상사화, 이질풀, 진득찰, 케일, 순비기, 산야초, 닥나무 및 주박을 세척하고 동결건조한 후 분쇄하여 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 준비하는 단계; 준비된 녹차분말, 백서향분말, 울금분말, 조릿대분말, 상사화분말, 이질풀분말, 진득찰분말, 케일분말, 순비기분말, 산야초분말, 닥나무분말 및 주박분말을 1:1:1:1:1:1:1:1:1:1:1:1의 중량비율로 혼합한 혼합분말을 에탄올 및 헥산을 1:1의 부피비로 혼합한 혼합 용매와 1:9의 중량비율로 혼합하고, 28-32℃의 온도에서 22-26시간 동안 추출하여 추출액을 제조하는 단계; 및 상기 추출액을 여과지로 여과하고, 여과된 여과액을 영하 50℃에서 감압농축 및 동결건조하는 단계;를 포함하는 제주산 식물 추출물을 제조하는 단계;
화산재 및 화산토를 분쇄하여 화산재 분말 및 화산토 분말을 준비하는 단계; 준비된 화산재 분말 50 중량부, 화산토 분말 50 중량부 및 물 280-320 중량부를 혼합하여 화산혼합물을 제조하는 단계; 상기 화산혼합물을 98-102℃의 온도에서 5-7시간 동안 열수추출하는 단계; 및 열수추출 후 여과하여 여과액을 얻는 단계;를 포함하는 화산추출물을 제조하는 단계;
오미자씨 및 메밀씨를 끓인 물로 세척하고, 분쇄하여 오미자씨분말 및 메밀씨분말을 준비하는 단계; 오미자씨분말 18-22 중량부, 메밀씨분말 18-22 중량부 및 물 58-62 중량부를 혼합하여 혼합물을 제조하고, 혼합물에 효모균으로 사카로미케스 케레비시아이(Saccharomyces cerevisiae) 1 중량부를 첨가한 후 38-42℃의 온도에서 34-38시간 동안 발효시키는 단계; 발효된 혼합물 및 부틸렌글리콜을 혼합하고, 28-32℃의 온도에서 4-6일 동안 교반하여 추출물을 제조하는 단계; 및 상기 추출물을 여과 및 감압농축한 후 동결건조하는 단계;를 포함하는 오미자씨 발효추출물 및 메밀씨 발효추출물을 제조하는 단계; 및
상기 제주산 과일 추출물 3-7 중량부, 상기 제주산 해조류 추출물 3-7 중량부, 상기 제주산 식물 추출물 3-7 중량부, 상기 화산추출물 1-5 중량부, 상기 오미자씨 발효추출물 및 메밀씨 발효추출물 0.3-3 중량부, 히알루론산 4-8 중량부, 아데노신 0.5-4 중량부, 나이아신아마이드 0.5-4 중량부, 부틸렌글리콜 3-7 중량부, 글리세린 1-5 중량부, 변성알코올 1-5 중량부, 다이프로필렌글리콜 1-5 중량부, 아스코빌글루코사이드 0.3-3 중량부, 스쿠알란 2-6 중량부, 아스파틱애씨드 0.05-0.2 중량부, 글루타믹애씨드 0.05-0.2 중량부, 폴리글리세릴-6스테아레이트 0.05-0.2 중량부, 스테아릴알코올 0.05-0.2 중량부, 이소퀘르시트린 0.05-0.2 중량부, 글리세릴스테아레이트 0.05-0.2 중량부, 발린 0.05-0.2 중량부, 트레오닌 0.05-0.2 중량부, 히스티딘 0.05-0.2 중량부, 소듐하이알루로네이트 0.05-0.2 중량부, 하이알루로닉애씨드 0.5-4 중량부, 덱스트린 0.5-4 중량부, 리날룰 0.5-4 중량부, 리모넨 0.5-4 중량부 및 브로콜리수 42-46 중량부를 혼합하는 단계;를 포함하는 화장료 조성물의 제조방법.Young tangerines, real tangerines, red tangerines, tangerines, kumquats, mandarins, citrons, and lemons are washed, cut, freeze-dried, and crushed to make young tangerine powder, real tangerine powder, red tangerine powder, tangerine powder, kumquat powder, mandarin powder, citron powder, and lemon. Preparing a Jeju fruit mixture containing powder in a weight ratio of 1:1:1:1:1:1:1:1; Mixing the Jeju fruit mixture and water, stirring, and performing primary hot water extraction at a temperature of 95-105°C for 9-15 hours; After performing the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After performing the first hot water extraction, filtering through filter paper, mixing the remaining solids with water again, and performing the second hot water extraction at a temperature of 125-135°C for 6-12 hours; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a second mixed extract; and mixing the first mixed extract and the second mixed extract; preparing a Jeju fruit extract comprising a;
Agar agar, silk mesh, gamtae, Japanese radish, ash, worms, sea kelp, kelp, seaweed, seaweed, sea radish, and radish are washed, freeze-dried, and crushed to produce agar agar powder, silk mesh powder, gamtae powder, and radish agaric. Preparing powder, hoe powder, vermicompost powder, shell powder, kelp powder, seaweed powder, seaweed powder, seaweed powder, and radish powder; Manufactured agar powder, silk mesh powder, Ecklonia cava powder, Red-eared cap powder, hoe powder, earthworm powder, shell powder, kelp powder, seaweed powder, seaweed powder, sea snail powder, and radish radish powder in a ratio of 1:1:1: 20 g of the mixed powder mixed at a weight ratio of 1:1:1:1:1:1:1:1:1 was mixed with 200 ml