KR102234579B1 - Bubble peel-off pack cosmetic composition and their manufacturing method - Google Patents

Abstract

The present invention relates to a bubble peel-off pack cosmetic composition and a manufacturing method thereof. More particularly, the present invention relates to a bubble peel-off pack cosmetic composition, which is excellent in usability by shortening the drying time when using products of a peel-off pack formulation, which is gently removed when a film is removed, thereby having little skin irritation, and which exhibits excellent moisturizing power.

Description

Bubble peel-off pack cosmetic composition and its manufacturing method {BUBBLE PEEL-OFF PACK COSMETIC COMPOSITION AND THEIR MANUFACTURING METHOD}

The present invention relates to a bubble peel-off pack cosmetic composition and a method of manufacturing the same, and more particularly, it has excellent usability by shortening the drying time when using the product of the peel-off pack formulation, and is gently removed when removing the film to reduce skin irritation. It relates to a cosmetic composition for a bubble peel-off type pack that is small and exhibits excellent moisturizing power.

Recently, consumers have used toners and lotions for hydration, cleanliness, epidermal blood circulation, removal of dead skin cells or foreign substances such as dead skin epithelial cells, oil control, skin nutrition, removal of wrinkle residues, skin uniformity, wrinkle reduction, etc. Pack products such as sheet masks and wash-off masks are used for special care purposes along with basic cosmetics such as, cream, etc. The function of such a pack varies depending on the formulation, but it refers to a cosmetic composition for the purpose of physical removal of waste products from the skin, improvement of skin blood circulation, and moisturization, which means'covering'.

Depending on how to use the pack, there are a wash-off type that rinses off after a short period of application, a sleep pack type that is washed the next morning, and a peel-off type that removes the film formed after a short period of application. Among them, in the case of a peel-off type pack, it does not require a base material made of non-woven fabric, and does not require a separate cleansing, and the skin contracts as a film is formed in the process of removing wastes on the skin surface and drying it. It is a product line that is growing rapidly in recent years because it shows a temporary pore contraction effect.

However, in the case of this peel-off type pack, since it has high adhesion to the skin, it is removed by a physical removal method when the pack is removed from the skin after drying, so irritation may appear on the skin depending on the skin condition of the consumer. The disadvantage is that it is difficult to use on the skin. In addition, when the pack is removed after drying, it is easily torn and a residue may remain on the skin.

A method of increasing the viscosity of the peel-off pack is used to solve the problem of not being able to remove the pack as described above. The first method is a method of increasing the viscosity by increasing the content of polyvinyl alcohol, which is a film forming agent. When the content of vinyl alcohol is used in an amount of 15 parts by weight or more, the viscosity increases, so that the spreadability decreases and the drying time is lengthened. The second method is to increase the viscosity of the formulation by using a high-molecular polymer, but this method also increases its own viscosity, but causes problems such as lowering of spreadability, and the function of increasing the tensile strength of the pack other than increasing the viscosity is weak. .

Republic of Korea Patent Publication No. 10-2017-0071313

The present invention is to solve the above problems, shortening the drying time after application to the skin, and allowing the dried product to be peeled off smoothly and without irritation when peeling off the skin surface after drying, for a bubble peel-off type pack To provide a cosmetic composition.

The above and other objects and advantages of the present invention will become apparent from the following description of preferred embodiments.

The object is purified water; Methyl perfluoroisobutyl ether, methyl perfluorobutyl ether, ethyl perfluorobutyl ether, ethyl perfluoroisobutyl ether, tetrafluoropropene, trifluoropropyldimethicone, perfluorooctylt A blowing agent comprising at least one selected from the group consisting of ethoxysilane, and combinations thereof; Surfactants including decyl glucoside and potassium cocoyl glycinate; A film forming agent including an acrylate copolymer and polyvinyl alcohol; And a solvent selected from the group consisting of ethanol, isopropyl alcohol, 1,3-butylene glycol, propylene glycol, propanediol, 1,2-hexanediol, and combinations thereof; Containing, can be achieved by a cosmetic composition for a bubble peel-off type pack.

Specifically, the cosmetic composition may be dried and peeled off after forming bubbles when applied to the skin.

