KR102293975B1 - Eco shampoo composition comprising hydrogen peroxide and extracts of Ulmus davidiana var. japonica and the preparation method of the same - Google Patents

Abstract

The present invention adds extracts and EM useful microorganisms extracted from hydrogen peroxide, elm extract and natural material malt extract, black bean extract, coriander fruit extract, sewage extract, bay leaf extract, tarragon leaf extract, and calamus extract, and is an eco-friendly surfactant It relates to an eco-friendly shampoo that is made by dissolving C08-14 alkyl polyglucoside in a mixed solution.

Description

Eco shampoo composition comprising hydrogen peroxide and extracts of elm tree and manufacturing method thereof japonica and the preparation method of the same}

The present invention adds extracts and EM useful microorganisms extracted from hydrogen peroxide, elm extract and natural material malt extract, black bean extract, coriander fruit extract, sewage extract, bay leaf extract, tarragon leaf extract, and calamus extract, and is an eco-friendly surfactant It relates to an eco-friendly shampoo that is made by dissolving C08-14 alkyl polyglucoside in a mixed solution. , It also makes the hair shiny, suppresses the bacteria that cause hair loss, and is effective for hair growth.

Most commonly used shampoos are shampoos that use synthetic chemical ingredients such as synthetic chemical surfactants, silicone, preservatives, and parabens. In the West, such as the United States and Europe, chemical treatment agents based on Western medicine have been proposed. There are side effects related to male hormones and there are parts that cannot be used by women, and there are topical treatments based on oriental medicine in Korea, China, Japan, etc.

To solve various skin allergies, inflammation, dandruff, and hair loss problems, natural and eco-friendly shampoos have come out a lot to solve chemical shampoos. . As a result, after using natural shampoo, problems such as scalp inflammation and dandruff occur, and hair loss starts due to ingredients that are not washed well. became desperate.

Korean Patent No. 10-1147984

Therefore, in order to overcome the above problems, the present invention is to eliminate the chemical elements of existing shampoos and to create eco-friendly materials so that people of all ages can use eco-friendly shampoos with hypoallergenicity.

In order to achieve the above object, this shampoo contains extracts extracted from hydrogen peroxide, elm extract and natural malt extract, black soybean extract, coriander fruit extract, sewage extract, bay leaf extract, tarragon leaf extract, iris extract and EM useful microorganisms. It is added and prepared by dissolving it in a mixed solution with an eco-friendly surfactant.

One aspect of the present invention provides an eco-friendly shampoo composition made without chemical stimulation using a natural material extract.

In one aspect of the present invention, there is provided a shampoo composition comprising a natural material elm tree extract, a natural material malt extract, a black bean extract, a coriander fruit extract, a sewage extract, a bay leaf extract, a tarragon leaf extract, and an iris extract.

In one aspect of the present invention, there is provided a shampoo composition comprising a natural surfactant, alkyl polyglucoside (C08-14 alkyl polyglucoside).

In one aspect of the present invention, there is provided an antibacterial and bactericidal shampoo composition using hydrogen peroxide.

In one aspect of the present invention, there is provided an eco-friendly shampoo composition made using useful microorganisms (EM).

Unlike conventional shampoos, the composition for hair according to one aspect of the present invention uses only eco-friendly materials to help manage scalp and hair, prevents aging, makes hair shiny, suppresses hair loss-causing bacteria, and promotes hair growth also effective

The composition for hair according to one aspect of the present invention is also effective in treating skin inflammation due to hydrogen peroxide and elm extract.

Unlike other chemical products, the composition for hair according to one aspect of the present invention can be used by men and women of all ages without irritation to the scalp.

The composition for hair according to one aspect of the present invention can provide various options to people who have to choose a shampoo with difficulty due to their sensitive scalp.

1 is a chemical structural formula of fulvic acid that may be included in a hair composition according to an aspect of the present invention.
2 is an effect of fulvic acid that may be included in the hair composition according to one aspect of the present invention.
Figure 3 shows the effect of hydration and nutrition of hydrolyzed collagen.
4 to 6 are photographs showing the cleaning power of the shampoo composition according to Experimental Example 1 of the present invention.

The above objects, other objects, features and advantages of the present invention will be easily understood through the following preferred embodiments in conjunction with the accompanying drawings. However, the present invention is not limited to the embodiments described herein and may be embodied in other forms. Rather, the embodiments introduced herein are provided so that the disclosed content may be thorough and complete, and the spirit of the present invention may be sufficiently conveyed to those skilled in the art.

