KR102209425B1 - Method for manufacturing deodorant using multiple function water containing minerals and deodorant manufactured by the same - Google Patents

Abstract

The present invention relates to a method for manufacturing a deodorant using mineral-containing complex functional water to provide increased deodorization. According to the present invention, the method comprises the following steps: mixing and stirring a mixed mineral powder including a calcined pulverized product of zeolite, elvan stone, vermiculite, and water-soluble silicate, carbon fiber, transition metal materials, and a dispersant to prepare a first mixture; performing a calcination process to acquire a base powder from the first mixture; immersing the base powder in mineral-containing complex functional water; coating the immersion-treated base powder with a natural oil mixture including two or more of olive oil, jojoba oil, coconut oil, and shea butter oil; and impregnating the coated base powder with a complex natural extract including two or more extracts of a pomegranate extract, a lavender extract, a rosemary extract, and a jasmine extract.

Description

Method for manufacturing deodorant using multiple function water containing minerals and deodorant manufactured by the same}

The present invention relates to a method of manufacturing a deodorant using a mineral-containing complex functional water and a deodorant thereof, and the deodorizing power due to the synergistic effect of antibacterial, sterilizing and antioxidant effects, along with reinforcing antibacterial and sterilizing effects through far infrared radiation and generation of anions. It relates to a method of manufacturing a deodorant using a mineral-containing complex functional water for augmentation, and a deodorant prepared accordingly.

In general, when microorganisms and bacteria ingest and decompose sweat, sebum, and contaminants secreted from the human body, inflammation is caused by strong skin irritation, and bacteria such as Staphylococcus Aureus and Escherichia Coli Severe odors may be caused by the field, and bacteria may multiply in everyday items such as clothing, bedding, and shoes contaminated with the human body's secretions such as the above, thereby threatening health.

In addition, in the case of offices or houses, various microorganisms such as bacteria, fungi, pathogenic bacteria, fungi, etc. are rich in nutrients to be ingested in corners where humidity and temperature conditions are appropriate, or under closets, shoe racks, and beds. They breed and cause allergic diseases such as respiratory disease, itching, rash, or odor indoors.

Various organic or inorganic synthetic antibacterial deodorants have been manufactured to inhibit the proliferation of microorganisms as described above and to remove odors caused by microorganisms. A method for preparing an antibacterial agent by synthesizing such conventional chemicals is described in detail in Korean Patent Registration No. 10-1180117.

However, the antibacterial deodorant synthesized with the conventional chemicals may cause harmful side effects to the human body such as respiratory diseases, itchiness, rash, etc. due to the antibacterial deodorant released when stored in a closet, shoe rack, office, living room, etc. In the case of direct contact, there was a problem that could corrode the skin.

On the other hand, functional water is a term that refers to activated water in which water is subjected to a special treatment to have a specific function, in other words, it refers to water activated by electrolysis, magnetic treatment, ultrasonic treatment, or the like. Therefore, there are various types of functional water, such as electrolyzed water, magnetically treated water, electronic water, ultrasonically treated water, resonant magnetic field water, ore or mineral functional water, and in addition to these, ozone water, degassed water, far infrared water, ceramic water, high frequency, etc. Eggplant active water is known.

Among them, mineral functional water is water that has improved water quality by adding various kinds of minerals to living water, such as mineral water and naturally occurring mineral water, and is the optimal mineral depending on the use and addition of research results on natural mineral water. It is possible to add more, and the functionality is further enhanced.

In particular, various studies that can be effectively applied to remove odors by utilizing such functional water have been attempted.

The technical problem to be solved in the present invention is a method of manufacturing a deodorant using complex functional water containing minerals capable of enhancing antibacterial properties and removing odors while harmless to the human body because there is no side effect on respiratory diseases, skin troubles, etc. It is to provide a prepared deodorant.

The problem to be solved by the present invention is not limited to the problems mentioned above, and other problems that are not mentioned will be clearly understood by those skilled in the art from the following description.

