KR102489350B1 - Preparation Method of peanut sprout extract And Cosmetic Composition comprising the same - Google Patents

Preparation Method of peanut sprout extract And Cosmetic Composition comprising the same Download PDF

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KR102489350B1
KR102489350B1 KR1020200184406A KR20200184406A KR102489350B1 KR 102489350 B1 KR102489350 B1 KR 102489350B1 KR 1020200184406 A KR1020200184406 A KR 1020200184406A KR 20200184406 A KR20200184406 A KR 20200184406A KR 102489350 B1 KR102489350 B1 KR 102489350B1
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sprout
peanut
weight
parts
extract
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KR20220093562A (en
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배미경
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주식회사 유아트코리아
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Abstract

본 발명은 새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물에 관한 것으로, 새싹땅콩 추출물 제조방법은, 새싹땅콩을 마련하여 데치거나 증숙시킨 후 건조하여 준비하는 (a)사전가공단계, 건조된 새싹땅콩을 세절하여 마련하는 (b)세절단계, 물에 세절된 새싹땅콩을 첨가 혼합하여 30~40℃에서 소정시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하는 (c)1차 추출단계, 상기 물과 상기 세절된 새싹땅콩과 1차로 추출된 상기 유효성분을 포함하는 혼합물에 열을 가하여 새싹땅콩에 함유된 수용성 유효성분은 2차로 추출하는 (d)2차 추출단계 및 상기 물과, 상기 세절된 새싹땅콩과, 1차 및 2차로 추출된 상기 유효성분을 포함하는 혼합물을 여과시켜, 상기 유효성분이 추출되고 잔여하는 상기 세절된 새싹땅콩을 제거하여 추출물을 제조하는 (e)여과단계를 포함하는 것을 특징으로 한다.The present invention relates to a method for preparing peanut sprout extract and a cosmetic composition comprising the peanut sprout extract prepared thereby. Processing step, (b) slicing step of preparing by cutting dried peanut sprouts, adding and mixing the chopped peanut sprouts in water and immersing them at 30-40 ° C for a predetermined time to first extract the water-soluble active ingredient contained in peanut sprouts (c) the first extraction step, heat is applied to the mixture containing the water, the chopped sprouted peanuts, and the first extracted active ingredient, and the water-soluble active ingredient contained in the sprouted peanuts is secondarily extracted (d) 2 The extract was obtained by filtering a mixture including the primary extraction step and the water, the chopped peanut sprouts, and the first and secondly extracted active ingredients to remove the remaining chopped peanut sprouts after the active ingredient was extracted. It is characterized in that it comprises the step of (e) filtration to prepare.

Description

새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물{Preparation Method of peanut sprout extract And Cosmetic Composition comprising the same}Method for manufacturing peanut sprout extract and a cosmetic composition comprising the peanut sprout extract prepared thereby

본 발명은 새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물에 관한 것으로, 더욱 상세하게는 새싹땅콩에 포함된 레스베라트롤 등의 유효성분 추출효율을 향상시킬 수 있는 새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물에 관한 것이다.The present invention relates to a method for preparing a peanut sprout extract and a cosmetic composition comprising the peanut sprout extract prepared thereby, and more particularly, to manufacturing a peanut sprout extract capable of improving the extraction efficiency of active ingredients such as resveratrol contained in peanut sprout It relates to a method and a cosmetic composition comprising the peanut sprout extract prepared thereby.

일반적으로, 새싹땅콩은 땅콩을 발아시켜 싹을 틔운 것을 말하는 것으로, 새싹땅콩은 땅콩의 싹이 발아할 때 외부의 자극으로부터 자신을 보호하기 위해 레스베라트롤 성분을 생산하게 되어, 땅콩 상태에서는 미량 포함된 레스베라트롤 성분이 새싹땅콩에는 그 90배 이상 증가하는 것으로 알려져있다.In general, sprouted peanuts refer to sprouted peanuts, and sprouted peanuts produce a resveratrol component to protect themselves from external stimuli when sprouts sprout. Ingredients are known to increase more than 90 times in sprouted peanuts.

상기와 같이 새싹땅콩은 레스베라트롤을 비롯한 유효성분으로 인해 암, 당뇨, 심장병, 관절염 등 각종 질병 예방에 효과가 있으며, 항산화 작용 또한 뛰어나다.As described above, sprouted peanuts are effective in preventing various diseases such as cancer, diabetes, heart disease, and arthritis due to active ingredients including resveratrol, and have excellent antioxidant activity.

그로 인해 최근 새싹땅콩을 식품, 의약품 및 화장품 원료로 활용하기 위한 기술개발이 활발하게 이루어지고 있는 추세이나, 새싹땅콩은 특유의 비린내와 맛으로 인해, 식품, 화장품 등의 원료로 사용하는데 어려움이 있어, 이에 대한 해결책이 필요하다.As a result, recently, technology development for using sprouted peanuts as a raw material for food, medicine, and cosmetics is actively being developed. , a solution is needed for this.

대한민국 등록특허 제2140163호(2020.07.27.등록)Korean Registered Patent No. 2140163 (registered on July 27, 2020)

본 발명은 상기의 문제점을 해결하기 위한 것으로서, 새싹땅콩의 비린내를 제거 가능하고, 더불어 새싹땅콩의 유효성분 추출 효율을 향상시킬 수 있도록 하는 새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물을 제공하는 것을 목적으로 한다.The present invention is intended to solve the above problems, and includes a method for preparing a peanut sprout extract that can remove the fishy smell of peanut sprout and improve the extraction efficiency of active ingredients of peanut sprout, and a peanut extract prepared thereby. It is an object to provide a cosmetic composition that does.

본 발명의 목적은 위에서 언급한 목적으로 제한되지 않으며, 언급되지 않은 다른 목적들은 아래의 기재로부터 명확한 이해가 될 것이다. The object of the present invention is not limited to the above-mentioned object, and other objects not mentioned will become clear from the description below.

본 발명에 따른 새싹땅콩 추출물 제조방법은, 새싹땅콩을 마련하여 증숙시킨 후 건조하여 준비하는 (a)사전가공단계, 건조된 새싹땅콩을 세절하여 마련하는 (b)세절단계, 물에 세절된 새싹땅콩을 첨가 혼합하여 40~50℃에서 5~6시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하는 (c)1차 추출단계, 상기 물과 상기 세절된 새싹땅콩과 1차로 추출된 상기 유효성분을 포함하는 혼합물에 열을 가하여 새싹땅콩에 함유된 수용성 유효성분은 2차로 추출하는 (d)2차 추출단계 및 상기 물과, 상기 세절된 새싹땅콩과, 1차 및 2차로 추출된 상기 유효성분을 포함하는 혼합물을 여과시켜, 상기 유효성분이 추출되고 잔여하는 상기 세절된 새싹땅콩을 분리 제거하여 추출물을 제조하는 (e)여과단계를 포함한다.The method for producing peanut sprout extract according to the present invention is to prepare and prepare peanut sprouts, steam them, and prepare by drying (a) pre-processing step, (b) cutting step to prepare by cutting dried peanut sprouts, sprouts cut in water (c) primary extraction step of firstly extracting the water-soluble active ingredient contained in sprouted peanuts by adding and mixing peanuts and immersing at 40 to 50 ° C for 5 to 6 hours; first extraction with the water and the chopped peanuts (d) secondary extraction step of secondly extracting the water-soluble active ingredient contained in the sprouted peanuts by applying heat to the mixture containing the active ingredient, and the water, the chopped sprouted peanuts, and the first and second extraction and (e) a filtration step of preparing an extract by filtering the mixture containing the active ingredient so as to separate and remove the chopped peanut sprouts remaining after the active ingredient is extracted.

또한, 상기 (a)사전가공단계는 마련된 새싹땅콩을 세척하는 세척단계와, 세척된 새싹땅콩을 머리부분(싹부분), 줄기부분(배축부분) 및 뿌리부분으로 분리하는 분리단계와, 분리된 새싹땅콩의 상기 머리부분(싹부분), 상기 줄기부분(배축부분) 및 상기 뿌리부분을 각각 별도로 증숙시키고, 건조하는 건조단계를 포함하는 것을 특징으로 한다.In addition, the (a) pre-processing step includes a washing step of washing the prepared peanut sprouts, a separation step of separating the washed peanut sprouts into a head part (sprout part), a stem part (hypocotyl part) and a root part, It is characterized in that it comprises a drying step of separately steaming and drying the head part (sprout part), the stem part (hypocotyl part) and the root part of the peanut sprout.