of water and subjected to primary hot water extraction at a temperature of 80°C for 8 hours while stirring. Steps to perform; After the first hot water extraction, filtering with filter paper and then freeze-drying the filtrate to prepare a first mixed extract; After the first hot water extraction, filter through filter paper and mix the remaining solids with water again so that the mixing ratio of solids and water is 0.1 g/ml, and perform the second hot water extraction at a temperature of 120°C for 12 hours while stirring. steps; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary mixed extract; After secondary hot water extraction and filtering with filter paper, the remaining solids are mixed with water again so that the mixing ratio of solids and water is 0.1 g/ml, and then mixed with [BMIm][TFSI](1-Butyl-3-methylimidazoliumbis) Adding 1-2 g of trifluoromethylsulfonyl)imide) and performing third hot water extraction at a temperature of 100°C for 8 hours while stirring; After the third hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a third mixed extract; And mixing the first mixed extract, second mixed extract, and third mixed extract; preparing a Jeju seaweed extract comprising a;
Green tea, white paper incense, turmeric, Chinese bamboo, silkworm, cranesbill, chinensis root, kale, sunbeam, wild grass, paper mulberry, and pumpkin are washed, freeze-dried, and crushed to make green tea powder, white paper scented powder, turmeric powder, Chinese bamboo powder, silkworm powder, cranesbill powder, Preparing Jindeukchal powder, kale powder, Sunbigi powder, Sanyacho powder, mulberry tree powder, and pumpkin powder; Prepared green tea powder, white paper incense powder, turmeric powder, bamboo shoot powder, silkworm powder, dysentery powder, jadeukchal powder, kale powder, pure beige powder, Sanya herb powder, paper mulberry powder and cucurbit powder in 1:1:1:1:1:1: The mixed powder mixed at a weight ratio of 1:1:1:1:1:1 is mixed with a mixed solvent of ethanol and hexane at a volume ratio of 1:1 and mixed at a weight ratio of 1:9, and stored at 28-32°C. Preparing an extract by extracting at temperature for 22-26 hours; and filtering the extract through filter paper, concentrating and freeze-drying the filtered filtrate at -50°C under reduced pressure. Preparing a plant extract from Jeju Island, including:
Preparing volcanic ash powder and volcanic soil powder by pulverizing volcanic ash and volcanic soil; Preparing a volcanic mixture by mixing 50 parts by weight of prepared volcanic ash powder, 50 parts by weight of volcanic soil powder, and 280-320 parts by weight of water; Hydrothermal extraction of the volcanic mixture at a temperature of 98-102°C for 5-7 hours; And obtaining a filtrate by filtering after hot water extraction; Preparing a volcanic extract including;
Washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; And filtering and concentrating the extract under reduced pressure and then freeze-drying; preparing a fermented Schisandra seed extract and a fermented buckwheat seed extract including; and
