KR102221423B1 - Composition for inhibiting halitosis and enhancing oral hygiene - Google Patents

Abstract

The present invention relates to a mouthwash composition for inhibiting bad breath and improving oral hygiene which contains a Glycyrrhiza uralensis extract, an Angelica keiskei extract, or a Portulaca oleracea extract to inhibit the occurrence of bad breath, improves oral hygiene such as preventing oral diseases, is safe due to having no toxicity, has few side effects, and is easy to use by being discharged in a foam form. The mouthwash composition for inhibiting bad breath and improving oral hygiene of the present invention contains at least one of the Glycyrrhiza uralensis extract, the Angelica keiskei extract, or the Portulaca oleracea extract as an active component for inhibiting bad breath and improving oral hygiene.

Description

Composition for inhibiting halitosis and enhancing oral hygiene}

The present invention relates to an oral cleanser composition for suppressing bad breath and improving oral hygiene, and is prepared in a foam type for cleaning teeth, and contains a natural extract capable of suppressing bad breath to suppress bad breath and improve oral hygiene. It relates to the composition.

In general, bad breath is caused by an acquired systemic disease, or when proteins and food debris in saliva are decomposed by microorganisms in the oral cavity, and the resulting amino acids are decomposed by deoxidation enzymes or amino enzymes to create substances that cause odor. It is generated by In addition, when garlic or red pepper is consumed, bad breath is also caused by sulfides contained in these substances. The main components that cause bad breath are volatile sulfide compounds (VSC). These volatile sulfides include hydrogen sulfide (H2S), methyl mercaptan (CH3SH), and dimethyl mercaptan [(CH3)2S]. It is known to be the main component of bad breath during bad breath. In addition, in the case of fish, as the freshness of the fish decreases, the fishy smell of trimethylamine [(CH3)3N] or δ-aminovaleric acid is formed, and these volatile amine compounds, especially trimethylamine, are odor components. It constitutes a major part of. Other bad breath-causing substances include aldehydes, fatty acids, ammonia or pyridine.

As a method for removing such bad breath, a method of physically removing a substrate in the oral cavity through tooth brushing, flossing, and tongue brushing, and a method of chemically removing VSC using a mouthwash are most commonly used. Research on antimicrobial properties and functional materials using synthetic processing agents is being conducted to satisfy consumers' desire for functional materials, but this can cause environmental pollution problems and problems that can harm the human body.

On the other hand, in recent years, there is increasing interest in oral cleansers that are easy to use and have less time and place restrictions, and synthetic substances such as chlorhexidine, triclosan, and cetylpyridinium chloride are mainly used as antimicrobial substances in existing oral cleansers.

However, side effects caused by conventional oral cleansers may appear, and when used for a long time, there is a possibility that trace amounts may be ingested into the human body, and the possibility of negatively affecting the oral environment by causing changes in normal strains has been raised. Therefore, oral hygiene products using herbal medicines are being developed to develop more effective and less side effects oral cleansers.

In addition, in general, oral hygiene products used for cleaning the oral cavity and teeth are mainly distributed in the form of a paste, powder, gel, mucus, and liquid, and there are certain advantages and disadvantages in use and handling thereof. For example, a paste-like oral hygiene product has a high viscosity of the composition, a high possibility of causing damage to the tooth enamel layer by an abrasive component, and is not only inconvenient to squeeze out when using, and the product in the container cannot be completely used, so it can be used in a container that is discarded. There is a problem of causing environmental pollution due to the remaining amount remaining. In addition, the powdery form is inconvenient to use because particles are scattered during its use, and the gel form is not easily dispersed in the oral cavity due to low spreadability due to high viscosity. In addition, in the case of a liquid, it is widely used as an oral gargling agent because it has a disadvantage that it flows easily due to its low viscosity, but it cannot exert a sufficient effect of brushing teeth.

As a method to solve this problem, oral hygiene products that are discharged in the form of bubbles are being developed.

In general, the mouthwash composition may include a solubilizing agent, a wetting agent, a surfactant, a lubricant, a flavoring agent, a sweetening agent, an antiseptic agent, a medicinal agent, and the like. However, preservatives are not included in the present invention.