또한, 상기 건조단계는 상기 머리부분(싹부분)을 60℃에서 1시간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하는 것을 특징으로 한다.In addition, the drying step is characterized in that the head (sprout) is steamed at 60 ° C. for 1 hour and then dried by hot air drying at 60 ° C. for 1 hour.

또한, 상기 건조단계는 상기 줄기부분(배축부분)을 60℃에서 1시간 증숙시킨 후, 70℃에서 2시간 열풍건조 방식으로 건조하는 것을 특징으로 한다.In addition, the drying step is characterized in that the stem part (hycobyl part) is steamed at 60 ° C. for 1 hour and then dried by hot air drying at 70 ° C. for 2 hours.

또한, 상기 건조단계는 상기 뿌리부분을 60℃에서 1시간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하는 것을 특징으로 한다.In addition, the drying step is characterized in that the root portion is steamed at 60 ° C. for 1 hour and then dried by hot air drying at 60 ° C. for 30 minutes.

또한, 상기 (c)1차 추출단계는 상기 물 100 중량부에 대하여 상기 세절된 새싹땅콩 0.5 중량부를 첨가 혼합하는 것을 특징으로 한다.In addition, the (c) primary extraction step is characterized in that 0.5 parts by weight of the chopped peanut sprouts are added and mixed with respect to 100 parts by weight of the water.

또한, 상기 (d)2차 추출단계는 상기 혼합물에 40~100℃의 온도범위 내에서 20~40분간 점차 승온시키면서 새싹땅콩에 함유된 수용성 유효성분을 추출하고, 이후 상기 혼합물을 100~110℃의 온도에서 1~4시간 동안 새싹땅콩에 함유된 수용성 유효성분을 추출하면서 상기 혼합물을 농축시키도록 구성되는 것을 특징으로 한다.In addition, in the (d) secondary extraction step, the water-soluble active ingredient contained in sprouted peanuts is extracted while gradually raising the temperature of the mixture in the temperature range of 40 to 100 ° C for 20 to 40 minutes, and then the mixture is heated to 100 to 110 ° C. It is characterized in that it is configured to concentrate the mixture while extracting the water-soluble active ingredient contained in sprouted peanuts for 1 to 4 hours at a temperature of.

한편, 본 발명의 새싹땅콩 추출물을 포함하는 화장료 조성물은, 상기와 같은 제조방법에 의해 제조된 새싹땅콩 추출물을 포함하며, 이때, 화장료 조성물 100 중량부에 대하여 상기 새싹땅콩 추출물을 0.5~50중량부를 함유하는 것을 특징으로 한다.On the other hand, the cosmetic composition containing the peanut sprout extract of the present invention includes the peanut sprout extract prepared by the above manufacturing method, and at this time, 0.5 to 50 parts by weight of the peanut sprout extract based on 100 parts by weight of the cosmetic composition characterized in that it contains

또한, 상기 화장료 조성물은 크림, 에센스, 용액, 폼, 겔, 화장수, 유연수, 유액, 로션, 현탁액, 유탁액, 오일로 구성되는 군으로부터 선택되는 제형을 갖는 것을 특징으로 한다.In addition, the cosmetic composition is characterized by having a formulation selected from the group consisting of cream, essence, solution, foam, gel, lotion, softening water, emulsion, lotion, suspension, emulsion, and oil.

또한, 상기 화장료 조성물은 세럼 제형으로 이루어지되, 상기 세럼 제형의 화장료 조성물은 총 100중량부에 대하여, 유상성분으로 땅콩오일 15 중량부, 올리브오일 5 중량부, 라놀린 2 중량부, 올리브유화왁스 6 중량부, 솔루빌라이저 1.5 중량부를 포함하고, 수상성분은 본 발명에 의해 제조되는 새싹땅콩 추출물 50 중량부를 포함하고, 첨가물은 글리세린 5 중량부, 1.3부틸렌글리콜(1.3BG) 3 중량부, 1.2헥산디올 2 중량부, 베타글루칸 1 중량부, 세라마이드 2 중량부, D-판테놀 1 중량부, 히알루론산 1 중량부, 나이아신아마이드 3 중량부, 아데노신 2 중량부, 알부틴 2 중량부를 포함하고, 나머지 48.5 중량부는 수상성분으로 상기 새싹땅콩 추출물을 포함하여, 상기 유상성분, 수상성분, 첨가물을 혼합하여 제조되는 것을 특징으로 한다.In addition, the cosmetic composition is composed of a serum formulation, and the cosmetic composition of the serum formulation contains 15 parts by weight of peanut oil, 5 parts by weight of olive oil, 2 parts by weight of lanolin, and 6 parts by weight of olive emulsified wax as oil components, based on a total of 100 parts by weight. parts by weight, including 1.5 parts by weight of solubilizer, the aqueous phase component includes 50 parts by weight of sprout peanut extract prepared according to the present invention, and the additives include 5 parts by weight of glycerin, 3 parts by weight of 1.3 butylene glycol (1.3BG), 1.2 parts by weight of glycerin 2 parts by weight of hexanediol, 1 part by weight of beta glucan, 2 parts by weight of ceramide, 1 part by weight of D-panthenol, 1 part by weight of hyaluronic acid, 3 parts by weight of niacinamide, 2 parts by weight of adenosine, 2 parts by weight of arbutin, and the remaining 48.5 parts by weight Part by weight is characterized in that it is prepared by mixing the oil phase component, the aqueous phase component, and additives, including the sprout peanut extract as an aqueous phase component.

본 발명에 따른 새싹땅콩 추출물 제조방법 및 이에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물은, 새싹땅콩을 증숙시킨 후 건조하도록 구성되고, 증숙 및 건조 조건에 의해 비린 새싹땅콩 특유의 향을 제거 가능하고 동시에 유효성분의 추출효율 또한 향상시킬 수 있도록 하는 효과가 있다.The method for manufacturing peanut sprout extract according to the present invention and the cosmetic composition containing the peanut sprout extract prepared thereby are configured to dry sprout peanut after steaming, and can remove fishy smell peculiar to peanut sprout by steaming and drying conditions. And at the same time, there is an effect of improving the extraction efficiency of the active ingredient.

도 1은 본 발명의 실시예에 따른 새싹땅콩 추출물 제조방법의 공정을 나타내는 순서도이다.1 is a flow chart showing the process of a sprout peanut extract manufacturing method according to an embodiment of the present invention.

이상과 같은 본 발명에 해결하고자 하는 과제, 과제의 해결수단, 발명의 효과를 포함한 구체적인 사항들은 다음에 기재할 실시예 및 도면들에 포함되어 있다. 본 발명의 이점 및 특징, 그리고 그것들을 달성하는 방법은 첨부되는 도면과 함께 상세하게 후술되어 있는 실시예들을 참조하면 명확해질 것이다.The specific details, including the problems to be solved in the present invention, the means for solving the problems, and the effect of the invention as described above are included in the embodiments and drawings to be described below. Advantages and features of the present invention, and methods of achieving them, will become clear with reference to the detailed description of the following embodiments taken in conjunction with the accompanying drawings.

또한, 명세서 전체에서 어떤 부분이 어떤 구성요소를 “포함” 또는 “구비”한다고 할 때, 이는 특별히 반대되는 기재가 없는 한 다른 구성요소를 제외하는 것이 아니라 다른 구성요소를 더 포함하거나 구비할 수 있는 것을 의미한다.In addition, when a part in the entire specification "includes" or "includes" a component, this does not exclude other components unless otherwise stated, but may further include or include other components. means that

이하, 첨부된 도면을 참조하여, 본 발명의 실시예에 따른 새싹땅콩 추출물 제조방법을 보다 상세히 설명하고자 한다.Hereinafter, with reference to the accompanying drawings, a method for preparing a peanut sprout extract according to an embodiment of the present invention will be described in more detail.

도 1은 본 발명의 실시예에 따른 새싹땅콩 추출물 제조방법의 공정을 나타내는 순서도이다.1 is a flow chart showing the process of a sprout peanut extract manufacturing method according to an embodiment of the present invention.

도 1을 참조하면, 본 발명의 실시예에 따른 새싹땅콩 추출물 제조방법은 크게, (a)사전가공단계, (b)세절단계, (c)1차 추출단계, (d)2차 추출단계 및 (e)여과단계를 포함한다.Referring to Figure 1, the sprout peanut extract manufacturing method according to an embodiment of the present invention is largely, (a) pre-processing step, (b) cutting step, (c) primary extraction step, (d) secondary extraction step and (e) includes a filtration step.