A method for producing a deodorant using a mineral-containing complex functional water according to embodiments of the present invention to achieve the above object is a mixed mineral powder including a calcined pulverized product of zeolite, elvanite, vermiculite and water-soluble silicate, carbon fiber, transition metal Mixing the substance and the dispersant and then stirring to prepare a first mixture; Performing a firing process to obtain a base powder from the first mixture; Immersing the base powder using mineral-containing complex functional water; Coating the immersion-treated base powder using a natural oil mixture containing two or more oils of olive oil, jojoba oil, coconut oil, and shea butter oil; And impregnating the coated base powder using a complex natural extract comprising two or more extracts of pomegranate extract, lavender extract, rosemary extract, and jasmine extract, wherein the method for preparing the mineral-containing complex functional water Silver: performing a heating process after preparing a second mixture by mixing purified water, dry shell powder, peach tree, persimmon tree, dry plant powder including a pulverized product of citrus fruit and Japanese pepper, and alcohol; Preparing a third mixture by adding an organic acid or its alkali salt and deep sea water to the second mixture in which the heating process is performed, and then performing a low-temperature aging process; And separating and extracting an aqueous solution from the third mixture subjected to the low temperature aging process to obtain the mineral-containing complex functional water.

According to an embodiment, the first mixture is a mixture of zeolite, elvanite, vermiculite and water-soluble silicate calcined pulverized product in a weight ratio of 1:1:0.5 to 1:1 to 2, and 30 to 40% by weight of mixed mineral powder, carbon Transition metal materials 1 to 3 containing 5 to 10% by weight of fiber, at least one of Cu(II), Fe(II), Ag(II), Ni(II), Pt(II) and Pd(II) It can be prepared by mixing and stirring the weight% and the remaining dispersant.

According to an embodiment, the second mixture is 15 to 30% by weight of dry shell powder mixed with two or more pulverized products of shells of conch, oyster, cockle, abalone, and scallops, citrus tree, persimmon tree, citrus leaf, and pepper. The pulverized product may be prepared by mixing 10 to 25% by weight of dried plant powder, 10 to 20% by weight of alcohol, and remaining purified water in a weight ratio of 1:1:1 to 2:0.5 to 1, followed by stirring.

According to an embodiment, the heating process of the second mixture is performed for 60 to 180 minutes at a temperature of 80 to 100°C, and the third mixture is an organic acid or its organic acid per 100 parts by weight of the second mixture in which the heating process is performed. It can be prepared by adding and stirring 5 to 10 parts by weight of an alkali salt and 1 to 5 parts by weight of deep sea water.

According to an embodiment, the low-temperature aging process of the third mixture is performed for 24 to 36 hours at a temperature of 10 to 20°C, and the immersion treatment of the base powder is performed by immersing the base powder in the mineral-containing complex functional water. Then, it may include heating for 60 to 120 minutes at a temperature condition of 25 to 45 ℃.

According to an embodiment, in the coating treatment of the immersion-treated base powder, olive oil, jojoba oil, coconut oil and shea butter oil are 1:1 to 1.5:0.5 to 1:0.5 per 100 parts by weight of the immersion-treated base powder. It may be carried out using 100 to 200 parts by weight of a natural oil mixture mixed in a weight ratio of ~1.

According to an embodiment, in the impregnation treatment of the coated base powder, pomegranate extract, lavender extract, rosemary extract and jasmine extract per 100 parts by weight of the coated base powder are mixed in a weight ratio of 1:1:1:1 Mixing 25 to 50 parts by weight of the complex natural extract, and may include stirring for 60 to 90 minutes at a temperature of 50 to 70 ℃.

The deodorant according to the embodiments of the present invention for achieving the above object is manufactured by any one of the above methods.

According to embodiments of the present invention, as the mixed mineral powder of the calcined pulverized product of zeolite, elvanite, vermiculite, and water-soluble silicate and the base powder including carbon fiber are impregnated with a transition metal, the adsorption and deodorization power is further increased, and far-infrared radiation and anion Antibacterial and bactericidal action can be enhanced through outbreaks.

In addition, as the base powder absorbs mineral components, polyphenols, and useful components for antibacterial, sterilization and deodorization by immersion treatment using mineral-containing complex functional water, the odor components adsorbed to the base powder are continuously decomposed. It is possible, and the deodorizing power can be further increased due to the synergistic effect of antibacterial, sterilizing and antioxidant effects.

In addition, since the useful components of the mineral-containing complex functional water absorbed in the base powder can be continuously discharged in a small amount by the coating treatment through the natural oil mixture, the effect of the useful components of the mineral-containing complex functional water can be maintained for a long time.

In addition, through the impregnation treatment of the base powder using the complex natural extract, the effect of neutralizing the sensory neutralization or offsetting the odor by using a fragrant substance for the odor component can be strengthened, so that antibacterial and deodorizing performance can be further enhanced.

As a result, it is possible to provide a method of manufacturing a deodorant using complex functional water containing minerals capable of enhancing antibacterial properties and removing odors while being harmless to the human body because there is no side effect on respiratory diseases and skin troubles, and a deodorant manufactured using the same. I can.