Specifically, the cosmetic composition, based on 100 parts by weight of the cosmetic composition, foaming agent 1 to 10 parts by weight, decyl glucoside 0.1 to 10 parts by weight, potassium cocoyl glycinate 0.1 to 10 parts by weight, acrylate copolymer 0.5 to 10 It may include parts by weight, 5 to 15 parts by weight of polyvinyl alcohol, 50 to 80 parts by weight of purified water, and 5 to 20 parts by weight of a solvent.

The cosmetic composition for a bubble peel-off type pack according to the present invention automatically generates bubbles (bubbles) after being applied to the skin, and the film-forming agent is softened by the generated bubbles, so that when the product is removed from the skin after drying, it is smooth without skin irritation. It has the effect of separating.

In addition, according to the present invention, the surface area of the film-forming agent is increased by bubbles generated after skin application, so that the time for natural drying is shortened, so that the product can be used quickly and conveniently.

The cosmetic composition for a bubble peel-off type pack according to the present invention exhibits excellent anti-inflammatory and antioxidant effects, has excellent antibacterial properties, and can relieve skin irritation without causing skin diseases such as dermatitis and allergies. By preventing the phenomenon, it has the effect that the storage period is long.

However, the effects of the present invention are not limited to the above-mentioned effects, and other effects not mentioned will be clearly understood by those skilled in the art from the following description.

Figure 1 (a) and (b) is a photo (a) and a dried bubble peel-off pack cosmetic composition removed from the skin after applying the bubble peel-off pack cosmetic composition to the skin according to an embodiment of the present invention. It shows the picture (b).

Hereinafter, the present invention will be described in detail with reference to embodiments of the present invention and drawings. These examples are only illustratively presented to explain the present invention in more detail, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not limited by these examples. .

In addition, unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs, and in case of conflict, the present specification including definitions The description of will take precedence.

In order to clearly describe the invention proposed in the drawings, parts irrelevant to the description are omitted, and similar reference numerals are attached to similar parts throughout the specification. And, when a certain part "includes" a certain component, this means that other components may be further included rather than excluding other components unless specifically stated to the contrary. In addition, the "unit" described in the specification means one unit or block that performs a specific function.

In each step, the identification code (first, second, etc.) is used for convenience of explanation, and the identification code does not describe the order of each step, and each step does not clearly describe a specific sequence in the context. It may be implemented differently from the order specified above. That is, each of the steps may be performed in the same order as the specified order, may be performed substantially simultaneously, or may be performed in the reverse order.

Hereinafter, embodiments and examples of the present application will be described in detail with reference to the accompanying drawings. However, it may not be limited to these embodiments and examples and drawings of the present application.

One aspect of the present application, purified water; Methyl perfluoroisobutyl ether, methyl perfluorobutyl ether, ethyl perfluorobutyl ether, ethyl perfluoroisobutyl ether, tetrafluoropropene, trifluoropropyldimethicone, perfluorooctylt A blowing agent comprising at least one selected from the group consisting of ethoxysilane, and combinations thereof; Surfactants including decyl glucoside and potassium cocoyl glycinate; A film forming agent including an acrylate copolymer and polyvinyl alcohol; And a solvent selected from the group consisting of ethanol, isopropyl alcohol, 1,3-butylene glycol, propylene glycol, propanediol, 1,2-hexanediol, and combinations thereof; It provides a cosmetic composition for a bubble peel-off type pack containing.

In one embodiment, the cosmetic composition may exhibit foaming properties. For example, as shown in FIG. 1, the cosmetic composition exhibits effervescent properties and forms bubbles when applied to the skin to express a foam shape (FIG. 1A), and may be peeled off from the skin after drying in the form of a film. Yes (Fig. 1B).

In one embodiment, the methylperfluoroisobutylether, methylperfluorobutylether, ethylperfluorobutylether, ethylperfluoroisobutylether, tetrafluoropropene, trifluoropropyldime A blowing agent containing at least one selected from the group consisting of chicon, perfluorooctyltriethoxysilane, and combinations thereof, is included to generate bubbles by using surfactants in the cosmetic composition and to promote the generation of bubbles. It can be. For example, when the cosmetic composition is applied to the skin, a volatile component contained in the foaming agent may be naturally vaporized into the air to form a bubble.

Specifically, the foaming agent can be used as a cosmetic composition and has excellent bubble generation power and high stability, methyl perfluoroisobutyl ether, methyl perfluorobutyl ether, or methyl perfluoroisobutyl ether and methyl purple It may contain a mixture of luorobutyl ether.