우선, (a)사전가공단계는, 새싹땅콩을 마련하여 증숙시킨 후 건조하여 준비하는 단계로, 일례로, 마련된 새싹땅콩을 세척하는 세척단계와, 세척된 새싹땅콩을 증숙시키고 건조하는 건조단계를 포함할 수 있으며, 건조단계에서 세척된 새싹땅콩을 증숙시킨 후 건조시킴으로써 증숙과정을 통해 새싹땅콩 특유의 비린 향을 제거할 수 있게 되며, 이때 새싹땅콩은 60℃에서 1시간 동안 이루어지는 것이 바람직하다. 60℃보다 높은 온도에서는 증숙된 새싹땅콩에서 비린 향은 제거되나 땅콩이 익은 경우 발생되는 구수한 향이 발생되어 바람직하지 않고, 60℃보다 낮은 온도에서는 새싹땅콩의 비린 향이 충분히 제거되지 않게 되어 바람직하지 않다.First, (a) the pre-processing step is a step of preparing, steaming and drying sprouted peanuts, for example, a washing step of washing the prepared peanut sprouts and a drying step of steaming and drying the washed peanut sprouts It may be included, and by steaming and drying the sprouted peanuts washed in the drying step, it is possible to remove the peculiar smell of sprouted peanuts through the steaming process. At this time, sprouted peanuts are preferably made at 60 ° C. for 1 hour. At a temperature higher than 60 ° C, the fishy flavor of the steamed peanuts is removed, but the fragrant flavor generated when the peanuts are ripe is generated, which is undesirable, and at a temperature lower than 60 ° C, the fishy flavor of the sprouted peanuts is not sufficiently removed.

한편, 다른 예로, (a)사전가공단계는, 마련된 새싹땅콩을 세척하는 세척단계와, 세척된 새싹땅콩을 머리부분(싹부분), 줄기부분(배축부분) 및 뿌리부분으로 분리하는 분리단계와, 분리된 새싹땅콩의 상기 머리부분(싹부분), 상기 줄기부분(배축부분) 및 상기 뿌리부분을 각각 별도로 증숙시키고, 건조하는 건조단계를 포함하도록 구성될 수 있으며, 이와 같은 경우 새싹땅콩의 머리부분(싹부분), 줄기부분(배축부분) 및 뿌리부분은 각각 향과 수분 함량이 상이하므로, 부분별로 별도로 증숙 및 건조하도록 구성됨으로써, 최종적으로 제조되는 새싹땅콩 추출물의 품질 향상과 품질의 균일성 또한 향상시킬 수 있도록 한다.On the other hand, as another example, (a) the pre-processing step is a washing step of washing the prepared peanut sprouts, a separation step of separating the washed peanut sprouts into a head part (sprout part), a stem part (hypocotyl part) and a root part, , It may be configured to include a drying step of separately steaming and drying the head part (sprout part), the stem part (hypocotyl part) and the root part of the separated peanut sprout, and in this case, the head of the sprout peanut Since each part (sprout part), stem part (hypocotyl part), and root part have different fragrance and water content, each part is steamed and dried separately, thereby improving the quality and uniformity of quality of the finally prepared peanut sprout extract. It also allows you to improve.

이때, 세척단계는, 마련된 새싹땅콩을 정제수에 담가 직접 흔들거나 미세한 진동을 가하여 이물질을 새싹땅콩으로부터 분리시키거나, 흐르는 물을 이용하여 새싹땅콩에 잔여하는 이물질을 분리시켜 제거하도록 구성될 수 있으나, 이에 한정되는 것은 아니며, 이물질을 용이하게 제거할 수 있는 세척 방법이 다양하게 실시될 수 있다.At this time, the washing step may be performed by immersing the prepared sprout peanuts in purified water and shaking them directly or applying fine vibration to separate foreign substances from the sprout peanuts, or using running water to separate and remove foreign substances remaining in the sprout peanuts, It is not limited thereto, and various cleaning methods capable of easily removing foreign substances may be implemented.

이때, 상기 건조단계에서, 상기 머리부분(싹부분은)은 60℃에서 1시간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하여, 함수율 0.1~20%가 되도록 한다.At this time, in the drying step, the head (sprout) is steamed at 60 ° C. for 1 hour, and then dried by hot air drying at 60 ° C. for 1 hour, so that the moisture content is 0.1 to 20%.

또한, 상기 건조단계에서, 상기 줄기부분(배축부분)은 60℃에서 1시간 증숙시킨 후, 70℃에서 2시간 열풍건조 방식으로 건조하여, 함수율 0.1~20%가 되도록 하며, 이는 줄기부분(배축부분)은 다른 부분에 비해 수분을 많이 함유하고 있는 부분이므로, 보다 높은 온도에서 보다 긴 시간 건조가 이루어지도록 한다.In addition, in the drying step, the stem portion (hypocotyl portion) is steamed at 60° C. for 1 hour and then dried by hot air drying at 70° C. for 2 hours to have a moisture content of 0.1 to 20%, which is Part) is a part that contains more moisture than other parts, so drying is performed at a higher temperature for a longer time.

또한, 상기 건조단계에서, 상기 뿌리부분은 60℃에서 1시간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하여, 함수율 0.1~20%가 되도록 하며, 이는 뿌리부분은 다른 부분에 비해 수분을 적게 함유하고 있어, 다른 부분에 비해 적은 시간 동안 건조가 이루어지도록 한다.In addition, in the drying step, the root part is steamed at 60 ° C. for 1 hour, and then dried by hot air drying at 60 ° C. for 30 minutes to obtain a moisture content of 0.1 to 20%, which means that the root part has a moisture content compared to other parts. contains less, allowing drying to take place in a shorter period of time compared to other parts.

다음으로, (b)세절단계는, 건조된 새싹땅콩을 세절하여 마련하도록 구성된다. 이때, 새싹땅콩을 수작업에 의해 직접 절단하거나, 세절기에 투입하여 세절할 수 있으며, 이때 세절된 새싹땅콩의 크기는 0.5mm 내지 1mm로 이루어지는 것이 바람직하다. 세절된 새싹땅콩의 크기가 1mm보다 크면 새싹땅콩의 수용성 유효성분이 추출되는 성능이 저하되므로 바람직하지 않고, 세절된 새싹땅콩의 크기가 0.5mm보다 작으면 후술할 여과단계에서 세절된 새싹땅콩을 혼합물에서 분리하는 과정에서 여과가 쉽지 않게 되어 바람직하지 않다.Next, (b) the cutting step is configured to prepare by cutting the dried peanut sprouts. At this time, the sprouted peanuts can be cut directly by hand or put into a chopper and chopped. At this time, the size of the chopped peanuts is preferably made of 0.5 mm to 1 mm. If the size of the chopped sprouted peanuts is larger than 1mm, it is not preferable because the performance of extracting the water-soluble active ingredients of the sprouted peanuts is lowered, and if the size of the chopped sprouted peanuts is smaller than 0.5mm, the chopped sprouted peanuts are removed from the mixture in the filtration step to be described later. In the process of separation, filtration becomes difficult, which is not preferable.

다음으로, (c)1차 추출단계와 (d)2차 추출단계는, 새싹땅콩에 함유된 유효성분을 추출하기 위한 단계로, 특히 본 발명에서는 새싹땅콩에 함유된 레스베라트롤 성분의 추출이 필요하며, 새싹땅콩에 함유된 레스베라트롤은 수용성이므로, 이를 추출하기 위해서는, 추출용매로 오일이나 에탄올에 비하여 물을 이용하는 것이 가장 추출 효율이 높은 것으로 확인되어, 추출용매로는 물을 이용하였으며, 물은 정제수를 이용하는 것이 바람직하다.Next, (c) the first extraction step and (d) the second extraction step are steps for extracting the active ingredient contained in sprout peanuts, in particular, in the present invention, extraction of resveratrol contained in sprout peanuts is required, , Since resveratrol contained in sprouted peanuts is water-soluble, in order to extract it, it was confirmed that using water as an extraction solvent has the highest extraction efficiency compared to oil or ethanol. It is preferable to use

이때, (c)1차 추출단계는, 새싹땅콩에 함유된 유효성분을 미온수에 의해 1차로 추출하기 위한 단계로, 물에 세절된 새싹땅콩을 첨가 혼합하여 40~50℃에서 5~6시간 동안 침지시켜 둔 상태를 유지하도록 하며, 이로 인해 물에 세절된 새싹땅콩이 침지된 상태에서 새싹땅콩으로부터 물에 새싹땅콩에 함유된 수용성 유효성분이 용출되어 추출되게 되어, 물과 세절된 새싹땅콩과 1차로 추출된 유효성분을 포함하는 1차 혼합물이 제조되게 된다.At this time, (c) the first extraction step is a step for firstly extracting the active ingredient contained in sprouted peanuts with lukewarm water, by adding chopped sprouted peanuts to water and mixing them at 40 to 50 ° C for 5 to 6 hours. It is kept immersed, and as a result, the water-soluble active ingredients contained in the sprouted peanuts are eluted and extracted from the sprouted peanuts in the state in which the chopped sprouted peanuts are immersed in water, and the water and the chopped sprouted peanuts are firstly extracted. A primary mixture containing the extracted active ingredient is prepared.

