CN106333870B - A kind of exfoliating MASQUE APAISANT HYDRATANT and preparation method thereof - Google Patents
A kind of exfoliating MASQUE APAISANT HYDRATANT and preparation method thereof Download PDFInfo
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- CN106333870B CN106333870B CN201510397834.5A CN201510397834A CN106333870B CN 106333870 B CN106333870 B CN 106333870B CN 201510397834 A CN201510397834 A CN 201510397834A CN 106333870 B CN106333870 B CN 106333870B
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Abstract
The invention discloses a kind of exfoliating MASQUE APAISANT HYDRATANTs, the exfoliating MASQUE APAISANT HYDRATANT includes the component of following mass percent: crystallite ferment 0.01-5%, hyaluronic acid 0.01-10%, cosmetic 4.98%-35% and medical grade deionized water 50%-95%, the beneficial effects of the present invention are: the present invention uses the collective effect effect of crystallite ferment and hyaluronic acid, while exfoliating, sufficiently lock moisture, skin care, with good beauty, nutrition, moistening effect, the exquisiteness and Guan Run that skin can be felt after use reach the cosmetic result for improving skin quality.
Description
Technical field
The present invention relates to a kind of facial masks, and in particular to a kind of exfoliating MASQUE APAISANT HYDRATANT.
Background technique
Crystallite ferment is a kind of water-solubility protein extracted from hay bacillus, is the essence in protein.Subtract with potent
Except skin melanin, desalination and the formation for preventing melanin dramatically increase the insulation lock outlet capacity of skin, not for cutin metabolism
Good skin, protease can remove the dirt of skin surface and pore, sweat gland, leniently remove aging cutin, promote
Cell metabolism accelerates the microcirculation of capillary, enhances the attachment force of the collagen between cell, and skin is made to restore light
It is sliding fine and smooth；Grease extra on skin is decomposed, effectively cleaning skin, clogging of pores --- this is that lipase is most main for prevention
The function of wanting；And antioxidative enzyme can then inhibit free radical to oxidative damage caused by skin, the speed of delay skin aging,
It can be very helpful to the skin of existing aging phenomenon.
Hyaluronic acid is a kind of acid mucopolysaccharide, is shown in body with its unique molecular structure and physicochemical property more
The important physiological function of kind, such as lubricating joint adjust the permeability of vascular wall, regulatory protein matter, Water-Electrolyte diffusion and operating,
Promote wound healing etc..Particular, it is important that hyaluronic acid has special water retention, it is to be protected in presently found nature
Moist best substance, referred to as ideal natural moisturizing factor, it can improve skin-nourishing metabolism, make that skin is tender, light
It slides, goes wrinkle, increase elasticity, prevent aging, be good skin penetration enhancer again while moisturizing.With other nutritional ingredients
It is used cooperatively, the more preferable effect for promoting nutrient absorption can be played.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of safely and effectively small exfoliating MASQUE APAISANT HYDRATANT and its preparation side
Method effectively solves the problems, such as the skin such as face's moisturizing deficiency, and while exfoliating, sufficiently latching moisture, skin care have good
Beauty well, nutrition, moistening effect, can feel the exquisiteness and smoothness of skin after use, reach the cosmetic result for improving skin quality,
The product is easy to use, significant effect, securely and reliably.
To achieve the above object, the invention adopts the following technical scheme:
A kind of exfoliating MASQUE APAISANT HYDRATANT, it is characterised in that: the facial mask includes the component of following mass percent: crystallite ferment
0.01-5%, hyaluronic acid 0.01-10%, cosmetic 4.98%-35% and medical grade deionized water 50%-95%.
Further, the crystallite ferment by following weight percent component: crystallite ferment 1%.
Further, the hyaluronic acid by following weight percent component: hyaluronic acid 1%.
Further, the cosmetic includes poly- Nexbase 2004, the smooth olive oleate of sorb, stearic acid, spermaceti
Alcohol, dimethyl silicone polymer, ring five dimethyl silicone polymer, double-PEG-15 methyl ether dimethicones, 1,2- penta 2
Alcohol, ammonium acryloyl taurate/VP copolymer, Butyrospermum parkii fruit rouge, essence, hydrogenated olive oil acid ethylhexyl, EDTA
Disodium, lipoic acid, glycerol.