In one embodiment, the foaming agent may be included in an amount of about 1 to about 10 parts by weight based on 100 parts by weight of the cosmetic composition. If the foaming agent is included in an amount of less than about 1 part by weight, sufficient bubbles may not be formed when the cosmetic composition is applied to the skin or disappear quickly after bubble formation, and if it exceeds about 10 parts by weight, excessive bubbles may occur for an appropriate time. Since the bubble may be continuously generated without subsidence, the foaming agent is preferably included in an amount of about 1 to about 10 parts by weight based on the total 100 parts by weight of the cosmetic composition.

In one embodiment, the surfactant including decyl glucoside and potassium cocoyl glycinate may be included for the role of forming bubbles when the cosmetic composition is applied to the skin. For example, the surfactant including decyl glucoside and potassium cocoyl glycinate is a compound containing both a hydrophilic portion and a hydrophobic portion, and forms a micelle structure at a certain concentration or higher. When the micelle structure is formed at the air-water interface, the hydrophilic portion faces water, which is a bubble wall, and the hydrophobic portion faces air avoiding water, thereby generating bubbles.

In one embodiment, the decyl glucoside and potassium cocoyl glycinate may be included in an amount of about 0.1 to about 10 parts by weight, respectively, based on 100 parts by weight of the cosmetic composition. If the decyl glucoside and potassium cocoyl glycinate are each contained in an amount of less than about 0.1 parts by weight, sufficient bubbles may not be formed, and when each exceeding about 10 parts by weight, the amount of bubbles generated is excessive and the film forming agent is excessive. As it is softened, there may be a problem that the film is not removed neatly even after drying. Preferably, the decyl glucoside and potassium cocoyl glycinate are each about 0.1 to about 5 parts by weight, about 0.1 to about 3 parts by weight, about 0.5 to about 5 parts by weight, or about 100 parts by weight of the cosmetic composition. It may be included in an amount of 0.5 to about 3 parts by weight.

In one embodiment, the film-forming agent may be included in the cosmetic composition to form a thin film on the skin surface to peel off after drying, and additionally, to be attached to the skin through an increasing effect. I can.

In one embodiment, the film forming agent may include polyvinyl alcohol. The polyvinyl alcohol is a polymer compound and may be prepared by adding ethanol to a vinyl acetate polymer to form a gum, but is not limited thereto.

In one embodiment, the polyvinyl alcohol may be included in an amount of about 5 to about 15 parts by weight based on 100 parts by weight of the cosmetic composition. If the polyvinyl alcohol is contained in less than about 5 parts by weight, the film is not sufficiently formed to function as a peel-off pack, and if it exceeds about 15 parts by weight, the film is excessively formed and a feeling of irritation during peel-off after use of the product This is severe and can take a long time to dry.

The cosmetic composition according to an embodiment of the present invention contains a small amount of the polyvinyl alcohol so as not to exceed about 15 parts by weight relative to the total cosmetic composition, but shows excellent peel-off performance and reduces skin irritation. It may be to include together. The acrylate copolymer refers to a copolymer composed of two or more monomers composed of acrylic acid, methacrylic acid, or simple esters thereof.

In one embodiment, the cosmetic composition includes an acrylate copolymer as a film forming agent, thereby helping to maintain the skin level while forming a thin film, and providing a soft finish, compared to when polyvinyl alcohol alone was included. While minimizing skin irritation, the film can be easily formed.

In one embodiment, the acrylate copolymer may be included in an amount of about 0.5 to about 10 parts by weight based on 100 parts by weight of the cosmetic composition. If the acrylate copolymer is included in an amount of less than about 0.5 parts by weight, the film-forming effect may be insignificant or skin irritation may increase, and if it exceeds about 10 parts by weight, the viscosity increases excessively, resulting in a decrease in spreadability and excessive film formation. This can increase the risk of causing irritation. Preferably, the acrylate copolymer may be included in an amount of about 0.5 to 5 parts by weight based on 100 parts by weight of the cosmetic composition.

In one embodiment, the purified water and the solvent serve as a medium for dissolving the components of the cosmetic composition, and at the same time, retain these components and maintain them as a liquid composition, and may affect the spreadability of the cosmetic composition. .

In addition, the solvent may improve the drying speed to rapidly form a film on the skin surface, and may serve to improve the foamability of the cosmetic composition by exhibiting a vaporizing power.