1 is a flowchart illustrating a method of manufacturing a deodorant using a mineral-containing complex functional water according to embodiments of the present invention.
2 is a flowchart illustrating a method of manufacturing a mineral-containing complex functional water according to embodiments of the present invention

Advantages and features of the present invention, and a method of achieving them will become apparent with reference to the embodiments described below in detail together with the accompanying drawings. However, the present invention is not limited to the embodiments disclosed below, but may be implemented in various different forms, and only this embodiment allows the disclosure of the present invention to be complete, and common knowledge in the art It is provided to completely inform the scope of the invention to the possessor, and the invention is only defined by the scope of the claims. The same reference numerals refer to the same elements throughout the specification.

In the present specification, when a member is positioned “on” another member, this includes not only a case where a member is in contact with another member, but also a case where another member exists between the two members. In addition, in the present specification, when a certain part "includes" a certain component, it means that other components may be further included rather than excluding other components unless otherwise stated.

The terms "about", "substantially", and the like, as used throughout the specification of the present application, are used at or close to the numerical value when manufacturing and material tolerances specific to the stated meaning are presented, and the understanding of the present application To aid in, accurate or absolute figures are used to prevent unfair use of the stated disclosure by unscrupulous infringers.

Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings.

1 is a flowchart illustrating a method of manufacturing a deodorant using a mineral-containing complex functional water according to embodiments of the present invention.

Referring to FIG. 1, mixing and stirring the mixed mineral powder, carbon fiber, transition metal material, and dispersant to prepare a first mixture (S10), performing a firing process to obtain a base powder from the first mixture ( S20), immersing the base powder using mineral-containing complex functional water (S30), coating the immersion-treated base powder using a natural oil mixture (S40), and coating treatment using a complex natural extract It may include the step of impregnating the base powder (S50).

Specifically, a first mixture may be prepared by first mixing and then stirring the mixed mineral powder, carbon fiber, transition metal material, and dispersant (S10).

The mixed mineral powder is a mineral mineral containing a natural mineral component, and may include, for example, a calcined pulverized product of zeolite, elvanite, vermiculite, and water-soluble silicate.

Zeolite is a generic term for aluminum silicate hydrate minerals of alkali and alkaline earth metals, and has a molecular structure having porosity due to loose atomic bonds in a crystal structure, and has a property of adsorbing other particulate matter. It is a mineral that can be used as an adsorbent or as a molecular sieve that separates other particulate matter by using this property. In particular, it can be seen that zeolite is used as a filter material for a water softener because it has the property of absorbing metal ions and converting hard water into sweet water. Zeolite erupts in large amounts of minerals, and by using such properties, it can be seen that it is used as an additive for soil improvement, fertilizer and pesticide, and additive for livestock feed.

Elvan is a rock that is rich in minerals enough to be called a mysterious stone or weak stone, and is a rock belonging to quartz porphyry among igneous rocks. Elvan stone is mainly composed of silicic anhydride (SiO2) and aluminum oxide (Al2O3), and is characterized by containing ferric oxide (Fe2O3), which is essential for the human body and living cells. It contains 40 kinds of minerals and radiates far-infrared rays. It is known as a bio mineral, and it is known as a mineral that has a function of adsorption, mineral elution, ion exchange, harmful metal adsorption and decomposition, decomposition cause removal, and freshness maintenance function as a porous structure. Due to these functions and actions, it can be seen that elvan stone is used as an activating agent for water, a water purifying agent, a soil improving agent, a deodorant, a far-infrared radiation agent, and an environmental improving agent.

Vermiculite is a mineral belonging to the monoclinic system having the same crystal structure as mica, and is also called vermiculite. Vermiculite is grayish white or brown in color, easily decomposed by acid, has a high cation exchange capacity, and expands when heated. Vermiculite is easily decomposed by acid, is porous, and has good absorption capacity, so it is widely used as a heat-resistant material and soundproofing material (防音材).

Water-soluble silicate (sodium silicate, potassium silicate, etc.) is a cleaning agent based on pollution-free silica stone, which has self-cleaning ability to decompose organic substances in water. Water-soluble silicate has the property of emitting far-infrared rays, adsorbs, decomposes, and neutralizes pesticide components, contains essential trace elements, and plays a role in activating beneficial microorganisms.