3-7 parts by weight of the Jeju fruit extract, 3-7 parts by weight of the Jeju seaweed extract, 3-7 parts by weight of the Jeju plant extract, 1-5 parts by weight of the volcanic extract, the Schisandra chinensis seed fermented extract and buckwheat seed Fermentation extract 0.3-3 parts by weight, hyaluronic acid 4-8 parts by weight, adenosine 0.5-4 parts by weight, niacinamide 0.5-4 parts by weight, butylene glycol 3-7 parts by weight, glycerin 1-5 parts by weight, denatured alcohol 1 -5 parts by weight, dipropylene glycol 1-5 parts by weight, ascorbyl glucoside 0.3-3 parts by weight, squalane 2-6 parts by weight, aspartic acid 0.05-0.2 parts by weight, glutamic acid 0.05-0.2 parts by weight, poly Glyceryl-6 stearate 0.05-0.2 parts by weight, stearyl alcohol 0.05-0.2 parts by weight, isoquercitrin 0.05-0.2 parts by weight, glyceryl stearate 0.05-0.2 parts by weight, valine 0.05-0.2 parts by weight, threonine 0.05- 0.2 parts by weight, histidine 0.05-0.2 parts by weight, sodium hyaluronate 0.05-0.2 parts by weight, hyaluronic acid 0.5-4 parts by weight, dextrin 0.5-4 parts by weight, linalool 0.5-4 parts by weight, limonene 0.5 - A method of producing a cosmetic composition comprising mixing 4 parts by weight and 42-46 parts by weight of broccoli water.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130023326A (en) * | 2013-02-17 | 2013-03-07 | 주식회사 내추럴솔루션 | Cosmetic composition containing the sargassum fulvellum, gelidium cartilagineum and hixikia fusiforme okamura extracts |
| KR101716106B1 (en) * | 2016-04-18 | 2017-04-06 | 주식회사 단정바이오 | Seaweed mixed fermentation with an anti-inflammatory, anti-allergic and atopic skin improvement, a preparation method thereof and a cosmetic composition of the same |
| KR20210047689A (en) * | 2019-10-22 | 2021-04-30 | 주식회사 단정바이오 | Cosmetic composition having skin moisturizing, skin calming, anti-oxidant and anti-inflammatory effects which comprise mixed seaweeds |
| KR102453269B1 (en) * | 2022-07-18 | 2022-10-11 | 주식회사 뷰티앤코스 | Cosmetic composition containing starfish extract and hydrolyzed collagen as active ingredients to improve skin wrinkles, promote collagen synthesis, and moisturize |
| KR102496399B1 (en) * | 2022-09-29 | 2023-02-06 | 단국대학교 천안캠퍼스 산학협력단 | Pharmaceutical composition for the prevention or treatment of respiratory diseases comprising seaweed complex extract as an active ingredient |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130023326A (en) * | 2013-02-17 | 2013-03-07 | 주식회사 내추럴솔루션 | Cosmetic composition containing the sargassum fulvellum, gelidium cartilagineum and hixikia fusiforme okamura extracts |
| KR101716106B1 (en) * | 2016-04-18 | 2017-04-06 | 주식회사 단정바이오 | Seaweed mixed fermentation with an anti-inflammatory, anti-allergic and atopic skin improvement, a preparation method thereof and a cosmetic composition of the same |
| KR20210047689A (en) * | 2019-10-22 | 2021-04-30 | 주식회사 단정바이오 | Cosmetic composition having skin moisturizing, skin calming, anti-oxidant and anti-inflammatory effects which comprise mixed seaweeds |
| KR102453269B1 (en) * | 2022-07-18 | 2022-10-11 | 주식회사 뷰티앤코스 | Cosmetic composition containing starfish extract and hydrolyzed collagen as active ingredients to improve skin wrinkles, promote collagen synthesis, and moisturize |
| KR102496399B1 (en) * | 2022-09-29 | 2023-02-06 | 단국대학교 천안캠퍼스 산학협력단 | Pharmaceutical composition for the prevention or treatment of respiratory diseases comprising seaweed complex extract as an active ingredient |
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