In an embodiment, the purified water may be included in an amount of about 50 to about 80 parts by weight based on 100 parts by weight of the cosmetic composition. If the purified water is contained in an amount of less than about 50 parts by weight, the viscosity of the cosmetic composition may increase excessively and thus spreadability may decrease, and if it exceeds about 80 parts by weight, the time required for drying may increase.

In one embodiment, the solvent may be used without limitation as long as it can dissolve the constituents included in the cosmetic composition, and specifically, ethanol, isopropyl alcohol, 1,3-butylene glycol, propylene glycol Cole, propanediol, 1,2-hexanediol, and may include those selected from the group consisting of combinations thereof, and more specifically, may include ethanol.

In one embodiment, the solvent may be included in an amount of about 5 to about 20 parts by weight based on 100 parts by weight of the total cosmetic composition, and if it is included in less than about 5 parts by weight, the effervescent power of the cosmetic composition is insufficient. It may be insufficient, and if it exceeds about 20 parts by weight, volatility becomes strong, and stability at high temperatures may decrease.

Specifically, the cosmetic composition, based on 100 parts by weight of the cosmetic composition, about 1 to about 10 parts by weight of a foaming agent, about 0.1 to about 10 parts by weight of decylglucoside, about 0.1 to about 10 parts by weight of potassium cocoyl glycinate, acrylic It may include about 0.5 to about 10 parts by weight of a rate copolymer, about 5 to about 15 parts by weight of polyvinyl alcohol, about 50 to about 80 parts by weight of purified water, and about 5 to about 20 parts by weight of a solvent.

In one embodiment, the cosmetic composition may further include a noni fruit extract. For example, the noni fruit extract may contain proxeronine, scopoletin, and iridoid as a phytochemical, which is a plant chemical. It recovers, helps to improve skin elasticity by promoting collagen synthesis, and can alleviate tension in the skin that may occur when using a peel-off pack.

In addition, the noni fruit extract contains damnacanthal, which is an antioxidant, so that it contains minerals and vitamin C abundantly, thereby exhibiting a skin whitening effect, protecting skin damaged by UV rays, and improving wrinkles. .

In one embodiment, the noni fruit extract may be included in an amount of about 0.1 to about 10 parts by weight based on 100 parts by weight of the cosmetic composition. If the noni fruit extract is contained in an amount less than about 0.1 parts by weight, skin elasticity improvement, skin tension relief, anti-inflammatory, and skin whitening effects may be insignificant due to the noni fruit extract. Since the cost included in the manufacturing may increase excessively, the noni fruit extract is preferably contained in an amount of about 0.1 to about 10 parts by weight. More preferably, it may be included in an amount of about 0.1 to about 5 parts by weight.

In one embodiment, the cosmetic composition may further include a mugwort extract. For example, the mugwort extract (Korean wormwood extract) refers to a mugwort belonging to a perennial plant of the dicotyledonous plant, Chrysanthemum, asteraceae, specifically, it means that it is extracted from mugwort, sajaebalduk, mosquito mugwort, or mugwort. The mugwort extract may contain minerals such as calcium, copper, manganese, and chromium, flavonoids, vitamin C, and beta-carotene as active ingredients, thereby exhibiting antibacterial, anti-inflammatory, and antioxidant effects. For example, as the mugwort extract contains minerals, flavonoids, vitamin C, and beta-carotene as active ingredients, it heals skin wounds, relieves inflammation, soothes irritated skin, and removes free radicals to reduce skin aging. It can help prevent. In addition, by removing the activity of foreign substances harmful to the skin, it can help to manage problem skin by suppressing skin hypersensitivity reactions, and it can promote collagen synthesis, thereby exhibiting an effect of improving wrinkles.

In one embodiment, the mugwort extract may be included in an amount of about 0.1 to about 3 parts by weight based on 100 parts by weight of the cosmetic composition. If the mugwort extract is contained in an amount of less than about 0.1 parts by weight, antibacterial, anti-inflammatory, skin soothing, and antioxidant effects may not be sufficiently exhibited, and if it is included in an amount exceeding about 3 parts by weight, a strong scent may be exhibited and the preference may decrease.