이때, 물 100중량부에 대하여 세절된 새싹땅콩 0.5 중량부를 첨가 혼합하는 것이 바람직하다. 세절된 새싹땅콩을 0.5 중량부 보다 많이 첨가하는 경우 At this time, it is preferable to add and mix 0.5 parts by weight of chopped peanuts with respect to 100 parts by weight of water. When adding more than 0.5 parts by weight of chopped sprouted peanuts

또한, (d)2차 추출단계는, 새싹땅콩에 함유된 유효성분을 열수에 의해 2차로 추출하기 위한 단계로, 물과 세절된 새싹땅콩과 1차로 추출된 유효성분을 포함하는 1차 혼합물에 열을 가하여 새싹땅콩에 함유된 수용성 유효성분은 2차로 추출하도록 하며, 이로 인해 물에 세절된 새싹땅콩이 침지된 상태에서 새싹땅콩으로부터 물에 새싹땅콩에 함유된 수용성 유효성분이 용출되어 추출되게 되어, 물과 세절된 새싹땅콩과 1차로 추출된 유효성분과 2차로 추출된 유효성분을 포함하는 2차 혼합물이 제조되게 된다.In addition, (d) the second extraction step is a step for secondarily extracting the active ingredient contained in sprouted peanuts by hot water, in a first mixture containing water, chopped sprouted peanuts, and the first extracted active ingredient. Heat is applied to extract the water-soluble active ingredients contained in sprout peanuts for a second time, and as a result, water-soluble active ingredients contained in sprout peanuts are eluted and extracted from sprout peanuts in water while the chopped sprout peanuts are immersed in water. A secondary mixture containing water, chopped sprouted peanuts, the firstly extracted active ingredient, and the secondly extracted active ingredient is prepared.

한편, (d)2차 추출단계는, 일례로, 물과 세절된 새싹땅콩과 1차로 추출된 유효성분을 포함하는 1차 혼합물에 40℃에서 100℃까지 20~40분간 점차 승온시키면서 새싹땅콩에 함유된 수용성 유효성분을 추출하고, 이후 해당 혼합물에 100~110℃의 온도에서 1~4시간 동안 새싹땅콩에 함유된 수용성 유효성분을 추출하면서 농축이 동시에 이루어지도록 구성될 수 있으며, 이는 2차 추출단계에서 처음부터 100℃가량의 높은 온도로 혼합물을 가열하여 추출이 이루어지는 경우, 물에 침지된 새싹땅콩 외표면이 높은 온도로 익게 되어 외표면의 섬유질을 통해 새싹땅콩 내부에 함유된 유효성분이 외부로 용출되지 못하는 것을 방지할 수 있도록 하여, 유효성분의 추출 효율을 보다 향상시킬 수 있게 된다.On the other hand, (d) the second extraction step, for example, while gradually raising the temperature from 40 ℃ to 100 ℃ for 20 to 40 minutes in the first mixture containing water, chopped peanut sprouts, and the first extracted active ingredient, After extracting the contained water-soluble active ingredient, and then extracting the water-soluble active ingredient contained in sprouted peanuts for 1 to 4 hours at a temperature of 100 ~ 110 ℃ in the mixture, it can be configured to be concentrated at the same time, which is secondary extraction In the step, when extraction is performed by heating the mixture at a high temperature of about 100 ° C from the beginning, the outer surface of the peanut sprouts immersed in water is cooked at a high temperature, and the active ingredients contained in the peanut sprouts are released to the outside through the fibers of the outer surface. By preventing dissolution, it is possible to further improve the extraction efficiency of the active ingredient.

다음으로, (e)여과단계는, 물과, 세절된 새싹땅콩과, 1차 및 2차로 추출된 유효성분을 포함하는 2차 혼합물을 여과시켜, 2차 혼합물로부터 유효성분이 추출된 상태로 잔여하는 세절된 새싹땅콩을 제거하여 최종적으로 추출물을 제조하도록 한다.Next, (e) the filtration step is to filter the secondary mixture including the water, the chopped peanut sprouts, and the first and secondly extracted active ingredients to remain in the state in which the active ingredients are extracted from the secondary mixture The chopped peanuts are removed to finally prepare an extract.

<실험예 1> 새싹땅콩 머리부분(싹부분)의 건조조건에 따른 유효성분(레스베라트롤) 함량 및 향 분석<Experimental Example 1> Analysis of active ingredient (resveratrol) content and flavor according to drying conditions of sprouted peanut head (sprout)

본 실험예에서는 하기에 기재된 바와 같이, 새싹땅콩 추출물을 제조하였으며, 제조된 새싹땅콩 추출물에 함유되는 새싹땅콩의 유효성분 중 레스베라트롤 함량을 분석하기 위해서, 고속액체크로마토그래피(HPLC) 분석 기법을 이용하여, 추출물에 함유된 레스베라트롤의 정량분석을 진행하였으며, 분석결과를 아래의 표 1에 나타내었다. In this experimental example, as described below, a sprout peanut extract was prepared, and in order to analyze the resveratrol content among the active ingredients of the sprout peanut contained in the prepared peanut sprout extract, using a high-performance liquid chromatography (HPLC) analysis technique , Quantitative analysis of resveratrol contained in the extract was performed, and the analysis results are shown in Table 1 below.

새싹땅콩을 마련하여, 새싹땅콩을 머리부분, 줄기부분, 뿌리부분으로 분리한 다음, 분리된 부분별로, 증숙시킨 후 건조한 후, 건조된 새싹땅콩 중 머리부분을 세절한 후 물 1000g 당 5g을 첨가하여 40℃에서 5시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하고, 이후 100℃로 가열하여 2시간 동안 추출 및 농축시킨 후 필터에 여과시켜 새싹땅콩 추출물을 제조하였다.Prepare sprouted peanuts, separate sprouted peanuts into head, stem, and root parts, steam and dry each separated part, cut the head of dried sprouted peanuts, and add 5g per 1000g of water Soaked at 40 ° C. for 5 hours to first extract the water-soluble active ingredient contained in sprout peanuts, then heated to 100 ° C. for 2 hours, extracted and concentrated, and then filtered through a filter to prepare peanut sprout extract.

제조예 1 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하였다.Preparation Example 1: The head of sprouted peanuts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 30 minutes.

제조예 2 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하였다.Preparation Example 2: The head of sprouted peanuts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 1 hour.

제조예 3 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 90분간 열풍건조 방식으로 건조하였다.Production Example 3: The head of sprouted peanuts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 90 minutes.

제조예 4 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 4: The head of peanut sprouts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 2 hours.

제조예 5 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 50℃에서 1시간 열풍건조 방식으로 건조하였다.Preparation Example 5: The head of peanut sprouts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 50°C for 1 hour.

제조예 6 : 새싹땅콩의 머리부분은 60℃에서 60분간 증숙시킨 후, 70℃에서 1시간 열풍건조 방식으로 건조하였다.Preparation Example 6: The head of peanut sprouts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 70°C for 1 hour.

구분division 건조온도drying temperature 건조시간drying time 레스베라트롤 함량Resveratrol content incense 제조예 1Preparation Example 1 60℃60℃ 30분30 minutes 53.54㎍/g53.54 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 2Preparation Example 2 60℃60℃ 60분60 minutes 61.52㎍/g 61.52 μg/g 향이 거의 없음almost no scent 제조예 3Preparation Example 3 60℃60℃ 90분90 minutes 61.52㎍/g 61.52 μg/g 향이 거의 없음almost no scent 제조예 4Production Example 4 60℃60℃ 120분120 minutes 61.53㎍/g 61.53 μg/g 향이 거의 없음almost no scent 제조예 5Preparation Example 5 50℃50℃ 60분60 minutes 58.76㎍/g 58.76 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 6Preparation Example 6 70℃70℃ 60분60 minutes 61.53㎍/g 61.53 μg/g 고소한 향 미세 발생Fragrant fragrance finely generated

표 1을 참고하면, 제조예 1 내지 제조예 6을 비교한 결과, 건조온도가 60℃인 경우 건조시간이 60분 이상인 경우 향이 발생되지 않았으나, 건조시간이 60분 이상이 되는 경우 레스베라트롤의 함량 변화 또한 거의 없어, 머리부분은 60℃에서 60분 건조시키는 것이 가장 바람직한 것으로 확인되었다.Referring to Table 1, as a result of comparing Preparation Examples 1 to 6, when the drying temperature is 60 ° C. and the drying time is 60 minutes or more, no fragrance is generated, but when the drying time is 60 minutes or more, the content of resveratrol changes Also, there is almost no, and it was confirmed that drying the hair part at 60 ° C. for 60 minutes is most preferable.