The solubilizing agent gives a refreshing feeling when used in a product and makes it possible to dissolve fragrances or preservatives that do not dissolve in water. Alcohols, polyoxypropylene copolymers, polyoxyethylene hydrogenated castor oil, higher alkyl acetates, and polyoxyethylene derivatives of sorbitan fatty esters can be listed. % By weight, preferably 5 to 20% by weight may be used.

The humectant plays a role in providing stability, sweetness, and slight viscosity of the product. Glycerin, sorbitol liquid, polyethylene glycol, etc., alone or in combination of two or more, are used in an amount of 20 to 60% by weight, preferably 20 to 50% by weight.

As a preservative, 0.05 to 0.25% by weight of methylparaben and propylparaben are used alone or in combination. The Korea Food and Drug Administration also restricts the amount of use, but when overexposed, the following side effects have been reported. Reacts with Asosan to irritate central nerve palsy, hemorrhagic gastritis, liver adverse effects, carcinogenicity, chromosomal abnormalities, eyes and skin mucous membranes. Parabens (methylparaben, ethylparaben, propylparaben, etc.)are widely used as cosmetic preservatives.When absorbed into the human body, they are known to cause endocrine disorders, skin aging, and breast cancer, and are classified as harmful substances.

As the pH adjuster, 0.02 to 1.5% by weight of phosphoric acid, sodium phosphate, citric acid, sodium citrate, succinic acid, sodium succinate, tartaric acid, sodium stannate, or the like is preferably used alone or in a mixture of two diacids.

The substances that make up perfume are aromatic substances used in ordinary toothpaste and substances used in food perfumes, such as peppermint oil, menthol, spearmint oil, carbon, anise oil, anitol, eucalyptus oil, clove oil. Type, eugenol, winter green oil type, methyl salicylate, cinnamon oil type, cinnamic aldehyde and other perfume ingredients are used, and the substance constituting the perfume is 0.1 to 2.0 weight by mixing one or two or more of the above ingredients %, preferably 0.5 to 1.5% by weight.

Sweeteners may be used to conquer the basic taste that may be possessed by the formulation of the toothpaste composition, and may play a role of sustaining the generation of saliva by providing taste while remaining in the oral cavity.

Patent Invention 001 relates to a composition for improving oral hygiene excellent in suppressing bad breath, and in more detail, a) xantorazole; b) milk bark extract, licorice acid, or a mixture thereof; And c) mokdan skin extract; And d) a composition for improving oral hygiene consisting of various formulations, such as chewing gum, dietary film, and mouth spray, using an oral disinfectant, an oral inflammation inhibitor, and a bad breath-causing substance removing agent, comprising a champignion extract. It is about.

Patent Invention 002 relates to a composition for enhancing oral hygiene containing a natural medicinal extract as an active ingredient, and more specifically, a natural medicinal extract selected from balsam and changija and a natural medicinal extract of golden/mokdan skin to cause bad breath and oral hygiene. It relates to a composition for improving oral hygiene containing as an active ingredient against infectious mucosal infections. The composition according to the present invention has excellent effects in preventing and treating periodontal diseases, preventing tooth decay and removing bad breath, as well as having natural antibiotic and antiseptic effects. More specifically, the composition according to the present invention has a synergistic effect of antibacterial activity against the bacteria causing bad breath and the bacteria causing mucosal infections in the oral cavity through proper mixing of the complex of substances derived from natural products that exhibit antibacterial and antifungal activity, and the effect of inhibiting plaque formation. And promotes the effect of alleviating gingivitis. In addition, by not using alcohol, not only prevents the cause of dry mouth, but also prevents oral mucosal infections (oral candidiasis) and texture inflammation, which frequently occur in infants and women.