Unless otherwise specified, all numbers, values, and/or expressions expressing ingredients, reaction conditions, and amounts of ingredients used herein refer to a variety of measures that may occur in obtaining such values, among others, in which such numbers are inherently different. Since they are approximations reflecting uncertainty, it should be understood as being modified by the term "about" in all cases. Also, where the disclosure discloses numerical ranges, such ranges are continuous and inclusive of all values from the minimum to the maximum inclusive of the range, unless otherwise indicated. Furthermore, when such ranges refer to integers, all integers inclusive from the minimum to the maximum inclusive are included, unless otherwise indicated.

In this specification, when a range is described for a variable, the variable will be understood to include all values within the stated range including the stated endpoints of the range. For example, a range of “5 to 10” includes the values of 5, 6, 7, 8, 9, and 10, as well as any subranges such as 6 to 10, 7 to 10, 6 to 9, 7 to 9, etc. It will be understood to include any value between integers that are appropriate for the scope of the recited range, such as 5.5, 6.5, 7.5, 5.5 to 8.5 and 6.5 to 9, and the like. Also for example, a range of "10% to 30%" includes values such as 10%, 11%, 12%, 13%, and all integers up to and including 30%, as well as 10% to 15%, 12% to It will be understood to include any subrange, such as 18%, 20% to 30%, etc., as well as any value between reasonable integers within the scope of the recited range, such as 10.5%, 15.5%, 25.5%, and the like.

In the present application, terms such as “comprise” or “have” are intended to designate that a feature, number, step, operation, component, part, or combination thereof described in the specification exists, but one or more other features It is to be understood that it does not preclude the possibility of the presence or addition of numbers, steps, operations, components, parts, or combinations thereof.

Various aspects of the present invention are as follows.

One aspect of the present invention includes a natural plant extract as an active ingredient, and the natural plant extract is an elm extract (Ulmus Campestris (Elm) Extract), malt extract, black bean (Glycine Soja (Soybeen) seed Extract) , Coriandrum Sativum (Coriander) Fruit Extract, Polygonum Multiflorum Extract, Laurus Nobilis Leaf Extract, Artemisia Dracunculus (Tarragon) Leaf/Stem Extract, and Calamus Extract ( Acorus Calamus Root Extract), wherein the natural plant extract is included in an amount of 0.1% to 1.0% by weight based on the total weight of the composition, and an alkyl polyglucoside as a natural surfactant, providing a hair composition .

The method for producing a natural plant extract according to the present invention comprises a natural plant (preferably elm tree) using at least one extraction solvent selected from _{water, dichloromethane, acetone, acetone aqueous solution, C 1-4} alcohol and C _{1-4 alcohol aqueous solution.} and extracting to obtain a solvent extract. As for the natural plant used in the step of obtaining the solvent extract, the whole plant of the above-ground part or underground part may be used. In the present invention, water or a common organic solvent may be used as the extraction solvent, and specifically, at _{least one selected from water, dichloromethane, acetone, aqueous acetone solution, C 1-5} alcohol, and C _1-5 alcohol aqueous solution may be used. have. If the extraction solvent is more specifically exemplified, water, dichloromethane, acetone, methanol, butanol or a mixed solvent thereof or an aqueous solution thereof containing 20 to 80% by volume of water may be used.

In one aspect of the present invention, it provides a composition for hair, further comprising 0.01 to 3% by weight of hydrogen peroxide. As the hydrogen peroxide, hydrogen peroxide having a concentration of 1 to 5% may be used, and preferably hydrogen peroxide having a concentration of 3% may be used.

In one aspect of the present invention, the composition comprises 0.1 wt% to 1.0 wt% of an elm extract based on the total weight of the composition; 0.01 to 3% by weight of hydrogen peroxide; 0.01 to 0.05 wt% of disodium EDI; Polyquaternium-10 0.1 wt% to 1.0 wt%; 1% to 5% by weight of cocamide mipa; 10% to 30% by weight of lauryl glucoside; 10% to 30% by weight of an alkyl polyglucoside; 3% to 7% by weight of cocobetaine; decyl glucoside 0.05 to 3% by weight; And Laureth-7 citrate 0.05 to 3% by weight; provides a composition for hair, including. When the above content range is satisfied, it helps the scalp and hair care, prevents aging, makes the hair shiny, inhibits bacteria that cause hair loss, and is effective for hair growth.