또한, 건조시간이 60분인 경우, 건조온도에 따른 함량과 향의 변화를 살펴보면, 건조온도가 50℃인 경우와 비교하여 건조온도가 60℃인 경우 레스베라트롤 함량이 크고, 추출물에서 향이 거의 발생되지 않았으나, 건조온도가 70℃인 경우 레스베라트롤 함량에는 큰 차이가 없으나, 추출물에서 고소한 향이 미세하게 발생되는 것으로 확인되어, 결과적으로, 건조온도 또한 60℃가 가장 바람직한 것으로 확인되었다.In addition, when the drying time was 60 minutes, looking at the change in content and fragrance according to the drying temperature, the resveratrol content was high when the drying temperature was 60 ℃ compared to the case when the drying temperature was 50 ℃, and the fragrance was hardly generated in the extract. , When the drying temperature was 70 ° C., there was no significant difference in the resveratrol content, but it was confirmed that a fine fragrance was generated from the extract, and as a result, the drying temperature was also confirmed to be 60 ° C.

<실험예 2> 새싹땅콩 줄기부분(배축부분)의 건조조건에 따른 유효성분(레스베라트롤) 함량 및 향 분석<Experimental Example 2> Analysis of active ingredient (resveratrol) content and flavor according to drying conditions of sprout peanut stem part (hypocotyl part)

본 실험예에서는 하기에 기재된 바와 같이, 새싹땅콩 추출물을 제조하였으며, 제조된 새싹땅콩 추출물에 함유되는 새싹땅콩의 유효성분 중 레스베라트롤 함량을 분석하기 위해서, 고속액체크로마토그래피(HPLC) 분석 기법을 이용하여, 추출물에 함유된 레스베라트롤의 정량분석을 진행하였으며, 분석결과를 아래의 표 2에 나타내었다. In this experimental example, as described below, a sprout peanut extract was prepared, and in order to analyze the resveratrol content among the active ingredients of the sprout peanut contained in the prepared peanut sprout extract, using a high-performance liquid chromatography (HPLC) analysis technique , Quantitative analysis of resveratrol contained in the extract was performed, and the analysis results are shown in Table 2 below.

새싹땅콩을 마련하여, 새싹땅콩을 머리부분, 줄기부분, 뿌리부분으로 분리한 다음, 분리된 부분별로, 증숙시킨 후 건조한 후, 건조된 새싹땅콩 줄기부분을 세절한 후 물 1000g 당 5g을 첨가하여 40℃에서 5시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하고, 이후 100℃로 가열하여 2시간 동안 추출 및 농축시킨 후 필터에 여과시켜 새싹땅콩 추출물을 제조하였다.Prepare sprouted peanuts, separate sprouted peanuts into head, stem, and root parts, then steam and dry each separated part, cut the dried sprouted peanut stems, add 5g per 1000g of water, Soaked at 40 ° C. for 5 hours to first extract the water-soluble active ingredient contained in sprout peanuts, then heated to 100 ° C. for 2 hours, extracted and concentrated, and then filtered through a filter to prepare peanut sprout extract.

제조예 7 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하였다.Preparation Example 7: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 30 minutes.

제조예 8 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하였다.Preparation Example 8: The stem portion of peanut sprouts was steamed at 60 ° C for 60 minutes, and then dried by hot air drying at 60 ° C for 1 hour.

제조예 9 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 90분간 열풍건조 방식으로 건조하였다.Preparation Example 9: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 90 minutes.

제조예 10 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 10: The stem portion of peanut sprouts was steamed at 60 ° C for 60 minutes, and then dried by hot air drying at 60 ° C for 2 hours.

제조예 11 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 150분간 열풍건조 방식으로 건조하였다.Preparation Example 11: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried at 60°C for 150 minutes in a hot air drying method.

제조예 12 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 50℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 12: The stem portion of peanut sprouts was steamed at 60 ° C for 60 minutes, and then dried by hot air drying at 50 ° C for 2 hours.

제조예 13 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 70℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 13: The stem portion of peanut sprouts was steamed at 60 ° C for 60 minutes, and then dried at 70 ° C for 2 hours in a hot air drying method.

제조예 14 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 80℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 14: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried at 80°C for 2 hours in a hot air drying method.

구분division 건조온도drying temperature 건조시간drying time 스베라트롤 함량Sveratrol content incense 제조예 7Preparation Example 7 60℃60℃ 30분30 minutes 6.56㎍/g6.56 μg/g 비린향 발생Occurrence of fishy smell 제조예 8Preparation Example 8 60℃60℃ 60분60 minutes 6.81㎍/g6.81 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 9Preparation Example 9 60℃60℃ 90분90 minutes 7.22㎍/g7.22 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 10Preparation Example 10 60℃60℃ 120분120 minutes 7.57㎍/g7.57 μg/g 향이 거의 없음almost no scent 제조예 11Preparation Example 11 60℃60℃ 150분150 minutes 7.57㎍/g7.57 μg/g 향이 거의 없음almost no scent 제조예 12Preparation Example 12 50℃50℃ 120분120 minutes 7.32㎍/g7.32 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 13Preparation Example 13 70℃70℃ 120분120 minutes 8.02㎍/g8.02 μg/g 향이 거의 없음almost no scent 제조예 14Preparation Example 14 80℃80℃ 120분120 minutes 8.02㎍/g8.02 μg/g 고소한 향 미세하게 발생Slightly fragrant scent

표 2를 참고하면, 제조예 7 내지 제조예 14를 비교한 결과, 건조온도가 60℃인 경우 건조시간이 120분 이상인 경우 향이 발생되지 않았으나, 건조시간이 120분 이상이 되는 경우 레스베라트롤의 함량 변화 또한 거의 없어, 줄기부분은 60℃에서 120분 건조시키는 것이 가장 바람직한 것으로 확인되었다.Referring to Table 2, as a result of comparing Preparation Examples 7 to 14, when the drying temperature is 60 ° C. and the drying time is 120 minutes or longer, no fragrance is generated, but when the drying time is 120 minutes or longer, resveratrol content change Also, almost no, it was confirmed that drying the stem part at 60 ℃ for 120 minutes is the most preferable.

한편, 건조시간이 120분인 경우, 건조온도에 따른 함량과 향의 변화를 살펴보면, 건조온도가 70℃인 경우에 추출물에서 향이 거의 발생되지 않음과 동시에 레스베라트롤 함량 또한 높아 가장 바람직한 것으로 확인되었다.On the other hand, when the drying time is 120 minutes, looking at the change in the content and fragrance according to the drying temperature, it was confirmed that the fragrance is hardly generated from the extract when the drying temperature is 70 ° C. and the resveratrol content is also high, which is the most preferable.

<실험예 3> 새싹땅콩 뿌리부분의 건조조건에 따른 유효성분(레스베라트롤) 함량 및 향 분석<Experimental Example 3> Analysis of active ingredient (resveratrol) content and flavor according to drying conditions of sprouted peanut roots

본 실험예에서는 하기에 기재된 바와 같이, 새싹땅콩 추출물을 제조하였으며, 제조된 새싹땅콩 추출물에 함유되는 새싹땅콩의 유효성분 중 레스베라트롤 함량을 분석하기 위해서, 고속액체크로마토그래피(HPLC) 분석 기법을 이용하여, 추출물에 함유된 레스베라트롤의 정량분석을 진행하였으며, 분석결과를 아래의 표 3에 나타내었다. In this experimental example, as described below, a sprout peanut extract was prepared, and in order to analyze the resveratrol content among the active ingredients of the sprout peanut contained in the prepared peanut sprout extract, using a high-performance liquid chromatography (HPLC) analysis technique , Quantitative analysis of resveratrol contained in the extract was performed, and the analysis results are shown in Table 3 below.