Patent Invention 003, in the composition of the present invention, in a foam toothpaste composition containing a base agent, a solvent, a surfactant, a PH regulator, a sweetener, a preservative, a flavoring agent, a solubilizer, a tooth decay prevention agent, a gum disease prevention agent, a wetting agent, and purified water, The main component contains at least one selected from 0.05 to 0.5% by weight of polygamma-glutamic acid, 0.01 to 0.03% by weight of cetylpyridinium chloride (CPC), and 0.01 to 0.1% by weight of aminocaproic acid, and the solvent is 3 to 12% by weight of ethanol And, the surfactant contains 0.5 to 2.0% by weight of sodium lauryl sulfate, the pH adjusting agent contains 0.1 to 3.0% by weight of citric acid, and the sweetener 0.1 to 1.5% by weight of sodium saccharin, 1.0 to 5.0% by weight of xylitol %, and the preservative contains 0.1-0.3% by weight of methyl paraoxybenzoate, and the flavoring agent contains 0.1-2.0% by weight of peppermint oil, 0.1-2.0% by weight of spearmint oil, 0.1% by weight of aroma oil It contains at least one selected from ~2.0% by weight, 0.1 to 2.0% by weight of herbal oil, and 0.1 to 2.0% by weight of L-menthol, and the solubilizing agent is 0.1 to 1% by weight of polyoxyethylene, 0.1% by weight of polyoxyethylene hydrogenated castor oil It contains at least one selected from ~0.9% by weight, and the caries preventing agent contains at least one selected from 0.02 to 0.22% by weight of sodium fluoride and 0.2 to 0.76% by weight of sodium monofluorophosphate, and the gum disease preventer is allantoin chloro It contains 0.01 to 0.5% by weight of hydroxyaluminum, the wetting agent contains 1 to 10% by weight of sorbitol and 0.5 to 5% by weight of glycerin, and the purified water is characterized by containing the remaining weight% of the respective components. It relates to a foam toothpaste composition.

Patent Invention 004 relates to a toothpaste composition, which is a tooth cleaner, which is used in a foam form through a foam generating device, and includes sodium lauroyl sacosinate, a surfactant that acts as a foaming agent and a cleaning agent; Polyoxyethylene hydrogenated castor oil as an emulsifier; And polyoxyl hydrogenated castor oil, which is an emulsifier, and is stable under various storage conditions, and it relates to a safe toothpaste composition for cleaning toothpaste, characterized in that the foaming amount is suitable and the taste is good.

KR 10-0797975 B1 (registration date January 18, 2008) KR 10-1778058 B1 (Registration date September 7, 2017) KR 10-1448283 B1 (registration date September 30, 2014) KR 10-0772210 B1 (registration date October 25, 2007)

The present invention relates to an oral cleansing composition for suppressing bad breath and improving oral hygiene, and by containing licorice extract, fresh herb extract or portulaca oleracea extract, it is possible to suppress the occurrence of bad breath and improve oral hygiene such as oral disease prevention, and there is no toxicity. It is safe, has few side effects, and is discharged in the form of a foam, so it is easy to use, and to a mouthwash composition for suppressing bad breath and improving oral hygiene.

In order to achieve the above object, the oral hygiene composition for suppressing bad breath and improving oral hygiene of the present invention contains at least one of licorice extract, fresh herb extract, and portulaca oleracea extract as an active ingredient for suppressing bad breath and improving oral hygiene.

It additionally contains green tea extract, aloe extract, eucalyptus extract, and chamomile extract.

It further contains sodium fluoride, glycerin, sodium saccharin, allantoin, ethanol, combined mint flavor, xylitol, sodium cocoyl glutamate, phloxamer 407, HCO40, L-menthol and purified water.

The oral cleansing composition for suppressing bad breath and improving oral hygiene of the present invention as described above has the following effects.

By containing any one or more of licorice extract, fresh herb extract, and portulaca oleracea extract, not only removes bad breath by suppressing bad breath-causing components, but also provides an effect of treating and preventing oral diseases such as dental caries.

In addition, since it contains natural extracts and removes preservatives, side effects are small, and while being safe for the human body, it suppresses the growth of bacteria in the oral cavity, and provides excellent effects of reducing the occurrence of bad breath.

In addition, by being configured to be discharged in the form of a bubble, it can be used without a residual amount in the container, and it provides a convenient effect of use due to appropriate spreadability and flowability.

Hereinafter, in order to describe in detail enough that those of ordinary skill in the art can easily implement the present invention, the most preferred embodiment of the present invention will be described in detail. The reference numbers presented in the above embodiments are not limited to the presented numbers, and can be applied to other embodiments. It corresponds to an equal target for objects that exhibit the same purpose and effect as the configuration presented in the present embodiment.