In one embodiment, the cosmetic composition may further include polylysine. The polylysine is a polymer of lysine, an amino acid, and is synthesized by polymerization and desorption of an N-carboxy amino acid anhydride protecting an ε-amino group, or is found by aerobic culture of microorganisms in nature. The polylysine exhibits an α-helical structure when the ε-amino group is positively charged at pH 11 or higher, an irregular structure at pH 11 or lower, and a β structure at pH 11.

In one embodiment, the polylysine may specifically represent epsilon poly-L-lysine. The epsilon poly-L-lysine is a substance known to be safe for humans, such as being used as food preservatives for several years in the United States and Japan, and L-lysine, an essential amino acid produced by fermentation of bacteria. It is a linear polymer of about 3,000 to about 10,000 Daltons in which the alpha-carboxyl group and epsilon-amino group (ε-amino group) between lysine are linked by peptide bonding. Means ).

In one embodiment, when the cosmetic composition further includes the epsilon poly-L-lysine, since it is a naturally derived ingredient, it is possible to increase the preservation effect of the cosmetic composition by inhibiting the growth of microorganisms without exhibiting skin irritation.

In one embodiment, the epsilon poly-L-lysine may be included in an amount of about 0.01 to about 1 part by weight based on 100 parts by weight of the cosmetic composition. If the epsilon poly-L-lysine is contained in an amount of less than about 0.01 parts by weight, the microbial growth inhibitory effect may not be sufficiently exhibited, and if it exceeds about 1 part by weight, the unit cost of the cosmetic composition to be produced may be too high. Poly-L-lysine is preferably contained in an amount of about 0.01 to about 1 part by weight based on 100 parts by weight of the cosmetic composition.

In one embodiment, the cosmetic composition may further include glutathione. The glutathione is an antioxidant that plays an important role in the redox reaction in vivo, and refers to a tripeptide in which three amino acids of glutamic acid, cysteine, and glycine are bonded through a peptide bond. The glutathione chemically binds to the indole portion of melanin in the skin, thereby preventing repetitive polymerization of melanin, thereby inhibiting the formation of melanin. Accordingly, the cosmetic composition containing glutathione may exhibit an excellent skin whitening effect.

In one embodiment, the glutathione may be included in an amount of about 0.1 to about 3 parts by weight based on 100 parts by weight of the cosmetic composition. If the glutathione is included in an amount of less than about 0.1 parts by weight, the skin whitening effect may not be sufficiently exhibited, and when it is included in an amount exceeding about 3 parts by weight, mixing with other components may be inhibited.

In one embodiment, the cosmetic composition may minimize skin irritation that may occur when using a peel-off pack by additionally including noni fruit extract, mugwort extract, polylysine, and glutathione in parts by weight of the above-described range, It can show wrinkle improvement and skin whitening effect, and can exert the effect that it can be stored in a stable state for a long time.

In one embodiment, the cosmetic composition may further include a black willow bark extract. Black willow bark extract refers to extract from the bark of the black willow tree (Salix Nigra). The black willow tree grows wild in Mississippi Valley, Louisiana, and may also be called a black willow tree.

In one embodiment, the black willow bark extract may contain a large amount of salicylic acid (BHA), thereby effectively removing sebum and dead skin cells in skin pores. Specifically, as the salicylic acid is included, dead skin cells are removed from the skin, thereby improving the circulation of the skin turnover cycle, and helping to convert to a new skin layer.

In one embodiment, the black willow bark extract may be included in an amount of about 0.1 to about 3 parts by weight based on 100 parts by weight of the cosmetic composition. If the black willow bark extract is included in an amount of less than about 0.1 parts by weight, the exfoliating effect may not be sufficiently exerted, and when it is included in an amount exceeding about 3 parts by weight, skin irritation may increase.

In one embodiment, the cosmetic composition may further include a zwitterionic material. Since the Zwitter ionic material is a biocompatible material due to low protein adsorption, it may have characteristics of preventing inflammation and imparting stability to cells or pharmaceuticals when applied as a biomaterial. For example, the zwitterionic material may include at least one selected from the group consisting of phosphoryl choline, phosphoryl ethanolamine, phosphoryl serine, sulfobetaine, carboxybetaine, and combinations thereof. , Specifically, it may include phosphoryl ethanolamine.

In one embodiment, the zwitter ionic material may have a protein non-adsorption property, but is not limited thereto. For example, due to the protein non-adsorption property of the zwitter ionic material, the cosmetic composition containing the zwitter ionic material may have biocompatibility, and thus, when applied to the human body, side effects such as allergy may not be caused. I can.