In one aspect of the present invention, the elm extract and hydrogen peroxide may be included in a weight ratio of 0.1 to 1: 0.01 to 3. When the above content range is satisfied, it helps the scalp and hair care, prevents aging, makes the hair shiny, inhibits bacteria that cause hair loss, and is effective for hair growth.

The present invention is an eco-friendly shampoo composition without chemical stimulation, and it is made of only natural ingredients without chemical ingredients, and suggests the treatment and prevention of allergies and various dermatitis.

In general, in recent years, air pollution has become more serious, and external and internal factors such as increased stress from daily life and the use of large amounts of chemical compounds in medicines and cosmetics increase the itching and dandruff of the scalp and the tendency of the hair to become coarser. have.

These shampoos are used to wash away the wastes of the hair, but the existing shampoos are manufactured for the purpose of being simply used to remove wastes, but are not effectively used when various troubles occur on the scalp. .

In addition, allantoin, ceptan, phenol, sulfur compounds, which are known as substances having an anti-dandruff effect, have toxicity or side effects in addition to the anti-dandruff effect. In addition, microparasites such as Demodex in the scalp and the proliferation of bacteria remaining in the skin pores adversely affect the hair, and there is a problem because products for suppressing this have not been proposed.

When the natural shampoo of the present invention is prepared, it is rich in minerals and can affect the scalp and hair. In addition, it can prevent hair loss by making the scalp healthy with antibacterial and antioxidant action, and the moisturizing function is effective. Using hydrogen peroxide, it is effective with only a small amount of addition, so it is not irritating to the scalp and can improve scalp health.

The present invention has been made from a bird's eye view of the above points, and by using natural materials that have not been utilized previously, to produce an eco-friendly and hypoallergenic shampoo composition having effects of hair root health, scalp protection, various scalp dermatitis treatments, and hair loss prevention effects. There is this.

Hereinafter, a method for producing the shampoo composition of the present invention will be described.

First, an extract is obtained by adding an extraction solvent to the elm tree.

Next, a formulation step of formulating by adding a thickener, a surfactant, and an additive based on the elm extract is performed.

The thickener is to increase the viscosity by being mixed with the elm extract, and Polyquaternium-10 may be used in the present invention. Polyquaternium prevents frizz and improves the shape and feel of the hair. Instead of polyquaternium, natural cellulose or xanthan gum can be used. The thickener may be mixed in an amount of 1 to 5% by weight of the hair shampoo composition.

Natural surfactants are used as surfactants.

An alkyl polyglucoside (C08-14 alkyl polyglucoside) is used as a natural surfactant. Alkyl polyglucoside is a molecular structure that can realize the advantages of nonionic surfactants and anionic surfactants. When combined with other surfactants, there is an irritation reduction effect.

Coco betaine is used as a cationic surfactant. Cocobetaine is a surfactant extracted from coconut oil and has a conditioning effect by preventing static electricity without irritating the scalp. The surfactant may be mixed in an amount of 20 to 50% by weight of the total composition.

And as additives, a moisturizing agent, a solubilizer, an essence oil, a natural preservative such as grapefruit extract, and the like are further added. Additives may be mixed in an amount of 5 to 20% by weight of the total composition.

As a moisturizer, glycerin, betaine extracted from sugar cane, dielpanthenol, etc. can be used.

Conventional emulsifiers may be used as the solubilizer, but olive liquid is preferably used. Olive Liquid is a solubilizer extracted from olive oil. The essential oil uses conventional herbal essence oil extracted from herbs as added for flavor.

In addition, the present invention may further mix the EM fermentation broth in the formulation step. For example, 20 to 80 parts by weight of the EM fermentation broth may be mixed with respect to 100 parts by weight of the elm extract. In this case, the amount of the hair shampoo composition of the present invention plus the elm extract and the EM fermentation broth from the total weight of the composition may be 30 to 70% by weight. In addition, hydrogen peroxide solution is added.

Hereinafter, a description of the ingredients for the shampoo composition.

The shampoo composition can be formulated using fulvic acid, hydrolyzed collagen, elm extract and natural malt extract, black soybean extract, cilantro extract, sorghum extract, bay leaf extract, tarragon leaf extract, and iris extract.

Fulvic acid is a type of humic acid synthesized by decomposing sediments of various animals and plants by microorganisms over a long period of time. plays a role It is registered with the US Food and Drug Administration (FDA) and the European Federal Food Safety Administration (EFSA). Fulvic acid plays a role in promoting growth and antibacterial effect, bacteriostatic effect (stop the proliferation of harmful bacteria), decomposition of toxic pollutants (antiviral characteristic), cell regeneration and growth effect, and actively helping metabolism. 1 is a chemical structural formula of fulvic acid. Figure 2 is the effect of fulvic acid.