The mixed mineral powder may be prepared by calcining zeolite, elvanite, vermiculite, and water-soluble silicate at a temperature of 800 to 960° C. for 20 to 30 minutes, and then pulverizing to have a particle size of 0.5 to 3 mm. If the particle size of the mixed mineral powder is less than 0.5 mm, the pulverization process becomes complicated and the process efficiency decreases. If the particle size exceeds 3 mm, the dispersibility may decrease, and the function as a carrier may be weakened.

According to an embodiment, the mixed mineral powder may be obtained by mixing the calcined pulverized product of zeolite, elvanite, vermiculite, and water-soluble silicate in a weight ratio of 1:1:0.5 to 1:1 to 2, through which the mixed mineral powders As a result, the effect of the deodorization function due to the generation of far-infrared rays and negative ions can be enhanced.

Carbon fibers are for far-infrared radiation and antibacterial effects, and may be pulverized to have a particle size of 0.5 to 1 mm.

For example, the carbon fiber may be prepared by mixing a trace amount of additives (antibacterial agent, mineral powder, etc.) to a thermosetting resin powder to prepare a raw material mixture, and forming the prepared raw material mixture into a fibrous form through a known method. Thermosetting resin powder is a carbon source of carbon fiber and is a raw material that is carbonized through a carbonization process and converted into activated carbon fiber. Although all of the conventional carbon compounds can be used, it may be preferable to use one capable of minimizing the stability of the process and the impurity content in the obtained carbon fiber. It does not deform even during sintering or carbonization, and exhibits a small content of impurities, and for example, a novolak-type phenol resin may be used. However, the present invention is not limited thereto, and various types of thermosetting resins may be used in addition to the novolak-type phenolic resin.

The transition metal material is for impregnating the transition metal into the porous material of the mixed mineral powder and carbon fiber during the preparation of the first mixture. For example, Cu(II), Fe(II), Ag(II), Ni(II), Pt( It may contain at least one of Ⅱ) and Pd(II). The mixed mineral powder and carbon fiber impregnated with the transition metal may further improve the deodorization performance due to the high oxidizing power of the transition metal. For effective impregnation of the transition metal, the first mixture may be stirred at a temperature of 40 to 50° C. for 1 hour or more.

The dispersant may be a water-soluble dispersant made of a water-soluble polymer. The dispersant is water, at least one of a hydrophilic alcohol-based solvent, an aldehyde-based solvent, an ester-based solvent and a ketone-based solvent, polyvinylpyrrolidone, polyvinyl alcohol, polyethylene glycol, polyethylene oxide, polyaspartic acid, alginic acid, Chitosan, hyaluronic acid, polyetherimide, and carboxymethyl cellulose may include at least one water-soluble polymer material.

According to one embodiment, the first mixture is a mixture of zeolite, elvanite, vermiculite and water-soluble silicate calcined pulverized product in a weight ratio of 1:1:0.5 to 1:1 to 2, and 30 to 40% by weight of mixed mineral powder, carbon fiber 5 to 10% by weight, 1 to 3 weight of a transition metal material including at least one of Cu(II), Fe(II), Ag(II), Ni(II), Pt(II), and Pd(II) % And the remaining dispersant may be mixed and then stirred. As the mixed mineral powder, carbon fiber, and transition metal material are mixed in a weight ratio within the above-described range, the above-described deodorizing effect may be further enhanced. For example, when each of the mineral powder, carbon fiber, and transition metal material is less than the lower limit, the respective effects are not sufficiently exhibited, and when the upper limit is exceeded, the cost may be excessively increased compared to the increase in the effect.

The firing process may be performed to obtain a base powder from the first mixture (S20).

According to an embodiment, the sintering process is agitated within 150 rpm for 2 to 4 hours at room temperature for stable chemical bonding of the mixture impregnated with the transition metal, and then solid-liquid separation and then at a temperature of 250 to 350°C for 2 to 3 hours. It can be carried out by heat treatment. Through this, a base powder including a mixture of a mixed mineral powder and carbon fibers impregnated with a transition metal can be obtained.

Then, the base powder may be immersed using the mineral-containing complex functional water (S30).

According to the concept of the present invention, the immersion treatment of the base powder using the mineral-containing complex functional water is absorbed into the base powder through impregnation or adsorption of the useful ingredients contained in the mineral-containing complex functional water, thereby antibacterial, sterilizing, antioxidant and deodorizing effects. It can be done to further strengthen. Hereinafter, a method of manufacturing the mineral-containing complex functional water will be described in detail with reference to FIG. 2.

2 is a flow chart illustrating a method of manufacturing a mineral-containing complex functional water according to embodiments of the present invention.