The inventors of the present invention were experimenting with various natural extracts in order to prepare a mouthwash composition with excellent anti-malodorant effect, while licorice extract, fresh herb extract, and portulaca oleracea extract not only suppress the components that cause bad breath, but also improve oral health. The present invention was completed by confirming that there is a high antibacterial activity and a refreshing feeling by mixing the conductive materials used in the products in an appropriate amount.

Thus, a mouthwash composition of various composition ratios was prepared according to the ingredients and contents described below.

[Example 1-1] The present invention is an invention for an oral hygiene composition for suppressing bad breath and improving oral hygiene, and any one or more of licorice extract, fresh herb extract, and portulaca oleracea extract as an active ingredient for suppressing bad breath and improving oral hygiene Contains.

[Example 1-2] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, containing licorice extract as an active ingredient for suppressing bad breath and improving oral hygiene, The licorice extract is contained in the range of 0.3% by weight of the total composition weight.

[Example 1-3] The present invention relates to an oral cleanser composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, it contains fresh herb extract as an active ingredient for suppressing bad breath and improving oral hygiene.

[Example 1-4] The present invention relates to an oral hygiene composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, it contains a portulaca oleracea extract as an active ingredient for suppressing bad breath and improving oral hygiene.

[Example 1-5] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, licorice extract and fresh herb extract were used as active ingredients for suppressing bad breath and improving oral hygiene. Contains.

[Example 1-6] The present invention is an invention of an oral cleansing composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, licorice extract and portulaca oleracea extract were used as active ingredients for suppressing bad breath and improving oral hygiene. Contains.

[Example 1-7] The present invention is an invention of an oral cleansing composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, fresh herb extract and portulaca oleracea extract were used as active ingredients for suppressing bad breath and improving oral hygiene. Contains.

[Example 1-8] The present invention is an invention for a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, the licorice extract, the fresh herb extract and the portulaca oleracea extract are each of the total composition weight It contains in the range of 0.001 to 5.0% by weight.

[Example 1-9] The present invention is an invention for a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, the licorice extract, the fresh herb extract and the portulaca oleracea extract are each of the total composition weight It contains in the range of 0.01 to 1.0% by weight.

[Example 1-10] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, licorice extract, fresh herb extract and The portulaca oleracea extract contains 0.1% by weight, respectively, of the total weight of the composition.

The present invention relates to a mouthwash composition for suppressing bad breath and improving oral hygiene by reducing components causing bad breath in the oral cavity, as well as improving oral hygiene and inhibiting bad breath, which is convenient to use because it is discharged in the form of a foam.

The licorice extract, the fresh vinegar extract, and the portulaca oleracea extract are used to remove bad breath-causing substances.

Specifically, licorice (Glycyrrhiza uralensis Fisch, locorice) is a medicinal plant most widely used as a herbal ingredient in Korea, China, and Japan, and is a perennial herb of the legume family. The physiological activity of licorice has been reported to have antiallergic, antioxidant, antiulcer, antiviral and anticancer properties. Licorice hot water extract significantly reduced the size and pain of aphthous ulcers called tongue needles in the liver. Among the effective versions of licorice, glycyrrhizin, a triterpenoid saponin, is contained in the roots of licorice by 3~5%. Licorice contains a lot of flavonoid substances in addition to saponin. Of these, licoricidin and licorisoflvan A inhibit the growth of S. mutans and Streptococus sobrinus (S. sobrinus), which are the causative agents of dental caries, and Porphyromonas gingivalis (P. gingivalis), a periodontal pathogen. ) And Prevotella intermedia (P. intermedia).

Angelicakeiskei is a perennial herb belonging to the parsley family and is called Myungilyeop, Sinripcho, and Seonsangcho. In Japanese, it is written as “Ashidaba” or “Myeongilyeop”, and as the name suggests, the order cut out today will rise again tomorrow. In Korea, it was introduced around the end of the 70s, and now Jeju Island is harvesting large amounts of it. It has been used in the form of tea, raw juice, powder, etc. for the purpose of preventing various adult diseases such as high blood pressure, diabetes, liver disease, neuralgia, and arteriosclerosis. In addition, in animal models, gastric acid secretion suppression, tumor formation suppression, antithrombosis, histamine secretion suppression, vascular hypertension, and hypertension suppression activity were found.