Further, which is grouped as by the group of following weight percent: crystallite ferment 1%, gathers hyaluronic acid 1%
The smooth olive oleate 3% of Nexbase 2004 3%, sorb, stearic acid 1.5%, cetanol 2%, dimethyl silicone polymer 1%, ring
Five dimethyl silicone polymers 2%, double-PEG-15 methyl ether dimethicones 5%, 1,2- pentanediol 3%, acryloyl diformazan
Base taurine ammonium/VP copolymer 0.4%, Butyrospermum parkii fruit rouge 3%, essence 0.15%, hydrogenated olive oil acid ethylhexyl 4%,
EDETATE SODIUM 0.1%, lipoic acid 1%, glycerol 5%, surplus are deionized water.
A kind of preparation method of exfoliating MASQUE APAISANT HYDRATANT, comprising the following steps:
1) hyaluronic acid is dissolved with medical grade deionized water, 70 DEG C is heated under stirring, continuing stirring makes
Bright matter acid can sufficiently dissolve, until forming clear, colorless viscous liquid, no gel bulk exists, spare；
2) crystallite ferment is dissolved with medical grade deionized water, the enabled sufficiently dissolution of stirring crystallite ferment maintains temperature not
More than 37 DEG C, until faint yellow micro- liquid of vicidity is formed, it is spare；
3) glycerol and EDETATE SODIUM are added into water under stirring, stirring is thermally formed Aqueous Phase Raw Material to transparent, standby
With；
4) poly- Nexbase 2004, the smooth olive oleate of sorb, stearic acid, cetanol, dimethyl silicone polymer, ring five are gathered
Dimethyl siloxane, double-PEG-15 methyl ether dimethicones, Butyrospermum parkii fruit rouge and hydrogenated olive oil acid ethylhexyl
Mixing is heated to 70 DEG C and is used as oily phase raw material, spare；
5) the oily phase raw material after heating is mixed with the Aqueous Phase Raw Material, acryloyldimethyl is added into it
Taurine ammonium/VP copolymer neutralizes, then the mixture of 1,2- pentanediol and lipoic acid is added into it, cold after the stirring of constant temperature homogeneous
But to 50 DEG C, deaerated under vacuum forms auxiliary material liquid, is cooled to 37 DEG C；
6) step mule 5 is added in the resulting solution of step 1) and the resulting solution of step 2) and essence simultaneously) resulting auxiliary material
In liquid, homogeneous stirring maintains vacuum outgas, continues to be cooled to 25 DEG C, discharge to get the original essence of exfoliating MASQUE APAISANT HYDRATANT
Magnificent liquid.
7) position relative to eye, nose, mouth is soaked in the original essence of facial mask equipped with the face paper of eyelet, nostril, nozzle aperture
In liquid, to its absorption；It is put into aluminium foil bag and encapsulates.
Further, step 1), 2), 5) in, the revolving speed of homogeneous stirring is not less than 3000rpm.
Further, in step 5) and step 6), the vacuum degree of the vacuum is -0.1MPa.
By adopting the above-described technical solution, the beneficial effect that the present invention obtains is:
1. exfoliating MASQUE APAISANT HYDRATANT provided by the present invention, while exfoliating, sufficiently latching moisture, skin care have
There are good beauty, nutrition, moistening effect, the exquisiteness and Guan Run of skin can be felt after use, reaches the beauty for improving skin quality
Effect.
2. the present invention is easy to use, i.e. the molding facial mask of patch i.e., effect can be quickly felt after use.
3. because exfoliating MASQUE APAISANT HYDRATANT does not contain any forbidden amphetamine (such as heavy metal, hormone, toxin, non-permitted chemicals
Matter etc.), so having no toxic side effect, being safe and reliable
7. the vacuum degree of vacuum is -0.1MPa in the preparation method of the exfoliating MASQUE APAISANT HYDRATANT, step 5) and step 6), most
Mitigate oxidation of the oxygen to active material to big degree.
