KR102345862B1 - Solid oral cleaning composition comprising popping component - Google Patents

Abstract

The present invention relates to a solid oral cleaning composition, and more specifically, to a solid oral cleaning composition containing a gas-filled popping ingredient, abrasive and lactic acid bacteria culture therein. In addition, according to the present invention, the solid oral cleaning composition contains a gas-filled popping ingredient, abrasive and lactic acid bacteria culture which has a popping effect and also a caries prevention effect by inhibiting the growth of Streptococcus mutans, which causes tooth decay, as the popping ingredient in the form of a capsule melts in the oral cavity, and thus satisfies the tastes of young and old, especially young children, who are prone to rejection of brushing teeth, and can contribute to the national oral health and insurance finance for tooth decay prevention.

Description

Solid oral cleaning composition comprising popping component

The present invention relates to a solid mouthwash composition, and more particularly, by including a gas-filled popping component, an abrasive and a lactic acid bacteria culture in the solid mouthwash composition, the popping component in the form of a capsule is melted in the oral cavity while popping ( Popping) and at the same time, it has a caries prevention effect that inhibits the growth of Streptococcus mutans, which causes tooth decay, so it satisfies the preferences of all ages, especially young children, who are prone to rejection when brushing their teeth. It relates to a composition for oral hygiene that can contribute to insurance finance according to health and prevention of tooth decay.

Tooth decay is a representative oral disease, and bacteria, especially Streptococcus mutans, present in the oral cavity decompose carbohydrates such as sugar or starch attached to teeth during metabolism to produce various organic acids, and these acids cause the mineral components of teeth to be demineralized. is known to be Fluorine compounds, aminocaproic acid, chlorhexidine, dextranase, etc. are currently being used to prevent various oral diseases including tooth decay. Oral products are being studied.

Toothpaste is a drug compound used to clean teeth and the inside of the oral cavity. It has various uses, such as whitening teeth, preventing tartar deposition, and removing bad breath, and is used as a daily necessities. It is common to put this in a tube container with a lid and use the toothpaste pushed out through the tube inlet by applying pressure to the tube each time it is used.

In order to solve this problem, a tablet-type toothpaste in pill form has been developed (Patent Application No. 10-2011-0083295), but a mouthwash composition that can still satisfy the preferences of young children who are prone to rejection when brushing their teeth development is required.

Therefore, the inventor of the present invention develops a composition for oral cleaning in a solid form by utilizing a component having a popping effect, satisfying the taste of not only the general public, but especially young children who are prone to rejection reaction to brushing, harmless to the human body, and A solid oral cleaning composition that is easy to carry was completed.

Korean Patent Laid-Open Patent No. 10-2019-0141372 (published date: 2019.12.24)

The present invention was devised to solve the above problems, and an object of the present invention is to provide a solid mouthwash composition comprising a popping component filled with gas, an abrasive, and a lactic acid bacteria culture in the solid mouthwash composition.

In order to achieve the above object, the present invention provides a solid mouthwash composition comprising a gas-filled popping component and an abrasive.

According to an embodiment of the present invention, the popping component may include a sugar component.

The sugar component may include xylitol.

According to an embodiment of the present invention, the gas may be at least one kind of gas selected from the group consisting of carbon dioxide, oxygen, nitrogen, helium and aromatic gas.

According to an embodiment of the present invention, the abrasive may include silicon dioxide.

According to an embodiment of the present invention, the popping component may be in the form of a capsule.

The capsule may be prepared by coating the popping ingredient with coconut oil and powdered lactose-oil mixture.

According to one embodiment of the present invention, the solid mouthwash composition may further include lactic acid bacteria or a culture of lactic acid bacteria that inhibit the growth of Streptococcus mutans causing tooth decay.

According to the present invention, the solid mouthwash composition contains a gas-filled popping component, an abrasive, and a lactic acid bacteria culture, so that the popping component in the form of a capsule is melted in the oral cavity while having a popping effect and at the same time causing tooth decay. It is possible to provide a caries preventive effect that inhibits the growth of Streptococcus mutans.

Hereinafter, a preferred embodiment of the present invention will be described in detail with respect to the solid oral care composition according to the present invention.

The solid mouthwash composition according to the present invention includes a gas-filled popping component and an abrasive.