Hydrolyzed collagen is a hard protein contained in many connective tissues such as bones, cartilage, tendons, ligaments, and skin of animals, and this substance is obtained through hydrolysis. It gives vitality and conditioning to the skin and hair, prevents static electricity in the hair and helps to form a film, so it gently wraps the skin, provides moisture to the skin, and keeps the skin moist. Figure 3 shows the effect of hydration and nutrition of hydrolyzed collagen.

The hair composition, particularly the shampoo composition, according to one aspect of the present invention may be configured as follows.

in the ratio of 100 purified water

Disodium EDTA 0.03,

Polyquaternium-10 0.40,

Potassium Cocoyl Hydrolyzed Collagen 6.00

Cocamide MIPA 3.50,

Lauryl Glucoside 20.00

Alkyl polyglucoside 20.00,

Potassium Cocoyl Glycinate 20.00,

Coco-Betaine 5.00,

Humic acid 2.00,

Polysorbate 2.00,

sodium chloride 2.00,

Decyl glucoside 1.00,

Laureth-7 Citrate 1.00,

Ulmus Campestris (Elm) Extract, Malt Extract, Glycine Soja(Soybeen) seed Extract, Coriandrum Sativum (Coriander) Fruit Extract, Polygonum Multiflorum Extract , Laurus Nobilis Leaf Extract, Artemisia Dracunculus (Tarragon) Leaf/Stem Extract, Acorus Calamus Root Extract - 0.50

Citric Acid 1.00,

Hydrogen peroxide (Hydrogen peroxide) 3% - It will be composed of 0.05 to 3.00.

Components of the hair composition according to one aspect of the present invention may be as shown in Table 1 below.

Part Trade Name INCI Name Content(%) A Di Water Water (purified water) To 100 EDTA-2Na Disodium EDTA 0.03 Miconium PQ10-J3000 Polyquaternium-10 (Polyquaternium-10) 0.40 Potassium Coco Hydrolyzed Protein Potassium Cocoyl Hydrolyzed Collagen 6.00 B Comperlan IP Cocamide MIPA 3.50 C MILCOSIDE 200 Lauryl Glucoside 20 MILCOSIDE 300 Alkyl polyglucoside 20 Amilite GCK-12 Potassium Cocoyl Glycinate 20 Dehyton AB30 Coco-Betaine 5.00 Humic acid Humic acid 2.00 Polysorbate Polysorbate 2.00 Salt Sodium chloride 2.00 PLANTACARE 2000 Decyl Glucoside (decyl glucoside) 1.00 D PLANTAPON LC 7 Laureth-7 Citrate 1.00 Fragrance - q.s. E Preservative - q.s. CS Comples G(H) Ulmus Campestris (Elm) Extract, MaltExtract, Glycine Soja(Soybeen) seed Extract, Coriandrum Sativum (Coriander) Fruit Extract, Polygonum Multiflorum Extract, Laurus Nobilis Leaf Extract, Artemisia Dracunculus (Tarragon) Leaf/Stem Extract), Acorus Calamus Root Extract) 0.50 Anhydrous Citric Acid Citric Acid 1.00 Hydrogen peroxide Hydrogen peroxide 3% (Hydrogen peroxide 3%) Food additive 0.05

In addition, the use of the compositions constituting the shampoo may be as shown in Table 2 below.

Part purpose INCI Name Content(%) A Water (purified water) To 100 hair conditioning agent
Surfactant-cleaning agent Potassium Cocoyl Glycinate 20 Surfactant (cleaning agent) Lauryl Glucoside 20 Surfactant (cleaning agent) Alkyl polyglucoside 20 B hair conditioning agent, skin conditioning agent,
Surfactant (cleaning agent) Potassium Cocoyl Hydrolyzed Collagen 6 C Antistatic agent, hair conditioning agent, skin conditioning agent, foaming agent, thickener Coco-Betain 5 skin conditioning agent Humic acid 2 D Denaturant, fragrance, hair conditioning agent, moisturizer, skin moisturizer, skin protectant, viscosity reducing agent Polysorbate 2 thickener - water soluble Sodium chloride 2 E Fragrance, pH regulator Citric acid One Antistatic agent, film forming agent,
hair fixative Polyquaternium-10 0.4

The effects of the components are as follows.