Porulaca oleracea linne is a medicinal herb belonging to the family Purslane, whose leaf shape is similar to the incisors of horses, and the name of the medicinal material is similar to that of amaranth. It is also called'jangmyeongcho' because it is said to have longevity when eaten for a long time. It has been used as a medicinal material for a long time, and has been used as a variety of antidote in folk remedies, and in the Arabian Peninsula, it has been widely used as a medicine such as antiseptic, anti-scurvy, antispasmodic, inos, anthelmintic, and skin soothing. Active ingredients contained include L-noradrenaline, dopamine, dopa, organic, glutamic acid, aspartic acid, alanine, noradrenalin, flavonoids, coumarin, succinic acid, etc., and vitamin B1, B2, malic acid, linolenic acid, etc. It has been reported that ω-6 fatty acids are abundant in Machi. These machi-hyuns have proven anti-oxidation, anti-inflammatory, antipruritic, lipolysis, and wound healing effects.

On the other hand, each extract of licorice, fresh vinegar, and machi-hage can be extracted by a solvent extraction method known in the art, and as an extraction solvent, alcohol having 1 to 6 carbon atoms such as water, ethanol and methanol, acetone, ethyl acetate, Any one selected from organic solvents such as n-nucleic acid, diethyl ether, acetone, and benzene, or a mixed solvent thereof may be used.

In addition, in the oral cleansing composition excellent in the specific inhibitory effect of the present invention, it is preferable to contain all of the licorice extract, the fresh herb extract and the portulaca oleracea extract, and the licorice extract, the fresh herb extract and the portulaca oleracea extract are the total composition weight It is most preferred to contain each of the in the range of 0.001 to 5.0% by weight in consideration of the effect or stability of the formulation.

When each extract component is 0.001% by weight or less, it is difficult to show the medicinal effect, and when it is more than 5.0% by weight, a precipitate may occur or the color of the formulation solution may change, which is not preferable.

[Example 2-1] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, green tea extract, aloe extract, eucalyptus extract, and chamomile extract are additionally contained.

[Example 2-2] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 2-1, the green tea extract, the aloe extract, the eucalyptus extract, and the chamomile extract are all It contains in the range of 0.001% to 5.0% by weight, respectively, of the composition weight.

[Example 2-3] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 2-1, the green tea extract, the aloe extract, the eucalyptus extract, and the chamomile extract are all It contains in the range of 0.01% to 1.0% by weight, respectively, of the weight of the composition.

The green tea extract, the aloe extract, the eucalyptus extract, and the chamomile extract are active ingredients for suppressing oral bad breath and improving oral hygiene.Since it is a natural substance with little irritation, it has a soothing effect on the skin in the oral cavity and prevents infection, etc. do.

Specifically, green tea is manufactured without fermenting the leaves of the tea tree, and its origin is in the mountainous area of the border between Sichuan and Tibet in China. Young leaves picked from newly sprouted branches are used for tea making, and the picked leaves are immediately heated to destroy coral enzymes to maintain the green color and evaporate moisture. The main ingredients are caffeine (3%), tannin, theanine, sekisenol, vitamin C (150-500 mg), vitamins B1, B2, niacin, pentothenic acid, inositol, and rutin. In particular, green tea contains a lot of tannins called catechins, and when ingested, it acts as an antioxidant, prevents blood clots from forming, and has the effect of lowering cholesterol and blood sugar. In addition, it has the effect of preventing tooth decay.

Aloe is a perennial succulent plant of the genus Asparagus, Xantoloia family, Asphodelus subfamily, and is native to the Middle East and Africa. Aloe has anti-inflammatory and antibacterial properties, and has a calming effect. Aloe can be used by mixing the extract extracted with ethanol as a solvent with another preparation solvent. The main ingredient is an antorakinone pigment component that has strong pharmacological activity such as anti-inflammatory.