Specific embodiment
Embodiment 1:
A kind of exfoliating MASQUE APAISANT HYDRATANT, the component including following weight percent: crystallite ferment 0.5%, hyaluronic acid
0.5%, the smooth olive oleate 3% of poly- Nexbase 2004 3%, sorb, stearic acid 1.5%, cetanol 2%, polydimethylsiloxanes
Alkane 1%, ring five dimethyl silicone polymer 2%, double-PEG-15 first
Base ether dimethyl silicone polymer 5%, 1,2- pentanediol 3%, ammonium acryloyl taurate/VP copolymer
0.4%, Butyrospermum parkii fruit rouge 3%, essence 0.15%, hydrogenated olive oil acid ethylhexyl 4%, EDETATE SODIUM 0.1%, lipoic acid
1%, glycerol 5%, surplus are deionized water.
Embodiment 2:
A kind of exfoliating MASQUE APAISANT HYDRATANT, the component including following weight percent: crystallite ferment 1%, hyaluronic acid 1%,
The smooth olive oleate 2.5% of poly- Nexbase 2004 2.5%, sorb, stearic acid 2.5%, cetanol 2%, dimethyl silicone polymer
0.5%, ring five dimethyl silicone polymer 1%, double-PEG-15 methyl ether dimethicones 3%, 1,2- pentanediol 4%, third
Alkene acyl dimethyltaurine ammonium/VP copolymer 0.5%, Butyrospermum parkii fruit rouge 5%, essence 0.15%, hydrogenated olive oil acid ethyl
Own ester 3%, EDETATE SODIUM 0.1%, lipoic acid 1%, glycerol 5%, surplus are deionized water.
Embodiment 3:
A kind of exfoliating MASQUE APAISANT HYDRATANT, the component including following weight percent: crystallite ferment 1.5%, hyaluronic acid
1.5%, the smooth olive oleate 1% of poly- Nexbase 2004 2%, sorb, stearic acid 2%, cetanol 2%, dimethyl silicone polymer
1.5%, ring five dimethyl silicone polymer 1.5%, double-PEG-15 methyl ether dimethicones 2%, 1,2- pentanediol 2%,
Ammonium acryloyl taurate/VP copolymer 0.5%, Butyrospermum parkii fruit rouge 2%, essence 0.15%, hydrogenated olive oil acid second
The own ester 2% of base, EDETATE SODIUM 0.1%, lipoic acid 1.5%, glycerol 5%, surplus are deionized water.
The preparation method of the exfoliating MASQUE APAISANT HYDRATANT, includes the following steps:
(1) hyaluronic acid is dissolved with medical grade deionized water, 70 DEG C is heated under stirring, continuing stirring makes
Bright matter acid can sufficiently dissolve, until forming clear, colorless viscous liquid, no gel bulk exists, spare；
(2) crystallite ferment is dissolved with medical grade deionized water, the enabled sufficiently dissolution of stirring crystallite ferment maintains temperature not
More than 37 DEG C, until faint yellow micro- liquid of vicidity is formed, it is spare；
(3) it is added glycerol and EDETATE SODIUM into water under stirring, stirring is thermally formed Aqueous Phase Raw Material to transparent,
It is spare；
(4) by poly- Nexbase 2004, the smooth olive oleate of sorb, stearic acid, cetanol, dimethyl silicone polymer, ring five
Dimethyl silicone polymer, double-PEG-15 methyl ether dimethicones, Butyrospermum parkii fruit rouge and hydrogenated olive oil acid ethyl hexyl
Ester mixing is heated to 70 DEG C and is used as oily phase raw material, spare；
(5) the oily phase raw material after heating is mixed with the Aqueous Phase Raw Material, acryloyl diformazan is added into it
Base taurine ammonium/VP copolymer neutralizes, then the mixture of 1,2- pentanediol and lipoic acid is added into it, after the stirring of constant temperature homogeneous
50 DEG C are cooled to, deaerated under vacuum forms auxiliary material liquid, is cooled to 37 DEG C；
(6) step mule 5 is added in the resulting solution of step 1) and the resulting solution of step 2) and essence simultaneously) resulting auxiliary material
In liquid, homogeneous stirring maintains vacuum outgas, continues to be cooled to 25 DEG C, discharge to get the original essence of exfoliating MASQUE APAISANT HYDRATANT
Magnificent liquid.
(7) position relative to eye, nose, mouth is soaked in the original essence of facial mask equipped with the face paper of eyelet, nostril, nozzle aperture
In liquid, to its absorption；It is put into aluminium foil bag and encapsulates.