The young leaves of the elm tree are edible in spring, and the bark of the elm tree is used as a medicinal herb called yew. It is used to detoxify and detoxify the skin. Respiratory, allergy, anti-cancer, diarrhoea, swelling, digestive, anti-inflammatory, anti-inflammatory, and detoxifying action. , blood circulation, and prevents the rise and accumulation of serum cholesterol levels, so it is a good material for hardening of the alliance and cerebrovascular disease. Elm is known to be effective in treating inflammation because it is rich in antioxidants and is effective in alleviating allergic reactions and relieving inflammation. It provides moisture to hair, prevents moisture evaporation, and has a protective effect from UV rays.

Malt extract is a substance made by filtering and drying a solution obtained by saccharifying malt in the same way as in brewing beer. It does not contain hops and is manufactured and sold by Difco Laboratories, etc. in the US for medium adjustment of yeast and mold. A 10% aqueous solution of malt extract has about 10% monosaccharides (mainly glucose), about 60% disaccharides (mainly maltose), and about 15% trisaccharides (mainly maltotriose) with almost the same sugar composition as 10% non-hoppy barley juice of the extract. . It is a plant extract obtained by evaporating the water-soluble extract of partially germinated barley seeds. It contains important substances as a growth factor for peptong, yeast, and filamentous fungi, so it can help to increase skin elasticity and luster and provide nutrition. It has mainly skin conditioning and skin soothing effects, so it can be used in various types of cosmetics.

Coriander fruit extract is an extract obtained by adding a solvent to the fruits of coriander (coriander, coriander, oleander, bedbug). Coriander is a dicotyledonous plant belonging to the umbel family, and is a type of herb that is native to many countries along the Mediterranean coast. It is similar to water parsley, has a rich aroma among spices, and has a flavor similar to a mixture of lemon peel and sage. Coriander is mainly cultivated in temples, and in oriental medicine, coriander fruit is called hoyuja and is used as a medicinal plant. Coriander fruit has an antibacterial effect and is used in cosmetics to add natural fragrance.

The sewage extract is taken from the sewage. The succulent is a tuberous root, which is in the shape of a square or a lump, and is 5-15 cm long and 3-10 cm in diameter. The outer surface is reddish-brown to blackish-brown, rather uneven, not flat, with shallow grooves, irregular wrinkle patterns and vertical grooves. In addition, there is a horizontally long bark or continuous stripe, a single cut mark is evident at both ends, and a fibrous vascular bundle is exposed. The vagina is tough and hard, making it difficult to cut. The cut side is light yellowish brown to light reddish brown, powdery, and on the skin 4 to 11 near-circular heterogonal vascular rings are gathered to form a flower pattern called "Golden Gate". The central neck is relatively large, and the neck can sometimes be seen. It has no odor and the taste is slightly bitter and astringent. It is said that the root of Hsuo was widely used as a medicine for longevity during the Tang Dynasty in China. It regulates skin immunity to prevent aging, and provides elasticity and energy to the skin, making it elastic and lively. In addition, it is excellent for protecting the skin by inhibiting the generation of active oxygen, one of the factors that cause skin troubles, and also protecting sensitive skin by inhibiting the production of TRAC and MDC, which are skin inflammatory substances, and EWG grade 0 for sensitive skin. People can also use it safely. It is also effective in alleviating troubles by inhibiting the production of nitric oxide, an inflammatory marker, in cells.

Bay leaf extract is a component obtained by cold-pressing bay leaves. Laurel is distributed along the Mediterranean coast and southern Europe. It has a unique scent and acts as a spice to add flavor to food, and the raw leaves are dried and used for medicine or cooking. Laurel leaves have antibacterial properties, so when used on acne or sensitive scalp, it has a calming effect and helps with hair health. It acts as a tonic to condition the skin and prevent dryness by blocking moisture evaporation. As a natural fragrance, it also serves to impart a fragrant natural fragrance to cosmetics. It protects the skin by removing free radicals including free radicals that damage cells, and when it enters into hair care products, it helps to relieve dandruff and provides nutrition to the scalp and hair.