Eucalyptus is an evergreen arboreous tree of the dicotyledonous plant, the family of the Eucalyptus, and is native to Australia. Eucalyptus is used by extracting essential oil from leaves and twigs by steam distillation (a method of extracting oil from plants with water vapor and then cooling it with cooling water and condensing). It accounts for 85%, and is composed of monoterpene types such as α-pinene and limonene. It is effective in protecting against diseases and infections by strengthening immunity, and it is effective in respiratory system diseases such as cold, cough, phlegm, bronchitis, sore throat, sinusitis with expectorant, sterilization, antibacterial, and antiviral effect. It helps. In addition, it has an analgesic effect, so it is used to relieve rheumatism and muscle pain, and it is helpful when applied to areas with burns, wounds, inflammation, and infections.

Chamomile is a medicinal plant belonging to the Asteraceae family, and it is read as'chamomile' in German pronunciation and'chamomile' in English. It contains apigenin, which is known as an anticancer component, and like other flavonoid components, apigenin has the effect of removing free radicals and inhibiting inflammation. In addition, since chamomile contains glycine, it relieves pain such as muscle pain, and has bactericidal and soothing effects, so it has effects such as relief of pain such as stomatitis and sore throat, relaxation of tension, and nerve stabilization.

Each extract of green tea, aloe, eucalyptus, and chamomile can be extracted by a solvent extraction method known in the art, and as an extraction solvent, an alcohol having 1 to 6 carbon atoms such as water, ethanol and methanol, acetone, ethyl acetate Any one selected from organic solvents such as de, n-nucleic acid, diethyl ether, acetone, and benzene, or a mixed solvent thereof may be used.

In addition, in the oral cleansing composition excellent in specific inhibitory effect of the present invention, the green tea extract, the aloe extract, the eucalyptus extract and the chamomile extract are preferably contained in a range of 0.001 to 5.0% by weight, respectively, of the total composition weight, and , Licorice, Sinseoncho, Portulaca, green tea, eucalyptus, aloe, and chamomile extracts containing each in the range of 0.01 to 1.0% by weight of the total composition weight, it is most preferable when it shows an effect or considers the stability of the formulation.

When each extract component is 0.001% by weight or less, it is difficult to show the medicinal effect, and when it is more than 5.0% by weight, a precipitate may occur or the color of the formulation solution may change, which is not preferable.

[Example 3] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, sodium fluoride, glycerin, sodium saccharin, allantoin, ethanol, combined mint flavor, xylitol, coco It additionally contains sodium ilglutamate, phloxamer 407, HCO40, L-menthol and purified water.

[Example 4] The present invention is an invention of a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, 0.1% by weight of the licorice extract, 0.1% by weight of the fresh herb extract, 0.1% by weight of the portulaca oleracea extract %, green tea extract 0.01 to 0.1 wt%, aloe extract 0.01 to 0.1 wt%, eucalyptus extract 0.01 to 0.1 wt%, chamomile extract 0.01 to 0.1 wt%, sodium fluoride 0.1 to 0.2 wt%, glycerin 1 to 10 wt%, saccharin Sodium 0.07% by weight, allantoin 0.05% by weight, ethanol 1 to 5% by weight, combined mint flavor 0.1 to 0.5% by weight, xylitol 0.1 to 0.3% by weight, sodium cocoyl glutamate 0.1 to 0.3% by weight, phloxamer 407 1 to 3% by weight %, HCO40 0.2 to 0.4% by weight, L-menthol 0.1 to 0.3% by weight, and the remaining purified water.

[Example 5] The present invention is an invention for a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, the licorice extract 0.3% by weight, green tea extract 0.01 to 0.1% by weight, aloe extract 0.01 to 0.1% by weight, eucalyptus extract 0.01 to 0.1% by weight, chamomile extract 0.01 to 0.1% by weight, sodium fluoride 0.1 to 0.2% by weight, glycerin 1 to 10% by weight, sodium saccharin 0.07% by weight, allantoin 0.05% by weight, ethanol 1 to 5 Wt%, combined mint flavor 0.1 to 0.5 wt%, xylitol 0.1 to 0.3 wt%, sodium cocoyl glutamate 0.1 to 0.3 wt%, phloxamer 407 1 to 3 wt%, HCO40 0.2 to 0.4 wt%, L-menthol 0.1 to It contains 0.3% by weight and the rest of purified water.