Referring to FIG. 2, a second mixture may be prepared by first mixing purified water, dried shell powder, dried plant powder, and alcohol, and then a heating process may be performed (S31).

The heating process of the second mixture may be performed, for example, at a temperature of 80 to 100° C. for 60 to 180 minutes. During heating of the second mixture, a mineral component may be extracted from the dry shell powder, and an active component such as a polyphenol-based compound may be extracted from the dried plant powder. When the heating temperature of the second mixture is less than 80° C., extraction efficiency decreases, and when it exceeds 100° C., deformation of the extracted components may occur.

In detail, the dried shell powder may be used by grinding and mixing one or two or more of all types of shells generated from animals forming shells. In general, the shell contains calcium carbonate (CaCO3) as the main component, and contains a small amount of calcium phosphate Ca3 (PO4)2] or magnesium carbonate (MgCO3), and the content ratio of inorganic matters varies depending on the species, but calcium carbonate is 89-99%, Calcium phosphate is 1 to 2%, and it is adhered to an organic substance peculiar to mollusks called conchiolin, and there are pigments and metal compounds in it, so that the unique color and pattern of the shell is displayed.

According to the embodiments of the present invention, the dry shell powder may be used as shells of various shellfish such as turban shell, oyster, cockle, abalone, and scallops, and preferably two kinds of shells of turban shell, oyster, cockle, abalone, and scallops The above pulverized material may be mixed and used. In addition, the dry shell powder may be pulverized to have a particle size of 100 to 250 μm after firing the shell from which foreign matter is removed at a high temperature (eg, a temperature of 1000 to 1200°C).

During the heating process of the second mixture, useful ingredients such as mineral components may be extracted from the dry shell powder, and such useful ingredients may have antibacterial and deodorizing effects. The particle size of the dried shell powder is for optimizing the extraction efficiency of the above-described useful components, and when the particle size exceeds 250 μm, the extraction efficiency decreases, and when the particle size is less than 100 μm, the pulverization process becomes complicated and process efficiency may decrease.

The dried plant powder is a pulverized product of a dried plant containing an active ingredient (e.g., a polyphenol compound) for antibacterial, sterilizing, antioxidant, and deodorizing, and may include, for example, a pulverized product of peach tree, persimmon tree, citrus leaf and Japanese pepper. I can.

Sophora japonica L. is a broad-leaved arboreous tree belonging to the legume family and is widely distributed in Korea, China, and Japan. The bark is gray or dark gray, and the inner bark is yellow with a peculiar smell, and the leaves grow alternately. It is known to be effective in strengthening blood pressure, preventing hypertension, and preventing hyperlipidemia as it contains lutein components in the flowers of the Japanese pica tree. It is known that the fruit of the peach tree is effective in improving liver function by lowering the heat of the liver, and it is known that the seeds of the peach tree have the effect of coagulating blood, so that when there is bleeding, the seeds are changed and drunk. In addition, it is known to be effective in preventing aging through the antioxidant function of polyphenols and the release of active oxygen because polyphenols are contained in much more than other food types.

Persimmon tree (Diospyros kaki Thunb) is mainly distributed in the sub-central region of Korea, and in addition to reproductive Shija, Shileaf, Shihwa, and corpse have been used as folk remedies for a long time. Among them, persimmon leaves are mainly used as tea, and it is recorded that Donguibogam is effective in preventing and treating vascular diseases, as well as purpura (vascular inflammation). Persimmon leaves contain various substances such as vitamin C, amino acids, nucleic acids, phenolic compounds, and free sugars. Flavonoids of persimmon leaves exist in the form of glycosides such as astragalin, a glycoside of kaempferol, and myricitrin, a glycoside of myricetin, and isoquercitrin. Persimmon leaves have a total phenolic compound content of 0.1 to 5.8%, which is higher than that of other plants, has excellent antioxidant and antibacterial properties, and is known to be involved in superoxide dismutase (SOD) activity.

Citrus peel is a tangerine peel and is known to contain vitamins and other nutrients. For example, citrus peel is known to contain pectin, flavonoids, alkaloids, hesperidin, and vitamins. These detoxification, lowering the blood cholesterol content, antibacterial, anti-inflammatory, as they show the efficacy of enhancing the immunity, their use is increasing.

Sancho (Zanthoxylum schinifolium) is warm in nature, it warms the inside, relieves pain by driving away cold energy and moisture, and has an insecticidal and detoxifying effect. Sancho contains 7% essential oils, among which geraniollimonene and cumic alcohol are included. Recently, it has been reported that essential oils extracted from Sancho tree seeds have local anesthetic and analgesic effects, and inhibit Escherichia coli, red lychee, aureus, diphtheria, Staphylococcus aureus, and dermatophytes through antibacterial action.