새싹땅콩을 마련하여, 새싹땅콩을 머리부분, 줄기부분, 뿌리부분으로 분리한 다음, 분리된 부분별로, 증숙시킨 후 건조한 후, 건조된 새싹땅콩 뿌리부분을 세절한 후 40℃에서 5시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하고, 이후 100℃로 가열하여 2시간 동안 추출 및 농축시킨 후 필터에 여과시켜 새싹땅콩 추출물을 제조하였다.Prepare sprouted peanuts, separate sprouted peanuts into head, stem, and root parts, steam each separated part, dry, cut dried peanut sprout roots, and immerse at 40℃ for 5 hours. The water-soluble active ingredient contained in sprout peanut was first extracted, then heated to 100 ° C. for 2 hours, extracted and concentrated, and then filtered through a filter to prepare peanut sprout extract.

제조예 15 : 새싹땅콩의 뿌리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하였다.Preparation Example 15: The roots of sprouted peanuts were steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 30 minutes.

제조예 16 : 새싹땅콩의 뿌리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하였다.Preparation Example 16: The roots of sprouted peanuts were steamed at 60 ° C for 60 minutes, and then dried by hot air drying at 60 ° C for 1 hour.

제조예 17 : 새싹땅콩의 뿌리부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 90분간 열풍건조 방식으로 건조하였다.Preparation Example 17: The roots of sprouted peanuts were steamed at 60°C for 60 minutes, and then dried by hot air drying at 60°C for 90 minutes.

제조예 18 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 60℃에서 2시간 열풍건조 방식으로 건조하였다.Preparation Example 18: The stem portion of peanut sprouts was steamed at 60 ° C for 60 minutes, and then dried by hot air drying at 60 ° C for 2 hours.

제조예 19 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 50℃에서 30분간 열풍건조 방식으로 건조하였다.Preparation Example 19: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried at 50°C for 30 minutes in a hot air drying method.

제조예 20 : 새싹땅콩의 줄기부분은 60℃에서 60분간 증숙시킨 후, 70℃에서 30분간 열풍건조 방식으로 건조하였다.Preparation Example 20: The stem portion of peanut sprouts was steamed at 60°C for 60 minutes, and then dried at 70°C for 30 minutes in a hot air drying method.

구분division 건조온도drying temperature 건조시간drying time 스베라트롤 함량Sveratrol content incense 제조예 15Preparation Example 15 60℃60℃ 30분30 minutes 81.34㎍/g81.34 μg/g 향이 거의 없음almost no scent 제조예 16Preparation Example 16 60℃60℃ 60분60 minutes 81.35㎍/g81.35 μg/g 향이 거의 없음almost no scent 제조예 17Preparation Example 17 60℃60℃ 90분90 minutes 81.35㎍/g81.35 μg/g 향이 거의 없음almost no scent 제조예 18Preparation Example 18 60℃60℃ 120분120 minutes 81.35㎍/g81.35 μg/g 향이 거의 없음almost no scent 제조예 19Preparation Example 19 50℃50℃ 30분30 minutes 73.57㎍/g73.57 μg/g 비린향 미세하게 발생Occur slightly fishy smell 제조예 20Production Example 20 70℃70℃ 30분30 minutes 81.35㎍/g81.35 μg/g 고소한 향 미세하게 발생Slightly fragrant scent

표 3을 참고하면, 제조예 15 내지 제조예 20를 비교한 결과, 뿌리부분의 경우 건조온도가 60℃인 경우 건조시간이 30분 이상인 경우 향이 거의 없으며, 레스베라트롤 함량 또한 크게 차이 나지 않는 것으로 확인되었다.Referring to Table 3, as a result of comparing Preparation Examples 15 to 20, in the case of the root part, when the drying temperature is 60 ° C. and the drying time is 30 minutes or more, there is almost no fragrance, and the resveratrol content is also not significantly different. .

또한, 건조시간을 30분으로 하여, 온도 변화에 따른 차이를 비교분석한 결과, 레스베라트롤 함량은 크게 차이가 없으나, 60℃인 경우 향이 거의 발생되지 않는 것으로 확인되어 가장 바람직한 것으로 확인되었다.In addition, as a result of comparative analysis of differences according to temperature changes with a drying time of 30 minutes, there was no significant difference in resveratrol content, but it was confirmed that fragrance was hardly generated at 60 ° C., which was confirmed to be the most preferable.

한편, 본 발명의 실시예에 따른 새싹땅콩 추출물을 포함하는 화장료 조성물은, 상기와 같이 구성되는 새싹땅콩 추출물 제조방법에 의해 제조되는 새싹땅콩 추출물을 이용하는 것이 특징이다.On the other hand, the cosmetic composition containing the peanut sprout extract according to an embodiment of the present invention is characterized by using the peanut sprout extract prepared by the method for preparing the peanut sprout extract configured as described above.

이때, 화장료 조성물은, 크림, 에센스, 용액, 폼, 겔, 화장수, 유연수, 유액, 로션, 현탁액, 유탁액, 오일로 구성되는 군으로부터 선택되는 제형을 갖도록 구성될 수 있다.At this time, the cosmetic composition may be configured to have a formulation selected from the group consisting of cream, essence, solution, foam, gel, lotion, softening water, emulsion, lotion, suspension, emulsion, and oil.

한편, 화장료 조성물은 총량인 100중량부에 대하여 새싹땅콩 추출물이 을 0.5~50중량부를 함유하도록 구성되며, 이때 0.5중량부보다 적게 함유되는 경우 새싹땅콩 추출물을 함유함에 따른 기능성 향상 효과가 미미하여 바람직하지 않고, 50중량부 보다 많이 함유하는 경우 새싹땅콩 추출물을 추가로 함유함에 따른 기능성 추가로 향상되는 효과가 미미하여 경제적이지 않아 바람직하지 않다.On the other hand, the cosmetic composition is configured to contain 0.5 to 50 parts by weight of sprout peanut extract with respect to 100 parts by weight, which is the total amount. At this time, when it is contained less than 0.5 parts by weight, the functional improvement effect due to the inclusion of peanut sprout extract is insignificant, which is not preferable. And, when it contains more than 50 parts by weight, the effect of improving the functional addition by additionally containing the peanut sprout extract is insignificant, which is not preferable because it is not economical.

한편, 화장료 조성물이 세럼으로 구성되는 경우, 세럼은 유상성분과 수상성분과 첨가물을 포함하고, 이때 유상성분은 땅콩오일, 올리브오일, 라놀린, 올리브유화왁스, 솔루빌라이저를 포함하고, 수상성분은 본 발명에 의해 제조되는 새싹땅콩 추출물을 포함하고, 첨가물은 글리세린, 1.3부틸렌글리콜(1.3BG), 1.2헥산디올, 베타글루칸, 세라마이드, D-판테놀, 히알루론산, 나이아신아마이드, 아데노신, 알부틴을 포함할 수 있다.On the other hand, when the cosmetic composition is composed of a serum, the serum includes an oily component, an aqueous component and an additive, wherein the oily component includes peanut oil, olive oil, lanolin, olive emulsified wax, and a solubilizer, and the aqueous component is Contains sprout peanut extract prepared by the present invention, additives include glycerin, 1.3 butylene glycol (1.3BG), 1.2 hexanediol, beta-glucan, ceramide, D-panthenol, hyaluronic acid, niacinamide, adenosine, arbutin can do.

보다 상세하게는, 일례로, 화장료 조성물 총 100중량부를 기준으로, 유상성분으로 땅콩오일 15 중량부, 올리브오일 5 중량부, 라놀린 2 중량부, 올리브유화왁스 6 중량부, 솔루빌라이저 1.5 중량부를 포함하고, 수상성분은 본 발명에 의해 제조되는 새싹땅콩 추출물 50 중량부를 포함하고, 첨가물은 글리세린 5 중량부, 1.3부틸렌글리콜(1.3BG) 3 중량부, 1.2헥산디올 2 중량부, 베타글루칸 1 중량부, 세라마이드 2 중량부, D-판테놀 1 중량부, 히알루론산 1 중량부, 나이아신아마이드 3 중량부, 아데노신 2 중량부, 알부틴 2 중량부를 포함하도록 구성되는 것이 바람직하다.More specifically, for example, based on the total 100 parts by weight of the cosmetic composition, 15 parts by weight of peanut oil, 5 parts by weight of olive oil, 2 parts by weight of lanolin, 6 parts by weight of olive oil wax, and 1.5 parts by weight of solubilizer as oily components. The aqueous phase component includes 50 parts by weight of sprout peanut extract prepared according to the present invention, and the additives include 5 parts by weight of glycerin, 3 parts by weight of 1.3 butylene glycol (1.3BG), 2 parts by weight of 1.2 hexanediol, and 1 beta glucan. It is preferably configured to include 2 parts by weight of ceramide, 1 part by weight of D-panthenol, 1 part by weight of hyaluronic acid, 3 parts by weight of niacinamide, 2 parts by weight of adenosine, and 2 parts by weight of arbutin.