In one embodiment, the zwitter ionic material may be included in an amount of about 0.01 to about 3 parts by weight based on 100 parts by weight of the cosmetic composition. If the zwitter ionic material is included in an amount of less than about 0.01 parts by weight, the biocompatibility effect may not be sufficiently exhibited, and when it is included in an amount exceeding about 3 parts by weight, mixing with other ingredients may be inhibited.

In one embodiment, the cosmetic composition, in addition to the above-described components, may further further include ingredients commonly required to prepare a cosmetic composition, but is not limited thereto.

In one embodiment, the cosmetic composition, as a carrier component, aliphatic alcohol sulfate, aliphatic alcohol ether sulfate, sulfosuccinic acid monoester, isethionate, imidazolinium derivative, methyltaurate, sarcosinate, fatty acid amide ether sulfate , Alkylamidobetaines, fatty alcohols, fatty acid glycerides, fatty acid diethanolamides, vegetable oils, lanolin derivatives or ethoxylated glycerol fatty acid esters, but are not limited thereto.

In one embodiment, the cosmetic composition may be added with a material arbitrarily selected according to the formulation or purpose of use of the cosmetic composition. For example, purified water, oil, surfactant, moisturizing agent, higher alcohol, thickening agent, chelating agent, colorant, fatty acid, antioxidant, preservative, wax, pH adjuster, fragrance, preservative, etc. may be added, but is not limited thereto. Does not. Parts by weight of additional components such as the preservative can be easily selected by a person skilled in the art within a range that does not impair the object and effect of the present invention. For example, about 0.001 to about 1 part by weight based on 100 parts by weight of the total cosmetic composition, Specifically, it may be included in an amount of about 0.01 to about 1 part by weight.

In one embodiment, the formulation of the cosmetic composition is preferably a peel-off pack formulation, and additionally, a skin, lotion, essence, cream, mist, sun cream, wash-off pack, soap, cleansing foam, mask pack, or mask sheet It can be prepared in a formulation containing. Compositions of these formulations can be prepared according to methods conventional in the art.

In one embodiment, when the formulation of the cosmetic composition is a paste, cream, or gel, as a carrier component, animal oil, vegetable oil, wax, paraffin, starch, tracant, cellulose derivative, polyethylene glycol, silicone, bentonite, silica, talc Or it may include zinc oxide, etc., but is not limited thereto.

In one embodiment, when the formulation of the cosmetic composition is a solution or emulsion, a solvent, a solubilizing agent or an emulsifying agent may be included as a carrier component, for example, isopropanol, ethyl carbonate, ethyl acetate, propylene glycol, 1,3-butyl glycol oil, glycerol aliphatic ester, polyethylene glycol, or fatty acid ester of sorbitan may be included, but is not limited thereto.

In one embodiment, when the formulation of the cosmetic composition is a suspension, as a carrier component, a liquid diluent such as water, ethanol or propylene glycol, ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester, and polyoxyethylene sorbitan ester A suspending agent such as, microcrystalline cellulose, aluminum metahydroxide, bentonite, agar, or tracant may be included, but is not limited thereto.

Hereinafter, the configuration of the present invention and effects thereof will be described in more detail through specific examples and comparative examples. However, the present examples are for explaining the present invention in more detail, and the scope of the present invention is not limited to these examples.

[Example 1]

The cosmetic composition of Example 1 was prepared according to the composition shown in Table 1 below. First, after heating the aqueous phase containing purified water to 80°C, polyvinyl alcohol and acrylate copolymer, which are film-forming agents, were added and mixed at a speed of 2,000 rpm using an azi mixer to form a gel-like composition. The gel composition was cooled to 45° C., and then potassium cocoyl glycinate and decyl glucoside, which were surfactants, were added and mixed at a speed of 1,000 rpm using an AGI MIXER. Then, ethanol as a solvent and 1,2-hexanediol as a preservative were added, mixed at a speed of 1,000 rpm using an azi mixer, and a defoaming process was performed. Then, finally, methylperfluoroisobutyl ether was added as a foaming agent and mixed at a speed of 1,000 rpm using an azi mixer to obtain a cosmetic composition, which was named Example 1.