The dried plant powder is a mixture of dried organs (e.g., roots, branches, stems, leaves, or flowers) of citrus trees, persimmons, citrus leaves, and Japanese peppers, and pulverized to have a particle size of 0.1 to 1 cm. have. If the particle size of the dried plant powder is less than 0.1 cm, the pulverization process becomes complicated and process efficiency decreases, and if the particle size exceeds 1 cm, the extraction efficiency of useful components such as polyphenol compounds may decrease.

According to an embodiment, the dried plant powder may be prepared by mixing a pulverized product of peach tree, persimmon tree, citrus leaf and Japanese pepper in a weight ratio of 1:1:1 to 2:0.5 to 1, through which the dried plant powder The synergistic effect and extraction efficiency according to the interaction of the extracted active ingredients can be optimized.

Alcohol is to increase the extraction efficiency of the useful components extracted from the dried shell powder and dried plant powder, it is possible to use a low-cost alcohol of C1 to C4. For example, ethanol may be used as alcohol.

Meanwhile, purified water can be used as a solvent for effectively dissolving or dispersing each component.

According to an embodiment, the second mixture is 15 to 30% by weight of dry shell powder mixed with two or more pulverized products among the shells of conch, oyster, cockle, abalone, and scallops, pulverization of peach tree, persimmon tree, citrus leaf and pepper Water may be prepared by mixing 10 to 25% by weight of dried plant powder, 10 to 20% by weight of alcohol, and remaining purified water in a weight ratio of 1:1:1 to 2:0.5 to 1, followed by stirring. If the dry shell powder is less than 15% by weight, the content of the mineral component to be extracted is low, and if it exceeds 30% by weight, extraction efficiency may decrease. If the dry plant powder is less than 10% by weight, the content of the active ingredient to be extracted is small, and if it exceeds 25% by weight, extraction efficiency may be lowered. In addition, if the alcohol is less than 10% by weight, extraction efficiency may decrease, and if it exceeds 20% by weight, solubility may decrease.

After preparing a third mixture by adding an organic acid or its alkali salt and deep sea water to the second mixture in which the heating process has been performed, a low-temperature aging process may be performed (S32).

The organic acid or its alkali salt can be used as a natural antibacterial substance that inhibits the growth of bacteria in the third mixture while promoting secondary extraction of mineral components from the dried shell powder during the low temperature aging process.

The organic acid may be a mixture of two or more selected from acetic acid, citric acid, malic acid, lactic acid, and ascorbic acid. As the alkali salt, an alkali metal salt or an alkaline earth metal salt of the organic acid may be used. As an example, the alkali salt may include sodium salt, potassium salt, calcium salt, and the like of the organic acid.

Deep ocean water refers to seawater less than 200m from the surface of the seawater, and contains a lot of inorganic nutrients such as nitrogen, phosphorus, and silicic acid, which are necessary for plant growth because photosynthesis does not occur, and pollution by air or chemicals, E. coli or general bacteria It is not contaminated with the body, so it has excellent physical cleanliness, contains essential trace elements and various minerals in a good balance, and includes 4 major minerals (magnesium, calcium, potassium, sodium), zinc, selenium, manganese, etc. It is also known to have excellent immune function against various diseases caused by such as.

In addition, since deep ocean water does not contain phytoplankton that consumes nutrients in the deep sea where sunlight does not reach, it is rich in nutrients decomposed by bacteria, etc., and contains a large amount of minerals such as calcium and magnesium. It is known that since it is water with little change and stable low water temperature, its properties are stable and contains various mineral components in a balanced manner, and it has excellent scavenging effects on active oxygen due to the action of dissolved metal ions. have.

According to an embodiment, the third mixture may be prepared by adding and stirring 5 to 10 parts by weight of an organic acid or an alkali salt thereof and 1 to 5 parts by weight of deep sea water per 100 parts by weight of the second mixture in which the heating process is performed. If the organic acid or its alkali salt is less than 5 parts by weight, the extraction efficiency and antibacterial effect of the mineral component are reduced, and if it exceeds 10 parts by weight, the solubility may be reduced. In addition, when the number of deep ocean waters is less than 1 part by weight, its efficacy is insignificant, and when it exceeds 5 parts by weight, there is a problem that the cost increases compared to the synergistic effect.