Exfoliating MASQUE APAISANT HYDRATANT of the present invention should be stored in shady place, be avoided directly by sunlight or strong illumination, can
Stablize storage 2 years.
We have found during screening study, although the removal cutin that crystallite ferment can be mild, hyaluronic acid energy
Moisture is lockked, but frequently removes cutin, the cuticula of skin can be had damage, to generate skin irritatin discomfort or allergy
Feeling.But it has been surprisingly found that the formula using the application will not then generate above-mentioned phenomenon.It is our specific experiments below
Situation.
Reference examples 1:
A kind of exfoliating MASQUE APAISANT HYDRATANT, the component including following weight percent: crystallite ferment 1%, hyaluronic acid 1%,
The smooth olive oleate 2.5% of poly- Nexbase 2004 2.5%, sorb, stearic acid 2.5%, cetanol 2%, dimethyl silicone polymer
0.5%, 1,2- pentanediol 4%, ammonium acryloyl taurate/VP copolymer 0.5%, Butyrospermum parkii fruit rouge 5%, essence
0.15%, hydrogenated olive oil acid ethylhexyl 3%, EDETATE SODIUM 0.1%, lipoic acid 1%, glycerol 5%, surplus are deionization
Water.Preparation method is identical as embodiment 1-3.
Reference examples 2:
A kind of exfoliating MASQUE APAISANT HYDRATANT, the component including following weight percent: crystallite ferment 1%, hyaluronic acid 1%,
The smooth olive oleate 2.5% of poly- Nexbase 2004 2.5%, sorb, stearic acid 2.5%, cetanol 2%, dimethyl silicone polymer
0.5%, 3- aminopropyltriethoxy diethoxy silane 2%, 1,2- pentanediol 4%, ammonium acryloyl taurate/VP copolymer
0.5%, Butyrospermum parkii fruit rouge 5%, essence 0.15%, hydrogenated olive oil acid ethylhexyl 3%, EDETATE SODIUM 0.1%, lipoic acid
1%, glycerol 5%, surplus are deionized water.Preparation method is identical as embodiment 1-3.
Application Example 1
Research object: volunteer, 50.
Application method: every night using the facial mask once prepared by embodiment 1, is used continuously 8 weeks.
Experimental result: facial skin can be effectively cleaned, 98% people thinks no skin irritatin sense, and does not have skin mistake
Quick phenomenon.
Application Example 2
Research object: volunteer, 50.
Application method: every night using the facial mask once prepared by embodiment 2, is used continuously 8 weeks.Experimental result: energy
Enough effectively cleaning facial skins, 100% people thinks no skin irritatin sense, and does not have phenomena of cutaneous irritation.
Using reference examples 1
Research object: volunteer, 50.
Application method: every night using the facial mask once prepared by reference examples 1, is used continuously 8 weeks.Experimental result: energy
Enough effectively cleaning facial skins, 24% people thinks there is skin irritatin sense, and has 2 phenomena of cutaneous irritation occur.
Using reference examples 2
Research object: volunteer, 50.
Application method: every night using the facial mask once prepared by reference examples 2, is used continuously 8 weeks.Experimental result: energy
Enough effectively cleaning facial skins, 20% people thinks there is skin irritatin sense, but does not occur phenomena of cutaneous irritation.
Claims (7)
1. a kind of exfoliating MASQUE APAISANT HYDRATANT, it is characterised in that: the facial mask consists of the following components in percentage by mass: crystallite ferment
0.01-5%, hyaluronic acid 0.01-10%, cosmetic 4.98%-35% and medical grade deionized water 50%-95%；Institute
Stating cosmetic includes poly- Nexbase 2004, the smooth olive oleate of sorb, stearic acid, cetanol, dimethyl silicone polymer, ring
Five dimethyl silicone polymers, double-PEG-15 methyl ether dimethicones, 1,2- pentanediol, acryloyldimethyl taurine
Ammonium/VP copolymer, Butyrospermum parkii fruit rouge, essence, hydrogenated olive oil acid ethylhexyl, EDETATE SODIUM, lipoic acid and glycerol.
2. exfoliating MASQUE APAISANT HYDRATANT as described in claim 1, it is characterised in that: the mass percent of crystallite ferment is 1%.
3. exfoliating MASQUE APAISANT HYDRATANT as described in claim 1, it is characterised in that: the mass percent of hyaluronic acid is 1%.