<실험예 4 - 화장료 조성물(세럼)의 관능 평가><Experimental Example 4 - Sensory evaluation of cosmetic composition (serum)>

본 실험예에서는 하기에 기재된 바와 같이, 하기 실험예에서 제조예 21에 의해 제조된 새싹땅콩 추출물을 포함하는 화장료 조성물(세럼)을 제조하였다.In this Experimental Example, a cosmetic composition (serum) containing the peanut sprout extract prepared by Preparation Example 21 was prepared in the following Experimental Example, as described below.

제조예 21 : 새싹땅콩을 마련하여, 새싹땅콩을 머리부분, 줄기부분, 뿌리부분으로 분리한 다음, 분리된 부분별로, 증숙시킨 후 건조한 후, 건조된 새싹땅콩 각 부분을 세절한 후 물 1000g 당 5g을 첨가하여 40℃에서 5시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하고, 이후 100℃로 가열하여 2시간 동안 추출 및 농축시킨 후 필터에 여과시켜 새싹땅콩 추출물을 제조하였으며, 이때, 머리부분은 60℃에서 1시간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하여 준비하고, 줄기부분은 60℃에서 1시간 증숙시킨 후, 70℃에서 2시간 열풍건조 방식으로 건조하여 준비하였다. 뿌리부분은 60℃에서 1시간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하여 준비하였다.Preparation Example 21: Prepare peanut sprouts, separate the peanut sprouts into head, stem, and root parts, and then steam and dry each separated part, cut each part of the dried peanut sprouts, and cut each part into 1000 g of water. 5 g was added and immersed at 40 ° C for 5 hours to first extract the water-soluble active ingredient contained in sprout peanuts, then heated to 100 ° C. for 2 hours, extracted and concentrated, and then filtered through a filter to prepare peanut extract. , At this time, the head is prepared by steaming at 60 ° C for 1 hour and then drying with hot air drying at 60 ° C for 1 hour. It was prepared by drying. The root portion was prepared by steaming at 60 ° C. for 1 hour and then drying by hot air drying at 60 ° C. for 30 minutes.

제조예 22 : 새싹땅콩을 마련하여, 새싹땅콩을 분리하지 않고, 60℃에서 1시간 증숙시킨 후, 60℃에서 1시간 열풍건조시킨 후, 건조된 새싹땅콩 각 부분을 세절한 후 물 1000g 당 5g을 첨가하여 40℃에서 5시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분을 1차로 추출하고, 이후 100℃로 가열하여 2시간 동안 추출 및 농축시킨 후 필터에 여과시켜 새싹땅콩 추출물을 제조하였다.Preparation Example 22: Prepare sprouted peanuts, steamed at 60 ° C for 1 hour without separating sprouted peanuts, dried with hot air at 60 ° C for 1 hour, cut each part of the dried sprouted peanuts, and then 5g per 1000g of water was added and immersed at 40 ° C. for 5 hours to first extract the water-soluble active ingredient contained in sprout peanuts, then heated to 100 ° C. for 2 hours, extracted and concentrated, and then filtered through a filter to prepare peanut sprout extract.

이때, 화장료 조성물(세럼)은 유상성분으로 땅콩오일 15 중량부, 올리브오일 5 중량부, 라놀린 2 중량부, 올리브유화왁스 6 중량부, 솔루빌라이저 1.5 중량부를 포함하고, 수상성분은 본 발명에 의해 제조되는 새싹땅콩 추출물 50 중량부를 포함하고, 첨가물은 글리세린 5 중량부, 1.3부틸렌글리콜(1.3BG) 3 중량부, 1.2헥산디올 2 중량부, 베타글루칸 1 중량부, 세라마이드 2 중량부, D-판테놀 1 중량부, 히알루론산 1 중량부, 나이아신아마이드 3 중량부, 아데노신 2 중량부, 알부틴 2 중량부를 포함하여 제조하였다.At this time, the cosmetic composition (serum) includes 15 parts by weight of peanut oil, 5 parts by weight of olive oil, 2 parts by weight of lanolin, 6 parts by weight of olive emulsified wax, and 1.5 parts by weight of a solubilizer as oil components, and the aqueous phase component is in the present invention. 50 parts by weight of sprout peanut extract prepared by, and additives include 5 parts by weight of glycerin, 3 parts by weight of 1.3 butylene glycol (1.3BG), 2 parts by weight of 1.2 hexanediol, 1 part by weight of beta glucan, 2 parts by weight of ceramide, D - It was prepared by including 1 part by weight of panthenol, 1 part by weight of hyaluronic acid, 3 parts by weight of niacinamide, 2 parts by weight of adenosine, and 2 parts by weight of arbutin.

상기와 같이 제조한 화장료 조성물(세럼)의 항산화성(리프팅 정도), 향(비린 향 발생 정도), 전반적인 선호도를 알아보고자, 본 실험에서는 20명의 여성을 각각 10명씩 2조로 나눠서 2주일간 매일 아침과 저녁에 각각 세안 후 안면에 도포하고, 처음 사용시 향(비린 향이나 고소한 향 등 향 발생 정도)과, 2주일간 항산화성(리프팅 정도) 개선정도와, 전반적인 선호도에 대한 점수를 0점에서 10점까지 점수를 부여하도록 하되, 향(향 발생 정도)는 비린 향이나 고소한 향 등 향의 발생 정도가 적을수록 높은 점수를, 항산화성(리프팅 정도)는 리프팅 효과가 높을수록 높은 점수를, 전반적인 선호도의 경우 선호도가 높을수록 높은 점수를 부여하도록 하였으며, 각 조의 실험자 평가점수를 평균하여 나타내었으며, 평가 결과는 하기 표 4와 같다.In order to investigate the antioxidant properties (degree of lifting), fragrance (degree of occurrence of fishy scent), and overall preference of the cosmetic composition (serum) prepared as described above, in this experiment, 20 women were divided into 2 groups of 10 each, and each morning and morning for 2 weeks. In the evening, apply it to the face after washing your face, and score the fragrance at the time of first use (degree of occurrence of scent such as fishy or savory scent), the degree of improvement in antioxidant properties (degree of lifting) for 2 weeks, and the overall preference score from 0 to 10 points. Scores are given, but for fragrance (degree of occurrence), the higher the score, the lower the degree of occurrence of scent, such as fishy or savory scent, and the higher the score for antioxidant (lifting degree), the higher the lifting effect. The higher the preference, the higher the score, and the average of the tester evaluation scores of each group was shown, and the evaluation results are shown in Table 4 below.

구분division 처음 사용시 향Fragrance on first use 항산화성antioxidant properties 전반적 선호도overall preference 제조예 21Production Example 21 99 88 88 제조예 22Production Example 22 99 66 77

표 4를 참조하면, 새싹땅콩을 부분별로 분리하여 건조조건을 달리한 제조예 21의 경우, 새싹땅콩을 분리없이 동시에 건조 가공한 것과 비교한 결과, 각 부분별로 가장 바람직한 건조조건에 따라 건조한 후 추출물을 제조한 결과 리프팅 효과가 보다 향상되는 것을 확인할 수 있다.Referring to Table 4, in the case of Preparation Example 21 in which the peanut sprouts were separated by parts and the drying conditions were different, as a result of comparing the dry processing of the peanut sprouts at the same time without separation, the extract after drying according to the most desirable drying conditions for each part As a result of manufacturing, it can be confirmed that the lifting effect is further improved.

이와 같이, 상술한 본 발명의 기술적 구성은 본 발명이 속하는 기술분야의 당업자가 본 발명의 그 기술적 사상이나 필수적 특징을 변경하지 않고서 다른 구체적인 형태로 실시될 수 있다는 것을 이해할 수 있을 것이다.As such, it will be understood that the technical configuration of the present invention described above can be implemented in other specific forms without changing the technical spirit or essential features of the present invention by those skilled in the art to which the present invention pertains.

그러므로 이상에서 기술한 실시예들은 모든 면에서 예시적인 것이며 한정적인 것이 아닌 것으로서 이해되어야 하고, 본 발명의 범위는 상기 상세한 설명보다는 후술하는 특허청구범위에 의하여 나타나며, 특허청구범위 의미 및 범위 그리고 그 등가 개념으로부터 도출되는 모든 변경 또는 변형된 형태가 본 발명의 범위에 포함되는 것으로 해석되어야 한다.Therefore, the embodiments described above should be understood as illustrative and not restrictive in all respects, and the scope of the present invention is indicated by the claims to be described later rather than the detailed description, and the meaning and scope of the claims and their equivalents All changes or modified forms derived from the concept should be construed as being included in the scope of the present invention.