The low-temperature aging process is for generating a synergistic effect due to the sufficient mixing of useful components in the third mixture and the interaction of each component therethrough, and may be performed at a temperature of 10 to 20° C. for 24 to 36 hours. If low-temperature aging proceeds for less than 24 hours, the ingredients in the third mixture may not be sufficiently mixed, so the efficacy of each ingredient may not be exhibited properly, and if it exceeds 36 hours, the aging has already been completed and the efficiency of work may decrease. .

A mineral-containing complex functional water may be obtained by separating and extracting the aqueous solution from the third mixture subjected to the low-temperature aging process (S33).

The separation and extraction method may use various known methods. For example, it is possible to obtain mineral-containing complex functional water by removing debris from the third mixture through filtration or centrifugation. The mineral-containing complex functional water obtained as described above may contain various useful components for antibacterial, sterilizing and deodorizing as well as mineral components and polyphenols components.

Referring back to FIG. 1, the immersion treatment of the base powder may include immersing the base powder in the mineral-containing complex functional water and then heating at a temperature of 25 to 45° C. for 60 to 120 minutes. If the immersion temperature is less than 25°C, absorption of the useful components contained in the mineral-containing complex functional water may not be sufficient. If the immersion temperature exceeds 45° C., it may be desirable to maintain the above range since there is a tendency to impair the stability of the absorbed mineral-containing complex functional water. If the immersion time is short (less than 60 minutes), the useful ingredients of the mineral-containing complex functional water tend not to be sufficiently absorbed into the base powder, and if the immersion time is longer than 120 minutes, the absorbed useful ingredients may be eluted again, making it difficult to expect a sufficient effect. .

The immersion-treated base powder may be dehydrated and blow dried, and the immersion, dehydration, and drying processes described above may be repeatedly performed a plurality of times.

Next, the base powder immersed using a natural oil mixture may be coated (S40).

The coating treatment of the base powder using a natural oil mixture may be performed to improve the dispersibility of the base powder while increasing the deodorizing and moisture-proof effect. As long as it can exert this effect, various natural oils can be selected and used regardless of the type. For example, the natural oil mixture may include two or more of olive oil, jojoba oil, coconut oil, and shea butter oil.

According to an embodiment, in the coating treatment of the immersion-treated base powder, olive oil, jojoba oil, coconut oil, and shea butter oil per 100 parts by weight of the immersion-treated base powder are 1:1 to 1.5:0.5 to 1:0.5 to 1 It may be carried out using 100 to 200 parts by weight of a natural oil mixture mixed in a weight ratio of.

For the coating treatment of the base powder, various known methods such as dipping method or spray spray method may be used. The surface of the base powder can be coated with a natural oil mixture through the coating treatment, and accordingly, the useful components of the mineral-containing complex functional water absorbed in the base powder can be continuously discharged in a certain amount, so that the mineral-containing complex functional water is useful. The effect of the ingredients can last for a long time.

Subsequently, the base powder coated with the composite natural extract may be impregnated (S50).

The impregnation treatment of the base powder using the complex natural extract may be performed for the effect of neutralizing the odor or neutralizing the odor by using a fragrant substance. For example, the complex natural extract includes two or more extracts of pomegranate extract, lavender extract, rosemary extract, and jasmine extract, and may be used in a liquid form.

According to an embodiment, the impregnation treatment of the base powder may be performed by mixing 25 to 50 parts by weight of the complex natural extract per 100 parts by weight of the coated base powder, and stirring for 60 to 90 minutes at a temperature of 50 to 70°C. Thereafter, the composite natural extract may be left for 2 to 3 hours at room temperature so that the base powder is completely impregnated. At this time, it may be preferable to use a composite natural extract in which a pomegranate extract, a lavender extract, a rosemary extract, and a jasmine extract are mixed in a weight ratio of 1:1:1:1.

Thus, the preparation of the deodorant using the mineral-containing complex functional water can be completed.

The thus prepared deodorant can be processed into a deodorant product through a series of known processes. For example, the deodorant prepared according to the embodiments of the present invention may be packaged in a solid powder form, processed in a filter form, or mixed with a binder and processed into a liquid form to be produced into various products having a deodorizing effect.

According to embodiments of the present invention, as the mixed mineral powder of the calcined pulverized product of zeolite, elvanite, vermiculite, and water-soluble silicate and the base powder including carbon fiber are impregnated with a transition metal, the adsorption and deodorization power is further increased, and far-infrared radiation and anion Antibacterial and bactericidal action can be enhanced through outbreaks.