Tarragon leaf extract is an extract obtained from tarragon. Tarragon has a sweet scent and a spicy yet bitter taste that French gourmet lovers regard as the queen of spices. It is an indispensable spice in French cuisine, and it is said that in the past, it was grown only in the gardens of the royal palace and used as a valuable medicinal herb in high society. The leaves are mainly used for cooking. It is said that Christians put a branch of tarragon in their shoes when they set out on a long road to Jerusalem and set out for the Holy Land. Tarragon is a tonic, good for the head, heart, and liver, and helps recover from fatigue. The leaves are rich in iodine, minerals, salt and vitamin C, and have been used as a remedy for vitamin deficiency. Tarragon is a rich source of vitamins such as vitamin C and vitamin A, as well as a group of B-complex vitamins such as folic acid, pyridoxine, niacin and riboflavin, and acts as an antioxidant and cofactor.

A natural surfactant, C08-14 alkyl polyglucoside, was added to remove chemical elements. The keyword in the recent development of surfactants was 'Sustainable'. The key was how sustainable natural materials could be without environmental destruction, and in the field of environment-oriented interfacial material research, representative categories are protein bases, vegetable oil bases, and carbohydrates. The sugar-based surfactant is also a representative carbohydrate-based surfactant. Alkylglucosides are nonionic (non-ionizing, non-charged) surfactants that come from sugars, usually glucose derivatives, and fatty alcohols. The raw materials are starch and fat, and the final product, alkyl polyglucoside, is a complex of various sugars with hydrophilic and lipophilic groups. Therefore, it is a non-irritating, non-toxic, and naturally renewable, eco-friendly surfactant that has excellent performance and is widely used in detergents, cosmetics, food, and high-end pharmaceutical soaps. It is a material with excellent safety for the human body and the environment, and has a molecular structure that can realize the advantages of nonionic surfactants and anionic surfactants. When combined with other surfactants, there is an irritation reduction effect. It has a structure that has no controversy over the harmfulness of ethylene oxide and nitrosamines (carcinogens), and is very stable in an alkaline environment.

Hydrogen peroxide is added. Hydrogen peroxide is a compound represented by _{H 2} O ₂ having a molecular weight of 34 in which hydrogen and oxygen are combined. It is used as a disinfectant for wounds, and is a liquid with a greater viscosity than water with a blue color. Because of its strong oxidizing power, it is often used to bleach organic materials such as silk, hair, feathers, and nails, as an oxidizing agent for analytical reagents, as a bleaching agent for silk or wool, and as a catalyst for vinyl polymerization in the plastics industry. The density of hydrogen peroxide is 1.463 g/cm ³ , and the melting point is 0.43°C and the boiling point is 150.2°C. It is characterized as a colorless liquid with a characteristic odor and slightly acidic taste. A solution diluted 20 to 40 times with hydrogen peroxide is used as a hair lightening agent, and a solution of 3 to 5% (6 to 10 times dilution) of hydrogen peroxide has sterilizing ability and is therefore widely used in treatment. Hydrogen peroxide decomposes to form water and is generally considered an environmentally safe alternative to chlorine-based bleach as it is safe as an antimicrobial agent by the U.S. Food and Drug Administration (FDA). As the hydrogen peroxide, hydrogen peroxide having a concentration of 1 to 5% may be used, and preferably hydrogen peroxide having a concentration of 3% may be used.

Add dietary sulfur. Sulfur is one of the main constituents of our human body. Sulfur is the second most abundant element after water, carbon, oxygen, hydrogen, nitrogen, calcium, and phosphorus. Sulfur is used a lot in the human body. It is also used as a raw material for 'cartilage' and 'collagen', and is also a substance necessary to produce 'glutathione', a core antioxidant in our body. It is an important ingredient. Since sulfur itself has very diverse uses in the human body, various effects can be expected when sulfur is used in the human body. Usually, when people think of sulfur, they think of sulfur, and sulfur is a substance that comes from volcanoes and is known as a poison. Dietary sulfur, which is sulfur added to the composition, is sulfur in the form of organic sulfur bound to oxygen. Such organic sulfur does not cause any problems in the human body. Inorganic sulfur is known to be poisonous and should be avoided. Dietary sulfur is a powerful anti-inflammatory substance, and the expression of pain in our body means that there is an inflammation somewhere. In addition, sulfur is required for the production of glutathione, an antioxidant that gives antioxidant action, and dietary sulfur is useful at this time. Dietary sulfur is good for healing damaged muscles, and it is often used as a treatment for skin diseases, and it helps to improve skin protein by adding sulfur, which has been used as an effective method for detoxification. You can also see the effect of improving the scalp by adding dietary sulfur.

When formulated in this way, the benefit of being able to use it easily even for people with sensitive skin or not seeing the effect due to chemical stimulation can be seen from the test results below.

