KR102546391B1 - 열가소성 중합체용 내식성 난연제 제형 - Google Patents

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Publication number

KR102546391B1

KR102546391B1 KR1020187002208A KR20187002208A KR102546391B1 KR 102546391 B1 KR102546391 B1 KR 102546391B1 KR 1020187002208 A KR1020187002208 A KR 1020187002208A KR 20187002208 A KR20187002208 A KR 20187002208A KR 102546391 B1 KR102546391 B1 KR 102546391B1

Authority

KR

South Korea

Prior art keywords

flame retardant

weight

acid

formula

polymer

Prior art date

2015-06-24

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• 239000000203 mixture Substances 0.000 title claims abstract description 97
• 239000003063 flame retardant Substances 0.000 title claims abstract description 81
• RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 66
• 238000009472 formulation Methods 0.000 title claims abstract description 32
• 229920001169 thermoplastic Polymers 0.000 title claims abstract description 27
• 238000005260 corrosion Methods 0.000 title abstract description 16
• 230000007797 corrosion Effects 0.000 title abstract description 15
• ACVYVLVWPXVTIT-UHFFFAOYSA-N phosphinic acid Chemical class O[PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-N 0.000 claims abstract description 17
• QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims abstract description 11
• 125000003118 aryl group Chemical group 0.000 claims abstract description 6
• 229910052791 calcium Inorganic materials 0.000 claims abstract description 6
• 229910052782 aluminium Inorganic materials 0.000 claims abstract description 5
• 229910052787 antimony Inorganic materials 0.000 claims abstract description 4
• 229910052749 magnesium Inorganic materials 0.000 claims abstract description 4
• 229910052748 manganese Inorganic materials 0.000 claims abstract description 4
• 229910052708 sodium Inorganic materials 0.000 claims abstract description 4
• 229910052718 tin Inorganic materials 0.000 claims abstract description 4
• 125000006832 (C1-C10) alkylene group Chemical group 0.000 claims abstract description 3
• 229910052732 germanium Inorganic materials 0.000 claims abstract description 3
• 229910052742 iron Inorganic materials 0.000 claims abstract description 3
• 229910052744 lithium Inorganic materials 0.000 claims abstract description 3
• 150000002829 nitrogen Chemical class 0.000 claims abstract description 3
• 229910052700 potassium Inorganic materials 0.000 claims abstract description 3
• 229910052712 strontium Inorganic materials 0.000 claims abstract description 3
• 229910052719 titanium Inorganic materials 0.000 claims abstract description 3
• 229910052726 zirconium Inorganic materials 0.000 claims abstract description 3
• -1 n-propylene Chemical group 0.000 claims description 98
• 229920000642 polymer Polymers 0.000 claims description 91
• 239000004952 Polyamide Substances 0.000 claims description 42
• 229920002647 polyamide Polymers 0.000 claims description 42
• 229920000728 polyester Polymers 0.000 claims description 42
• 150000001875 compounds Chemical class 0.000 claims description 30
• 238000000465 moulding Methods 0.000 claims description 28
• 239000000654 additive Substances 0.000 claims description 21
• 229920000877 Melamine resin Polymers 0.000 claims description 19
• 229920000388 Polyphosphate Polymers 0.000 claims description 19
• 239000001205 polyphosphate Substances 0.000 claims description 19
• 235000011176 polyphosphates Nutrition 0.000 claims description 19
• 239000004416 thermosoftening plastic Substances 0.000 claims description 19
• JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 17
• 150000002148 esters Chemical class 0.000 claims description 16
• 150000003839 salts Chemical class 0.000 claims description 16
• 239000000945 filler Substances 0.000 claims description 13
• 239000002253 acid Substances 0.000 claims description 12
• 239000000835 fiber Substances 0.000 claims description 12
• 238000000034 method Methods 0.000 claims description 12
• 238000004519 manufacturing process Methods 0.000 claims description 7
• YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 claims description 7
• YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 claims description 6
• 241000219112 Cucumis Species 0.000 claims description 6
• 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 6
• FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 6
• QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 claims description 6
• 239000012779 reinforcing material Substances 0.000 claims description 6
• 150000007513 acids Chemical class 0.000 claims description 5
• 238000000576 coating method Methods 0.000 claims description 5
• 239000000047 product Substances 0.000 claims description 5
• BNEMLSQAJOPTGK-UHFFFAOYSA-N zinc;dioxido(oxo)tin Chemical compound [Zn+2].[O-][Sn]([O-])=O BNEMLSQAJOPTGK-UHFFFAOYSA-N 0.000 claims description 5
• BPXVHIRIPLPOPT-UHFFFAOYSA-N 1,3,5-tris(2-hydroxyethyl)-1,3,5-triazinane-2,4,6-trione Chemical compound OCCN1C(=O)N(CCO)C(=O)N(CCO)C1=O BPXVHIRIPLPOPT-UHFFFAOYSA-N 0.000 claims description 4
• 125000002853 C1-C4 hydroxyalkyl group Chemical group 0.000 claims description 4
• ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 claims description 4
• 230000000996 additive effect Effects 0.000 claims description 4
• POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 4
• 239000001257 hydrogen Substances 0.000 claims description 4
• 229910052739 hydrogen Inorganic materials 0.000 claims description 4
• 125000004356 hydroxy functional group Chemical group O* 0.000 claims description 4
• ZQKXQUJXLSSJCH-UHFFFAOYSA-N melamine cyanurate Chemical compound NC1=NC(N)=NC(N)=N1.O=C1NC(=O)NC(=O)N1 ZQKXQUJXLSSJCH-UHFFFAOYSA-N 0.000 claims description 4
• XFZRQAZGUOTJCS-UHFFFAOYSA-N phosphoric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OP(O)(O)=O.NC1=NC(N)=NC(N)=N1 XFZRQAZGUOTJCS-UHFFFAOYSA-N 0.000 claims description 4