[Example 2]

Prepared in the same manner as in Example 1 according to the components and contents shown in Table 1 below, but after mixing the blowing agent, Noni fruit extract, mugwort extract, epsilon poly-L-lysine, and glutathione were added, and then at 1,000 rpm. After further mixing for 15 minutes at a speed to obtain a cosmetic composition, this was named as Example 2.

[Example 3]

Prepared in the same manner as in Example 1 according to the components and contents shown in Table 1 below, but after mixing the foaming agent, Noni fruit extract, mugwort extract, black willow bark extract, epsilon poly-L-lysine, glutathione, and After adding phosphoryl ethanolamine, the mixture was further mixed for 15 minutes at a speed of 1,000 rpm to obtain a cosmetic composition, which was named Example 3.

Ingredients
(Based on 100 parts by weight of the total cosmetic composition) purpose Example 1 Example 2 Example 3 Purified water solvent 68.40 62.30 58.30 Polyvinyl alcohol Film forming agent 12.00 12.00 12.00 Acrylate copolymer Film forming agent 3.00 3.00 3.00 Potassium cocoyl glycinate Surfactants 1.00 1.00 1.00 Decylglucoside Surfactants 1.00 1.00 1.00 ethanol solvent 10.00 8.50 8.50 1,2-hexanediol Preservative 0.60 0.60 0.60 Methyl perfluoroisobutyl ether blowing agent 4.00 4.00 4.00 Noni Fruit Extract additive - 3.50 3.50 Mugwort extract additive - 1.25 1.25 Epsilon poly-L-lysine additive - 0.35 0.35 Glutathione additive - 2.50 2.50 Black Willow Bark Extract additive - - 2.75 Phosphoryl ethanolamine additive - - 1.25

[Comparative Example 1 and Comparative Example 2]

According to the components and contents shown in Table 2 below, a cosmetic composition was obtained by preparing in the same manner as in Example 1, and it was named Comparative Example 1 and Comparative Example 2.

Ingredients
(Based on 100 parts by weight of the total cosmetic composition) purpose Comparative Example 1 Comparative Example 2 Purified water solvent 74.40 70.40 Polyvinyl alcohol Film forming agent 12.00 12.00 Acrylate copolymer Film forming agent 3.00 3.00 ethanol solvent 10.00 10.00 1,2-hexanediol Preservative 0.60 0.60 Methyl perfluoroisobutyl ether blowing agent - 4.00

[Experimental Example 1: Drying time measurement experiment]

The drying time was measured after application of the cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 2. The measurement method is to pump the cosmetic composition contained in the pump container twice on the back of the hand, apply evenly, measure and compare the time to dry completely enough to peel off the product after application, and the results are shown in Table 3 below. Shown in.

division Drying time Example 1 19 minutes 35 seconds Example 2 15 minutes 01 seconds Example 3 10 minutes 12 seconds Comparative Example 1 40 minutes 23 seconds Comparative Example 2 34 minutes 31 seconds

As a result of the measurement, as shown in Table 3, in the case of the cosmetic compositions of Examples 1 to 3 according to the present invention, Comparative Example 1 not including both a surfactant and a foaming agent, and Comparative Example in which only a foaming agent was added without including a surfactant. It was confirmed that the drying time was shorter than that of the cosmetic composition of 2.

[Experimental Example 2: Comparative experiment of irritation]

When using the cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 2, irritation felt when removing the film was performed as a sensory evaluation. The experimental method is to first pump the cosmetic composition contained in the pump container twice on the back of the hand for 20 men and women in their 20s to 40s, apply evenly, confirm that they are completely dry, and then determine the irritation index felt when removing the film. The average value was given in a numerical value ranging from 1 to 10, and the results are shown in Table 4 below.

division Stimulation index Example 1 1.6 Example 2 1.4 Example 3 1.1 Comparative Example 1 7.2 Comparative Example 2 6.6

As a result of the measurement, as shown in Table 4, in the case of the cosmetic compositions of Examples 1 to 3 according to the present invention, Comparative Example 1 not including both a surfactant and a foaming agent, and Comparative Example in which only a foaming agent was added without including a surfactant. Compared to the cosmetic composition of 2, it was confirmed that the irritation index was markedly reduced.