Hereinafter, the present invention will be described in more detail through specific experimental examples. The following experimental examples are merely examples to help the understanding of the present invention, and the scope of the present invention is not limited thereto.

Example 1. Preparation of shampoo hair composition

A shampoo hair composition was prepared based on Table 1 above. Part A of Table 1 is first added to the composition constituting the shampoo, and then B, C, and D are added after mixing. After mixing after 1 hour, elm extract among the extracts of E was added and stirred in a bath to prepare a natural shampoo. The elm extract was prepared by the following process.

A method of extracting distillate by mixing 5 kg of dried elm bark and leaves with 1.5% distilled water and heating it with an ultra-high-speed vacuum low temperature concentration extractor (capacity 50L) at the water temperature of 85℃, and then cooling the steam through a tube was used to extract for 4 hours. After extracting for 4 hours, about 10 kg of extract comes out. The extract of elm tree prepared through the above process was used.

In addition, the composition of Example 1 was the same as in Table 1, that is, Disodium EDTA 0.03, Polyquaternium-10 0.40, Potassium Cocoyl Hydrolyzed Collagen (Potassium Cocoyl Hydrolyzed) Collagen 6.00, Cocamide MIPA 3.50, Lauryl Glucoside 20.00, Alkyl polyglucoside 20.00, Potassium Cocoyl Glycinate 20.00, Cocobetaine ( Coco-Betaine) 5.00, Humic acid 2.00, Polysorbate 2.00, Sodium chloride 2.00, Decyl glucoside 1.00, Laureth-7 Citrate 1.00 , Citric Acid 1.00, Ulmus Campestris (Elm) Extract, 3% hydrogen peroxide (Hydrogen peroxide 3%) - A shampoo hair composition was prepared with a composition of 0.05. The hydrogen peroxide 3% is a food additive pharmaceutical grade 3% hydrogen peroxide solution.

Experimental Example 1. Clinical follow-up experiment through several test subjects for 6 months

The present applicant conducted an observational study on the shampoo prepared as described above by conducting a research experiment through several test subjects over 6 months. Below, 20 subjects, regardless of gender, were selected to shampoo every day, and the results were observed and studied after shampooing.

In fact, after using the shampoo, secretions and sebum were washed away much more cleanly as an effect of cleaning power, and it was visually confirmed that the red scalp regained its original color due to the reduced fever. It was visually confirmed that the hair, which had been falling out to some extent, was restored to the scalp and the hair loss gradually decreased.

Among them, three patients with severe symptoms were selected and the following experimental results were confirmed in FIGS. 4 to 6 .

Figure 4 is a scalp diagram showing the effect of using the shampoo of a 32-year-old woman, Kim ㅇㅇ, who participated in the experiment. 4A is a photograph before shampoo use. Figure 4b is a picture after 2 weeks of shampoo use. Figure 4c is a picture after 4 weeks of shampoo use. As shown in Fig. 4, it can be seen that the composition of the present invention has excellent cleaning power and is quite effective in preventing dandruff and dermatitis. Seborrheic dermatitis can also be treated.

5 is a photo of the scalp showing the effect of using the shampoo of a 21-year-old female, Mr. Lee ㅇㅇ, who participated in the experiment. Figure 5a is a picture before shampoo use, Figure 5b is a picture after 2 weeks of shampoo use. Figure 5c is a picture of the shampoo after 4 weeks of use, the reddish scalp returned to its original color much compared to the previous one, and the hair loss due to increased heat was also improved, showing the appearance of less falling out. In fact, when the experimenter checked the hair loss after drying every day, it continued to shrink.

6 is a photo of the scalp showing the effect of using the shampoo of a 56-year-old male, Mr. Lee ㅇㅇ, who participated in the experiment. 6A is a picture before shampoo use, and FIG. 6B is a picture after 4 weeks of shampoo, and it can be seen that inflammatory wounds such as pimples on the scalp disappear over time.

Experimental Example 2. A survey after shampoo use for 3 months in the age group in their 20s and 30s

Recently, the number of hair loss patients in the age group in their 20s and 30s has increased, and most of them are suffering from hair loss symptoms due to scalp fever. With this shampoo composition, 20 people in their 20s and 30s suffering from scalp fever were selected and asked to use the shampoo for 3 months and received a questionnaire once a week.

The results of using the shampoo of Example 1 for 20 people suffering from scalp fever for 3 months were shown in Table 3 below.