Claims (10)

새싹땅콩을 마련하여 증숙시킨 후 건조하여 준비하는 (a)사전가공단계;
건조된 새싹땅콩을 세절하여 마련하는 (b)세절단계;
물에 세절된 새싹땅콩을 첨가 혼합하여 40~50℃에서 5~6시간 동안 침지시켜 새싹땅콩에 함유된 수용성 유효성분인 레스베라트롤 추출물을 1차로 추출하는 (c)1차 추출단계;
상기 물과 상기 세절된 새싹땅콩과 1차로 추출된 상기 레스베라트롤 추출물을 포함하는 제1 혼합물을 40~100℃의 온도범위 내에서 20~40분간 점차 승온시키면서 새싹땅콩에 함유된 수용성 유효성분인 레스베라트롤 추출물을 2차로 추출하여 제2 혼합물을 제조하며,
이후 상기 제2 혼합물을 100~110℃의 온도에서 1~4시간 동안 새싹땅콩에 함유된 수용성 유효성분인 레스베라트롤 추출물을 3차로 추출하여 농축시켜 제3 혼합물을 제조하는 (d)2차 추출단계; 및
상기 제3 혼합물을 여과시켜, 상기 레스베라트롤 추출물이 추출되고 잔여하는 상기 세절된 새싹땅콩을 분리 제거하여 새싹땅콩 추출물을 제조하는 (e)여과단계;를 포함하는, 새싹땅콩 추출물 제조방법.
(a) a pre-processing step of preparing sprouted peanuts, steaming them, and drying them;
(b) the cutting step of preparing by cutting the dried sprout peanuts;
(c) a first extraction step of firstly extracting resveratrol extract, a water-soluble active ingredient contained in peanut sprouts, by adding and mixing chopped sprout peanuts in water and immersing at 40 to 50 ° C for 5 to 6 hours;
Resveratrol extract, which is a water-soluble active ingredient contained in sprout peanuts, while gradually raising the temperature of the first mixture containing the water, the chopped sprout peanuts, and the firstly extracted resveratrol extract within a temperature range of 40 to 100 ° C for 20 to 40 minutes Secondarily extracted to prepare a second mixture,
(d) a second extraction step of preparing a third mixture by tertiarily extracting and concentrating the resveratrol extract, which is a water-soluble active ingredient contained in sprouted peanuts, from the second mixture at a temperature of 100 to 110 ° C. for 1 to 4 hours; and
(e) filtering the third mixture to prepare a peanut sprout extract by filtering the resveratrol extract and separating and removing the remaining chopped peanut sprout extract; Containing, sprout peanut extract manufacturing method.
제1항에 있어서,
상기 (a)사전가공단계는
마련된 새싹땅콩을 세척하는 세척단계와,
세척된 새싹땅콩을 머리부분(싹부분), 줄기부분(배축부분) 및 뿌리부분으로 분리하는 분리단계와,
분리된 새싹땅콩의 상기 머리부분(싹부분), 상기 줄기부분(배축부분) 및 상기 뿌리부분을 각각 별도로 증숙시키고, 건조하는 건조단계를 포함하는 것을 특징으로 하는, 새싹땅콩 추출물 제조방법.
According to claim 1,
The (a) pre-processing step
A washing step of washing the prepared peanuts;
A separation step of separating the washed sprout peanuts into a head part (sprout part), a stem part (hypocotyl part) and a root part;
A method for producing peanut sprout extract, characterized in that it comprises a drying step of separately steaming and drying the head part (sprout part), the stem part (hypocotyl part) and the root part of the separated sprout peanut.
제2항에 있어서,
상기 건조단계는
상기 머리부분(싹부분)을 60℃에서 1시간 증숙시킨 후, 60℃에서 1시간 열풍건조 방식으로 건조하는 것을 특징으로 하는, 새싹땅콩 추출물 제조방법.
According to claim 2,
The drying step is
Characterized in that, after steaming the head (sprout portion) at 60 ° C. for 1 hour, drying by hot air drying method at 60 ° C. for 1 hour, sprout peanut extract manufacturing method.
제2항에 있어서,
상기 건조단계는
상기 줄기부분(배축부분)을 60℃에서 1시간 증숙시킨 후, 70℃에서 2시간 열풍건조 방식으로 건조하는 것을 특징으로 하는, 새싹땅콩 추출물 제조방법.
According to claim 2,
The drying step is
The stem portion (hypocotyl portion) is steamed at 60 ° C. for 1 hour and then dried by hot air drying at 70 ° C. for 2 hours.
제2항에 있어서,
상기 건조단계는
상기 뿌리부분을 60℃에서 1시간 증숙시킨 후, 60℃에서 30분간 열풍건조 방식으로 건조하는 것을 특징으로 하는, 새싹땅콩 추출물 제조방법.
According to claim 2,
The drying step is
After steaming the root portion at 60 ° C. for 1 hour, drying by hot air drying method at 60 ° C. for 30 minutes, sprout peanut extract manufacturing method.
제1항에 있어서,
상기 (c)1차 추출단계는
상기 물 100 중량부에 대하여 상기 세절된 새싹땅콩 0.5 중량부를 첨가 혼합하는 것을 특징으로 하는, 새싹땅콩 추출물 제조방법.
According to claim 1,
The (c) first extraction step
Characterized in that adding and mixing 0.5 parts by weight of the chopped sprout peanuts with respect to 100 parts by weight of the water, sprout peanut extract manufacturing method.
삭제delete 제1항 내지 제6항 중 어느 한 항에 기재된 제조방법에 의해 제조된 새싹땅콩 추출물을 포함하며, 화장료 조성물 100중량부에 대하여 상기 새싹땅콩 추출물을 0.5~50중량부를 함유하는 것을 특징으로 하는 새싹땅콩 추출물을 포함하는 화장료 조성물.
It contains the peanut sprout extract prepared by the manufacturing method according to any one of claims 1 to 6, and the sprout is characterized in that it contains 0.5 to 50 parts by weight of the peanut extract with respect to 100 parts by weight of the cosmetic composition. A cosmetic composition comprising a peanut extract.
제8항에 있어서,
상기 화장료 조성물은
크림, 에센스, 용액, 폼, 겔, 화장수, 유연수, 유액, 로션, 현탁액, 유탁액, 오일로 구성되는 군으로부터 선택되는 제형을 갖는 것을 특징으로 하는 새싹땅콩 추출물을 포함하는 화장료 조성물.
According to claim 8,
The cosmetic composition
A cosmetic composition containing sprout peanut extract, characterized in that it has a formulation selected from the group consisting of cream, essence, solution, foam, gel, lotion, softening water, emulsion, lotion, suspension, emulsion, oil.
제8항에 있어서,
상기 화장료 조성물은
세럼 제형으로 이루어지되,
상기 세럼 제형의 화장료 조성물은 유상성분으로 땅콩오일 15 중량부, 올리브오일 5 중량부, 라놀린 2 중량부, 올리브유화왁스 6 중량부, 솔루빌라이저 1.5 중량부를 포함하고, 수상성분은 본 발명에 의해 제조되는 새싹땅콩 추출물 50 중량부를 포함하고, 첨가물은 글리세린 5 중량부, 1.3부틸렌글리콜(1.3BG) 3 중량부, 1.2헥산디올 2 중량부, 베타글루칸 1 중량부, 세라마이드 2 중량부, D-판테놀 1 중량부, 히알루론산 1 중량부, 나이아신아마이드 3 중량부, 아데노신 2 중량부, 알부틴 2 중량부를 포함하는 것을 특징으로 하는 새싹땅콩 추출물을 포함하는 화장료 조성물.
According to claim 8,
The cosmetic composition
It consists of a serum formulation,
The cosmetic composition of the serum formulation includes 15 parts by weight of peanut oil, 5 parts by weight of olive oil, 2 parts by weight of lanolin, 6 parts by weight of olive emulsified wax, and 1.5 parts by weight of a solubilizer as oil components, and the aqueous phase component is according to the present invention. It contains 50 parts by weight of sprout peanut extract, and additives include 5 parts by weight of glycerin, 3 parts by weight of 1.3 butylene glycol (1.3BG), 2 parts by weight of 1.2 hexanediol, 1 part by weight of beta glucan, 2 parts by weight of ceramide, D- A cosmetic composition comprising a peanut sprout extract comprising 1 part by weight of panthenol, 1 part by weight of hyaluronic acid, 3 parts by weight of niacinamide, 2 parts by weight of adenosine, and 2 parts by weight of arbutin.
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