4. exfoliating MASQUE APAISANT HYDRATANT as claimed in any one of claims 1-3, it is characterised in that: the exfoliating MASQUE APAISANT HYDRATANT by
The group of following weight percent is grouped as: crystallite ferment 1%, hyaluronic acid 1%, poly- Nexbase 2004 3%, the smooth olive oil of sorb
Acid esters 3%, stearic acid 1.5%, cetanol 2%, dimethyl silicone polymer 1%, ring five dimethyl silicone polymer 2%, double-PEG-
15 methyl ether dimethicones 5%, 1,2- pentanediol 3%, ammonium acryloyl taurate/VP copolymer 0.4%, ox
Oily fruit tree fruit rouge 3%, essence 0.15%, hydrogenated olive oil acid ethylhexyl 4%, EDETATE SODIUM 0.1%, lipoic acid 1%, glycerol
5%, surplus is deionized water.
5. a kind of preparation method of exfoliating MASQUE APAISANT HYDRATANT as described in claim 1, it is characterised in that: the following steps are included:
1) hyaluronic acid is dissolved with medical grade deionized water, 70 DEG C is heated under stirring, continuing stirring makes hyalomitome
Acid can sufficiently dissolve, until forming clear, colorless viscous liquid, no gel bulk exists, spare；
2) crystallite ferment is dissolved with medical grade deionized water, the enabled sufficiently dissolution of stirring crystallite ferment maintains temperature to be no more than
37 DEG C, until faint yellow micro- liquid of vicidity is formed, it is spare；
3) glycerol and EDETATE SODIUM are added into water under stirring, stirring is thermally formed Aqueous Phase Raw Material to transparent, spare；
4) by poly- Nexbase 2004, the smooth olive oleate of sorb, stearic acid, cetanol, dimethyl silicone polymer, the poly- diformazan of ring five
Radical siloxane, double-PEG-15 methyl ether dimethicones, Butyrospermum parkii fruit rouge and hydrogenated olive oil acid ethylhexyl are mixed
It closes, is heated to 70 DEG C and is used as oily phase raw material, it is spare；
5) the oily phase raw material after heating is mixed with the Aqueous Phase Raw Material, acryloyldimethyl ox sulphur is added into it
Sour ammonium/VP copolymer neutralizes, then the mixture of 1,2- pentanediol and lipoic acid is added into it, is cooled to after the stirring of constant temperature homogeneous
50 DEG C, deaerated under vacuum forms auxiliary material liquid, is cooled to 37 DEG C；
6) step mule 5 is added in the resulting solution of step 1) and the resulting solution of step 2) and essence simultaneously) in resulting auxiliary material liquid,
Homogeneous stirring, maintains vacuum outgas, continues to be cooled to 25 DEG C, discharge to get the original Essence of exfoliating MASQUE APAISANT HYDRATANT；
7) position relative to eye, nose, mouth is soaked in the original Essence of facial mask equipped with the face paper of eyelet, nostril, nozzle aperture,
To its absorption；It is put into aluminium foil bag and encapsulates.
6. preparation method as claimed in claim 5, it is characterised in that: in step 1), 2), 5) in, homogeneous stirring turns
Speed is not less than 3000rpm.
7. preparation method as claimed in claim 5, it is characterised in that: in step 5) and step 6), the vacuum of the vacuum
Degree is -0.1MPa.
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| CN107412102A (en) * | 2017-08-15 | 2017-12-01 | 广西民族大学 | A kind of exfoliating formula and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705392A (en) * | 2012-09-29 | 2014-04-09 | 黄兵 | Small nucleic acid whitening and freckle-removing cream, and preparation method thereof |
| CN104688615A (en) * | 2014-09-06 | 2015-06-10 | 杭州诺丽生物技术有限公司 | Enzyme facial mask essence with moisturizing and whitening functions |
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2015
- 2015-07-08 CN CN201510397834.5A patent/CN106333870B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705392A (en) * | 2012-09-29 | 2014-04-09 | 黄兵 | Small nucleic acid whitening and freckle-removing cream, and preparation method thereof |
| CN104688615A (en) * | 2014-09-06 | 2015-06-10 | 杭州诺丽生物技术有限公司 | Enzyme facial mask essence with moisturizing and whitening functions |
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