[Example 6] The present invention is an invention for a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, the fresh vinegar extract 0.3% by weight, green tea extract 0.01 to 0.1% by weight, aloe extract 0.01 to 0.1% by weight, eucalyptus extract 0.01 to 0.1% by weight, chamomile extract 0.01 to 0.1% by weight, sodium fluoride 0.1 to 0.2% by weight, glycerin 1 to 10% by weight, sodium saccharin 0.07% by weight, allantoin 0.05% by weight, ethanol 1 to 5 Wt%, combined mint flavor 0.1 to 0.5 wt%, xylitol 0.1 to 0.3 wt%, sodium cocoyl glutamate 0.1 to 0.3 wt%, phloxamer 407 1 to 3 wt%, HCO40 0.2 to 0.4 wt%, L-menthol 0.1 to It contains 0.3% by weight and the rest of purified water.

[Example 7] The present invention is an invention for a mouthwash composition for suppressing bad breath and improving oral hygiene, and in Example 1-1, 0.3% by weight of the portulaca oleracea extract, 0.01 to 0.1% by weight of green tea extract, 0.01 to the aloe extract 0.1% by weight, eucalyptus extract 0.01 to 0.1% by weight, chamomile extract 0.01 to 0.1% by weight, sodium fluoride 0.1 to 0.2% by weight, glycerin 1 to 10% by weight, sodium saccharin 0.07% by weight, allantoin 0.05% by weight, ethanol 1 to 5 Wt%, combined mint flavor 0.1 to 0.5 wt%, xylitol 0.1 to 0.3 wt%, sodium cocoyl glutamate 0.1 to 0.3 wt%, phloxamer 407 1 to 3 wt%, HCO40 0.2 to 0.4 wt%, L-menthol 0.1 to It contains 0.3% by weight and the rest of purified water.

[Comparative Example 1] Sodium fluoride, glycerin, sodium saccharin, allantoin, ethanol, combined mint flavor, xylitol, sodium cocoyl glutamate, phloxamer 407 and the remaining purified water are contained, and the component content is as shown in Table 1 below.

[Comparative Example 2] Sodium fluoride, glycerin, sodium saccharin, allantoin, ethanol, combined mint flavor, xylitol, cocoyl glutamate sodium, phloxamer 407, green tea extract, aloe extract, eucalyptus extract, chamomile extract and the remaining purified water, The component content is as described in Table 1 below.

[Comparative Example 3] A commercially available mouthwash product from L company, and its composition is as shown in Table 1 below.

The ingredients and contents described in the Examples and Comparative Examples are summarized as shown in Table 1 below.

Ingredient name Example Comparative example 4 5 6 7 One 2 3 Sodium fluoride 0.1~0.2 0.1~0.2 0.1~0.2 0.1~0.2 0.1~0.2 0.1~0.2 0.01~0.2 Allantoin 0.05 0.05 0.05 0.05 0.05 0.05 0.01~0.1 glycerin 1-10 1-10 1-10 1-10 1-10 1-10 1-10 Sodium saccharin 0.07 0.07 0.07 0.07 0.07 0.07 0.01~0.1 ethanol 1-5 1-5 1-5 1-5 1-5 1-5 1-5 Combination Mint Scent 0.1~0.5 0.1~0.5 0.1~0.5 0.1~0.5 0.1~0.5 0.1~0.5 0.1~0.5 Xylitol 0.1~1 0.1~1 0.1~1 0.1~1 0.1~1 0.1~1 - Sodium Cocoyl Glutamate 0.1~0.3 0.1~0.3 0.1~0.3 0.1~0.3 0.1~0.3 0.1~0.3 - Flosamer 407 1~3 1~3 1~3 1~3 1~3 1~3 1~3 HCO40 0.2~0.4 0.2~0.4 0.2~0.4 0.2~0.4 L-menthol 0.1~0.3 0.1~0.3 0.1~0.3 0.1~0.3 Green tea extract 0.01~0.1 0.01~0.1 0.01~0.1 0.01~0.1 Aloe extract 0.01~0.1 0.01~0.1 0.01~0.1 0.01~0.1 Eucalyptus extract 0.01~0.1 0.01~0.1 0.01~0.1 0.01~0.1 Chamomile extract 0.01~0.1 0.01~0.1 0.01~0.1 0.01~0.1 Licorice extract 0.1 0.3 Fresh vinegar extract 0.1 0.3 Portion string extract 0.1 0.3 Sucralose 0.1~1 Sodium citrate hydrate 0.1~0.2 Citric acid hydrate 0.01~0.05 Erythritol 0.1~1 Bamboo salt 0.01~0.1 Cocamidopropylbetaine 0.1~0.5 Polyethylene glycol 300 0.1~0.5 Polyoxyethylstyrene hydrogenated castor oil 0.2~0.4 Other salt 0.01~0.1 Purified water to 100 to 100 to 100 to 100 to 100 to 100 to 100