In the present invention, the term 'popping component' refers to a gas-containing component, stirring the melt of the sugar component under conditions of high temperature and high pressure, and spraying ultra-high pressure carbon dioxide to melt and/or contain a large amount of carbon dioxide gas in the melt, As a component obtained by cooling and solidifying under ultra-high pressure conditions, when the popping component melts in the oral cavity, the high-pressure carbon dioxide gas contained in the melt rapidly expands and spontaneously mixes with the liquid in the process of being released into the oral cavity, popping (popping) ) means a component that has an effect.

In the present invention, the sugar component functions as a carrier to fill and capture gas, and the sugar component includes xylitol, sorbitol, maltitol, erythritol, reduced palatinose, and mannitol. (mannitol) and may be selected from the group consisting of lactitol xylitol, and preferably may be xylitol, but is not limited thereto.

The xylitol is an alcoholic sugar made by processing xylose, and is a substance used as a sugar substitute or dental care product. It has the same sweetness as sucrose of the same mass, but contains about 60% of the calories of sucrose. Unlike hexoses such as sucrose, glucose, and fructose, xylitol is a pentose sugar, and Streptococcus mutans cannot ferment sugar, making acid production impossible, so it helps protect teeth or restore damaged tooth surfaces. give Xylitol can help prevent tooth decay, protect teeth, and restore damaged teeth.

In the present invention, 'gas' is a relatively harmless or inert gas to the human body, such as carbon dioxide, oxygen, nitrogen, helium, etc., or a relatively harmless aromatic gas, or Any mixture of these means.

In the present invention, 'filled' specifically means a state in which the gas is at least partially or under pressure filled in the sugar component.

The abrasive is made of silicon dioxide, precipitated silica, silica gel, silicic anhydride, zirconium silicate, calcium hydrogen phosphate, anhydrous calcium hydrogen phosphate, hydrous alumina, light calcium carbonate, heavy calcium carbonate, calcium pyrophosphate, insoluble metaphosphate, and aluminum silicate. It may be selected from the group, preferably silicon dioxide.

Silicon dioxide does not have a salty taste and has a neutral pH, so it does not irritate the mucous membranes in the oral cavity, so it has the advantage that anyone, regardless of age or sex, can use it safely.

The capsule-type popping component can be prepared in capsule form by coating it with coconut oil and powdered lactose-oil mixture. The first coating may be performed, and the final capsule-type popping ingredient may be prepared by spraying the powdery lactose-oil mixture and coating it evenly, but the present invention is not necessarily limited thereto.

The solid mouthwash composition according to the present invention may further include lactic acid bacteria or a culture of lactic acid bacteria that inhibit the growth of Streptococcus mutans that causes tooth decay.

In the present invention, the 'lactic acid bacteria culture' may be a culture medium of lactic acid bacteria, a cell-free supernatant thereof, or a lactic acid bacteria culture dried product, but is not limited thereto.

The lactic acid bacteria culture contains bacteriocin, which is a natural antibacterial material produced by microorganisms, and the bacteriocin has been proven to effectively inhibit the growth of Streptococcus mutans that causes tooth decay (Korea Patent No. 10). -0158048).

The lactic acid bacteria are Streptococcus mutans , known as functional lactic acid bacteria that inhibit the growth, Lactobacillus reuteri (Korean Patent No. 10-1966772), Lactobacillus gasseri (Korea) Registered Patent No. 10-2198553), Lactobacillus fermentum (Korea Patent No. 10-2198552), Lactobacillus helveticus (Lactobacillus helveticus) (Korean Patent Publication No. 10-2016-0030956) and It may be one or more selected from the group consisting of Lactobacillus salivarius (Korean Patent Publication No. 10-2020-0070081), but is not limited thereto.

The solid mouthwash composition according to the present invention may further include a surfactant, a flavoring agent, a sweetener, sodium fluoride, and propolis as other additives.

The surfactant may be one or two or more selected from anionic surfactants, cationic surfactants, nonionic surfactants, amphoteric surfactants, and zwitterionic surfactants.

The flavoring agent may be selected from one or two or more types of mint-based flavors such as peppermint and spearmint and flavorings such as menthol, eucalyptus, anise, thymol, lemon, lime, coffee, green tea, rosemary, and jasmine. doesn't happen

The sweetener may be at least one selected from the group consisting of sucralose, erythritol, aspartame, and combinations thereof, but is not limited thereto.

The propolis (Propolis) is a natural antibacterial material that the Food and Drug Administration has announced as a functional antioxidant action and antibacterial action in the oral cavity. Streptococcus mutans ( Streptococcus mutans ) Since it can have a synergistic effect on growth inhibition, it is possible to provide an excellent composition for oral hygiene.