[Experimental Example 3: Moisturizing power measurement experiment]

The moisturizing power was measured after use of the cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 2. For the measurement, the cosmetic composition was first applied to the back of the hand of an adult man and woman in their 20s to 40s, and then completely dried and then the film was removed, and then the moisture retention of the stratum corneum of the back of the hand was measured and evaluated. Moisture measurement was performed by measuring skin moisture levels immediately after removal of the film and from 1 hour to 4 hours to evaluate the moisturizing effect. As a measuring device, a'P-Sensor', a device of'A-One Smart Facial Recognition (BOMTECH)', was used, and the average value of the subject's moisture content (AU) is shown in Table 5 below.

division Moisture level (AU) Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 Immediately after removal of the film 46 52 56 41 42 1 hour later 42 49 51 38 38 2 hours later 38 47 49 34 35 4 hours later 34 38 41 28 31

As a result of the measurement, as shown in Table 5, it was found that the cosmetic compositions of Examples 1 to 3 according to the present invention have superior moisture retention compared to the cosmetic compositions of Comparative Examples 1 and 2.

[Experimental Example 4: Stability Evaluation]

Stability evaluation of the cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 2 was performed. In the stability evaluation, when the prepared cosmetic compositions were left at room temperature (25° C.) and above room temperature (50° C.) for 3 months, respectively, it was visually determined whether or not separation of components occurred. The criterion was described as'unstable' when the separation of the components occurred, and'stable' when the separation of the components did not occur. The stability evaluation results are shown in Table 6 below.

Temperature Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 25℃ stability stability stability stability stability 50℃ stability stability stability Instability Instability

As shown in Table 6, the cosmetic compositions of Examples 1 to 3 according to the present invention are at room temperature and above room temperature, unlike the cosmetic compositions of Comparative Examples 1 and 2 in which the separation phenomenon occurred when left for 3 months at a temperature of 50° Even during long-term storage, it was confirmed that it was stable without separation.

[Experimental Example 5: Measurement of anti-inflammatory effect]

The anti-inflammatory effects of the cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 2 were measured. First, macrophages (Raw 264.7 mouse cells) were dispensed into 96-well microplates by 4 × 10 ⁵ cells per well, and then the cosmetic composition of each of the Examples and Comparative Examples was added at a concentration of 1,000 μg/ml at 37° C. It was treated for 24 hours in _{CO 2 conditions.} After treatment, the supernatant was taken and the amount of TNF-α was measured by the sandwich ELISA method, and the results are shown in Table 7 below.

TNF-α assay division Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 TNF-α expression rate (%) 46.6 53.9 59.7 16.0 21.3

As shown in Table 7, the cosmetic compositions of Examples 1 to 3 according to the present invention exhibited a higher TNF-α induction effect compared to the cosmetic compositions of Comparative Examples 1 and 2.

In the present specification, only a few examples of various embodiments performed by the present inventors are described, but the technical spirit of the present invention is not limited thereto or is not limited thereto, and may be modified and variously implemented by those skilled in the art.

Claims (3)

As a cosmetic composition for a bubble peel-off type pack,
50 to 80 parts by weight of purified water based on 100 parts by weight of the cosmetic composition;
Methyl perfluoroisobutyl ether, methyl perfluorobutyl ether, ethyl perfluorobutyl ether, ethyl perfluoroisobutyl ether, tetrafluoropropene, trifluoropropyldimethicone, perfluorooctylt 1 to 10 parts by weight of a blowing agent containing at least one selected from the group consisting of lyethoxysilane, and combinations thereof;
A surfactant containing 0.1 to 10 parts by weight of decyl glucoside and 0.1 to 10 parts by weight of potassium cocoyl glycinate;
A film forming agent comprising 0.5 to 10 parts by weight of an acrylate copolymer and 5 to 15 parts by weight of polyvinyl alcohol;
Solvents 5 to 20 including those selected from the group consisting of ethanol, isopropyl alcohol, 1,3-butylene glycol, propylene glycol, propanediol, 1,2-hexanediol, and combinations thereof Parts by weight;
0.1 to 10 parts by weight of noni fruit extract;
0.1 to 3 parts by weight of mugwort extract;
0.01 to 1 part by weight of epsilon poly-L-lysine; And
0.1 to 3 parts by weight of glutathione;
Containing, a cosmetic composition for a bubble peel-off type pack.
The method of claim 1, wherein the cosmetic composition,
A cosmetic composition for a bubble peel-off type pack, characterized in that it can be dried and peeled off after forming a bubble when applied to the skin.
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