(Unit:% by weight)

<Experimental Example> Measurement of bad breath removal effect

By preparing Examples 4 to 7 and Comparative Examples 1 to 3, the effect of inhibiting bad breath on the oral cleanser composition was measured as follows.

Prepare a 250ml plastic transparent container, put Methlmercaptan, Methylamine, and Ammonium hydroxide, which are components that cause bad breath, in each container, cover and seal a lid equipped with a detector tube, and measure with a GASTEC gas measuring instrument. Methl mercaptan 130±5ppm, Methylamine 90±2ppm, respectively. , Ammonium hydroxide 190±5ppm was set as the initial value.

After dividing the test group, the oral cleansing composition prepared in Examples 1 to 4 and Comparative Examples 1 to 3 was added to each 250 ml plastic transparent container, and then the bad breath-causing component was added to the container, and the lid was sealed with a detection tube. After curing for 30 minutes, the value measured by the GASTEC gas meter was used as the final value and compared with the initial value. The measurement results are as described in Table 2.

At this time, the usage of GASTEC gas meter is as follows.

1) Cut both ends of the detector tube for the odor component to be measured.

2) Insert the tube into the rubber inlet.

3) Pull the handle until it locks.

4) Wait for the sampling time to cure.

5) Wait for the required sampling time and read the measured value at the end of the color layer.

division Measured value of suppression of components that cause bad breath (ppm) Methyl mercaptan Methylamine Ammonium hydroxide blank 128 91 189 Example 1 53 42 73 Example 2 76 64 89 Example 3 87 52 102 Example 4 66 67 94 Comparative Example 1 101 81 155 Comparative Example 2 91 75 146 Comparative Example 3 86 72 137

When the halitosis inhibitory effect was observed compared to the initial value (blank) through the results shown in Table 2, the reduction rates for the components that cause bad breath, Methlmercaptan, Methylamine, and Ammonium hydroxide, are shown in Table 3.

division Inhibition rate (%) Methyl mercaptan Methylamine Ammonium hydroxide Example 1 59 53 62 Example 2 42 29 53 Example 3 33 42 46 Example 4 49 26 51 Comparative Example 1 22 10 18 Comparative Example 2 30 17 23 Comparative Example 3 34 20 28

As shown in Table 3 above, when comparing the difference between the licorice extract, fresh vinegar extract, and machisuki extract are all added and the licorice extract, fresh vinegar extract, and chinensis extract are contained in a single single type, licorice extract, It was confirmed that when fresh vinegar extract and portulaca oleracea extract were added together, bad breath could be more effectively suppressed.

The present invention is not limited thereto, and may be modified in various forms by those skilled in the art without departing from the spirit and scope of the following appended claims, and thus such modifications should be interpreted as being within the scope of the present invention. something to do.

Claims (3)

It contains all of licorice extract, fresh herb extract and portulaca oleracea extract as active ingredients for suppressing bad breath and improving oral hygiene,
It additionally contains green tea extract, aloe extract, eucalyptus extract and chamomile extract,
The licorice extract, fresh vinegar extract, and machisuki extract are contained in the range of 0.001 to 0.5% by weight, respectively, of the total weight of the composition,
The green tea extract, aloe extract, eucalyptus extract, and chamomile extract are contained in the range of 0.01 to 1.0% by weight, respectively, of the total composition weight.
delete The method of claim 1,
Sodium fluoride, glycerin, sodium saccharin, allantoin, ethanol, combined mint flavor, xylitol, sodium cocoyl glutamate, phloxamer 407, HCO40, L-menthol, and purified water. Cleaning agent composition.