• 125000004648 C2-C8 alkenyl group Chemical group 0.000 claims description 3
• 229910019142 PO4 Inorganic materials 0.000 claims description 3
• 239000007859 condensation product Substances 0.000 claims description 3
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 3
• 235000021317 phosphate Nutrition 0.000 claims description 3
• XZTOTRSSGPPNTB-UHFFFAOYSA-N phosphono dihydrogen phosphate;1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(N)=N1.OP(O)(=O)OP(O)(O)=O XZTOTRSSGPPNTB-UHFFFAOYSA-N 0.000 claims description 3
• QVJYHZQHDMNONA-UHFFFAOYSA-N phosphoric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OP(O)(O)=O.NC1=NC(N)=NC(N)=N1.NC1=NC(N)=NC(N)=N1 QVJYHZQHDMNONA-UHFFFAOYSA-N 0.000 claims description 3
• 229920002959 polymer blend Polymers 0.000 claims description 3
• 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 3
• VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical group CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 claims description 2
• GZVHEAJQGPRDLQ-UHFFFAOYSA-N 6-phenyl-1,3,5-triazine-2,4-diamine Chemical compound NC1=NC(N)=NC(C=2C=CC=CC=2)=N1 GZVHEAJQGPRDLQ-UHFFFAOYSA-N 0.000 claims description 2
• POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 2
• CHJJGSNFBQVOTG-UHFFFAOYSA-N N-methyl-guanidine Natural products CNC(N)=N CHJJGSNFBQVOTG-UHFFFAOYSA-N 0.000 claims description 2
• 125000000217 alkyl group Chemical group 0.000 claims description 2
• 229960000458 allantoin Drugs 0.000 claims description 2
• IYABWNGZIDDRAK-UHFFFAOYSA-N allene Chemical group C=C=C IYABWNGZIDDRAK-UHFFFAOYSA-N 0.000 claims description 2
• 239000003990 capacitor Substances 0.000 claims description 2
• 238000005266 casting Methods 0.000 claims description 2
• SWSQBOPZIKWTGO-UHFFFAOYSA-N dimethylaminoamidine Natural products CN(C)C(N)=N SWSQBOPZIKWTGO-UHFFFAOYSA-N 0.000 claims description 2
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
• 239000004744 fabric Substances 0.000 claims description 2
• 125000000524 functional group Chemical group 0.000 claims description 2
• 238000005470 impregnation Methods 0.000 claims description 2
• 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 2
• 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
• 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
• 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
• 125000004957 naphthylene group Chemical group 0.000 claims description 2
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
• 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 claims description 2
• 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
• 239000004753 textile Substances 0.000 claims description 2
• 239000002023 wood Substances 0.000 claims description 2
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
• 229920002678 cellulose Polymers 0.000 claims 1
• 239000001913 cellulose Substances 0.000 claims 1
• GKTNLYAAZKKMTQ-UHFFFAOYSA-N n-[bis(dimethylamino)phosphinimyl]-n-methylmethanamine Chemical compound CN(C)P(=N)(N(C)C)N(C)C GKTNLYAAZKKMTQ-UHFFFAOYSA-N 0.000 abstract description 20
• 150000003606 tin compounds Chemical class 0.000 abstract 1
• PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 33
• 229920001577 copolymer Polymers 0.000 description 33
• 239000004677 Nylon Substances 0.000 description 19
• 229920001778 nylon Polymers 0.000 description 19
• 229920001707 polybutylene terephthalate Polymers 0.000 description 18
• LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 14
• NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 14
• 239000000463 material Substances 0.000 description 14
• 239000004417 polycarbonate Substances 0.000 description 14
• XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 13
• 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 13
• 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 13
• 229920003023 plastic Polymers 0.000 description 13
• 239000004033 plastic Substances 0.000 description 13
• 238000012360 testing method Methods 0.000 description 13
• 239000004800 polyvinyl chloride Substances 0.000 description 11
• 125000004432 carbon atom Chemical group C* 0.000 description 10
• 229920000515 polycarbonate Polymers 0.000 description 10
• 229920006324 polyoxymethylene Polymers 0.000 description 10
• 238000012545 processing Methods 0.000 description 10
• 239000003381 stabilizer Substances 0.000 description 10
• 229920001283 Polyalkylene terephthalate Polymers 0.000 description 9
• 239000004721 Polyphenylene oxide Substances 0.000 description 9
• KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 9
• 239000000314 lubricant Substances 0.000 description 9
• 229920002857 polybutadiene Polymers 0.000 description 9
• 229920000915 polyvinyl chloride Polymers 0.000 description 9
• NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 8
• 239000005062 Polybutadiene Substances 0.000 description 8
• WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 8
• 239000007795 chemical reaction product Substances 0.000 description 8
• 239000003822 epoxy resin Substances 0.000 description 8
• UTOPWMOLSKOLTQ-UHFFFAOYSA-N octacosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCC(O)=O UTOPWMOLSKOLTQ-UHFFFAOYSA-N 0.000 description 8
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• 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 7
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• NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 6
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• RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 5
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• QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 4
• 239000011777 magnesium Substances 0.000 description 4
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• 239000005995 Aluminium silicate Substances 0.000 description 3
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