Out of 5 points per person, based on a total of 100 points (5 points - very good effect, 4 points - good effect, 3 points - moderate effect, 2 points - not very effective, 1 point - no effect at all none)

division 4 weeks 8 weeks 12 weeks dandruff and dead skin cells 27 62 83 flexibility 35 70 90 hair loss 19 51 73 itching 22 50 84

Experimental results show that it is getting more and more effective. In general, the stress given by the accumulation of internal and external wastes and dead skin cells covering the pores affects the secretion of hormones, weakening the health of the scalp, and bacteria and mold caused by wastes generate unpleasant odors. It was found that it made the scalp healthy first and led to other effects.

Lee OO (30 years old, female), who participated in the experiment, has a seborrheic scalp, and the scalp is always red due to fever. It was confirmed that the scalp became healthy and the itchiness disappeared. As a result, Lee OO liked it, saying that it does not itch, the scalp becomes healthy, and dandruff disappears so that he can lead a social life with confidence. Another participant, Yoo OO (27 years old, male), has a dry scalp, and her hair is also dry. When she goes outside after washing her hair, she looks frizzy and her hair keeps getting thinner and hair loss occurs. In order to solve the problem, the hair fell out more by winding it with a shampoo with a lot of chemical ingredients, so I used a shampoo composition during the trouble. Seo OO (32 years old, female) said that she had the best cleaning feeling among the eco-friendly shampoos she used, and that her hair seemed to be shiny. What was gradually more satisfying was that the more I touched the scalp, the less pimples I was worried about.

Also, as a clinical example, when one person's hair was wound with the shampoo containing chemical components on one side and the shampoo composition on the other side, it was confirmed that the hair on the side wound with the shampoo composition was much less damaged.

Preparation of Examples 2-4

[Example 2]

It was prepared in the same manner as in Example 1, except that 1.00 wt% of hydrogen peroxide was used. The hydrogen peroxide is a food additive pharmaceutical grade 3% hydrogen peroxide solution.

[Example 3]

It was prepared in the same manner as in Example 1, except that 2.00 wt% of hydrogen peroxide was used. The hydrogen peroxide is a food additive pharmaceutical grade 3% hydrogen peroxide solution.

[Example 4]

It was prepared in the same manner as in Example 1, except that 3.00% by weight of hydrogen peroxide was used. The hydrogen peroxide is a food additive pharmaceutical grade 3% hydrogen peroxide solution.

Experimental Example 3. Investigation of the effect of Examples 1-4

The following effects were investigated by randomly selecting 20 people in their 20s and 50s at random. Effect investigation was conducted using a 5-point measurement method (1: no effect, 2: problematic, 3: moderate, 4: effective, 5: very effective), with irritation or no stimulation, and the average was derived.

The survey results are shown in Table 4 below.

hair loss effect itching
ease moisturizing power shampoo foam detergency pepper Example 1 2.82 3.66 3.55 3.61 3.24 does not exist Example 2 3.12 4.18 3.52 4.11 4.28 does not exist Example 3 3.28 4.21 3.52 4.12 4.52 does not exist Example 4 4.16 4.56 3.55 4.12 4.50 does not exist

From the above results, it can be seen that the shampoo composition of the present invention has an effect on preventing hair loss, and at the same time plays a role in preventing dandruff, maintaining hair gloss, and reducing heat. In addition, it can be confirmed that the use of hydrogen peroxide has good results in eradicating bacteria. Good bacteria are generally aerobic and basically need oxygen to survive. Conversely, harmful bacteria are anaerobic and cannot survive in an oxygen-rich environment. Hydrogen peroxide is an all-weather eco-friendly shampoo composition that not only acts as a preservative in the manufacture of natural shampoo, but also blocks the environment for bacteria and bacteria to survive.

Claims (3)

In the hair composition comprising a natural plant extract as an active ingredient,
The natural plant extract includes an elm extract (Ulmus Campestris (Elm) Extract),
The composition is based on the total weight of the composition
0.1% to 1.0% by weight of elm extract;
0.01 to 0.1% by weight of hydrogen peroxide;
0.01 to 0.05 wt% of disodium EDI;
Polyquaternium-10 0.1 wt% to 1.0 wt%;
1% to 5% by weight of cocamide mipa;
10% to 30% by weight of lauryl glucoside;
10% to 30% by weight of an alkyl polyglucoside;
3% to 7% by weight of cocobetaine;
decyl glucoside 0.05 to 3% by weight; and
Laureth-7 citrate 0.05 to 3% by weight; containing,
composition for hair.
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