Example

Hereinafter, the present invention will be described in more detail through examples. These examples are only for illustrating the present invention, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not to be construed as being limited by these examples.

Preparation Example 1:

The solid oral cleaning composition is prepared by mixing 10% by weight of a gas-filled popping component, 50% by weight of silicon dioxide, 1% by weight of lactic acid bacteria culture dried product, and 39% by weight of other additives with respect to the entire composition, and various drying methods such as freeze drying or hot air drying Drying in a manner to prepare a composition for mouthwash in a solid form.

The popping component was specifically prepared through the following process.

First, the raw material mixture (sugar component and aqueous solvent) is put into an autoclave, and after cooking at a steam pressure of 5 kg/cm 2 and a temperature of 118 to 120° C. for 18 to 20 minutes, a steam pressure of 10 kg/cm 2 and a temperature of 142 to By vacuum-cooking at 144° C. for 18 to 20 minutes, the moisture content was adjusted to 3% by weight or less to prepare a melt of the sugar component.

Next, fragrances and dyes were added to the melt of sugar components obtained through the above process, and then for 4 minutes under the conditions of jacket steam pressure of 2 kg/cm 2 , carbon dioxide gas pressure of 48 kg/cm 2 , and stirring water 800 rpm. While stirring, carbon dioxide gas was mixed.

Next, the melt of the sugar component mixed with carbon dioxide gas obtained through the above process is transferred to a cooling pipe under a carbon dioxide gas pressure of 48 kg/cm 2 , and then the temperature of the cooling water is 20±3° C., and the circulation rate of the cooling water is 10G.P0. M. And the carbon dioxide gas pressure was 48 kg/cm 2 to cool and solidify to produce a popping component filled with carbon dioxide gas, and then suddenly release the carbon dioxide gas to fragment the cooled and solidified popping component.

Next, by recovering the fragmented popping component and selecting the size (4 mesh or more, 20 mesh or less are discarded), a popping component suitable for use in this preparation example was completed.

The lactobacillus culture dried product was obtained by centrifugation (4,000 × g, 4 ℃, 5 minutes) of a culture solution obtained by culturing Lactobacillus reuteri in MRS liquid medium for 24 hours, and then using a 0.22 μm filter to obtain a sterilized supernatant. was lyophilized to complete.

As the other additives, 0.5 to 2% by weight of sodium lauryl sulfate, 0.1 to 5% by weight of a menthol flavoring agent, 0.01 to 0.5% by weight of aspartame, and 0.01 to 0.3% by weight of sodium fluoride were included.

Preparation Example 2:

The popping ingredient prepared by the method described above in [Preparation Example 1] was first coated with coconut oil in a rotating pan at 18 rpm under a humidity of 20 ° C and 45%, and then powdered lactose at 20 to 26 ° C. A capsule-type popping component was prepared by spraying the oil mixture and evenly coating it, and the other manufacturing methods were the same as in [Preparation Example 1].

Preparation Example 3:

The solid oral cleaning compositions prepared in Preparation Examples 1 and 2 were molded into powder, granular, or regular shape for ease of use, or put into a regular mold to prepare a molded product.

Experimental example

The solid oral cleaning composition prepared in Preparation Example 1 and Preparation Example 2 was put into water and the time the carbon dioxide was released was measured (time to visually confirm that bubbles were generated in the popping component), as a result The composition (Preparation Example 2) coated in the form of a capsule continued the release of carbon dioxide significantly longer than the uncoated composition (Preparation Example 1). This indicates that the solid mouthwash composition coated in the capsule form of the present invention can sustain the popping effect in the oral cavity while brushing teeth.

As described above in detail a specific part of the present invention, for those of ordinary skill in the art, this specific description is only a preferred embodiment, and it is clear that the scope of the present invention is not limited thereto. Accordingly, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

Claims (8)

Contains a popping ingredient filled with aromatic gas and an abrasive,
The popping ingredient is a solid mouthwash composition, characterized in that it is in the form of a capsule prepared by coating with coconut oil and powdered lactose-oil mixture. The method of claim 1,
The popping component is a solid mouthwash composition comprising a sugar component. 3. The method of claim 2,
The sugar component is a solid mouthwash composition comprising xylitol. delete The method of claim 1,
The abrasive is a solid mouthwash composition comprising silicon dioxide. delete delete The method of claim 1,
A solid mouthwash composition comprising lactic acid bacteria or a culture of lactic acid bacteria that inhibits the growth of Streptococcus mutans causing tooth decay.