In addition, as the base powder absorbs mineral components, polyphenols, and useful components for antibacterial, sterilization and deodorization by immersion treatment using mineral-containing complex functional water, the odor components adsorbed to the base powder are continuously decomposed. It is possible, and the deodorizing power can be further increased due to the synergistic effect of antibacterial, sterilizing and antioxidant effects.

In addition, since the useful components of the mineral-containing complex functional water absorbed in the base powder can be continuously discharged in a small amount by the coating treatment through the natural oil mixture, the effect of the useful components of the mineral-containing complex functional water can be maintained for a long time.

In addition, through the impregnation treatment of the base powder using the complex natural extract, the effect of neutralizing the sensory neutralization or offsetting the odor by using a fragrant substance for the odor component can be strengthened, so that antibacterial and deodorizing performance can be further enhanced.

As a result, it is possible to provide a method of manufacturing a deodorant using complex functional water containing minerals capable of enhancing antibacterial properties and removing odors while being harmless to the human body because there is no side effect on respiratory diseases and skin troubles, and a deodorant manufactured using the same. I can.

Hereinafter, the present invention will be described in detail through examples.

[Example 1]

Zeolite, elvanite, vermiculite, and water-soluble silicate were each mixed in a weight ratio of 1:1:0.5:1, fired at a temperature of about 900°C for 30 minutes, and then pulverized to have an average particle size of 1.5mm to prepare a mixed mineral powder. . 30 parts by weight of the mixed mineral powder thus prepared and 5 parts by weight of carbon fiber pulverized to a particle size of about 1 mm were mixed with a solution in which 1 part by weight of polyvinylpyrrolidone, a water-soluble dispersant was added to DIW, a water-soluble solvent, and then Cu A transition metal material including (II) and Ag(II) was added in an amount of 1 part by weight, and stirred at a temperature of about 50° C. for 1 hour to prepare a first mixture.

Thereafter, at room temperature, the first mixture was stirred at 100 rpm for 2 hours, and after solid-liquid separation, calcined treatment was performed at a temperature of about 300° C. for 2 hours to obtain a base powder.

Subsequently, after mixing the mineral-containing complex functional water and the base powder prepared according to the embodiments of the present invention, the mixture was heated at a temperature of 40° C. for 90 minutes. At this time, the mineral-containing complex functional water was prepared as follows.

Drying of 15% by weight of dried shell powder including pulverized conch, oyster and abalone shells crushed to a particle size of about 150 μm, mixed with a weight ratio of 1:1:1:0.5 A second mixture was prepared by mixing 10 parts by weight of dry plant powder, 10 parts by weight of ethanol, and remaining purified water including the pulverized material of the engine, and heated at a temperature of about 100° C. for 120 minutes. Thereafter, 5 parts by weight of acetic acid and 1 part by weight of deep sea water per 100 parts by weight of the second mixture subjected to the heating process were added and stirred to prepare a third mixture, followed by aging at a temperature of about 18° C. for 48 hours, and the separation process The mineral-containing complex functional water was obtained through

After drying the immersion-treated base powder as described above, the surface of the base powder was coated by immersion in a natural oil mixture in which olive oil, jojoba oil, coconut oil, and shea butter oil were mixed. At this time, the natural oil mixture was 200 parts by weight of a natural oil mixture in which olive oil, jojoba oil, coconut oil, and shea butter oil were mixed in a weight ratio of 1:1:0.5:0.5 per 100 parts by weight of the immersion-treated base powder. .

Thereafter, 50 parts by weight of a complex natural extract in which pomegranate extract, lavender extract, rosemary extract and jasmine extract are mixed in a weight ratio of 1:1:1:1 are mixed with 100 parts by weight of the coated base powder, and this is at a temperature of 70°C. Stir for 90 minutes at. After that, it was left again at room temperature for 3 hours to complete the preparation of the deodorant.

[Example 2]

In Example 1, a deodorant was prepared in the same manner, except that the first mixture used 40 parts by weight of mixed mineral powder, 10 parts by weight of carbon fiber, and 3 parts by weight of a transition metal material.

[Example 3]

In Example 1, a second mixture was prepared using 30 parts by weight of dry shell powder, 25 parts by weight of dried plant powder, 20 parts by weight of ethanol, and the remaining purified water with mineral-containing complex functional water, and the second heating process was performed. A deodorant was prepared in the same manner, except that the third mixture was prepared using 10 parts by weight of acetic acid and 5 parts by weight of deep sea water per 100 parts by weight of the mixture.

[Comparative Example 1]

In Example 1, using only the mixed mineral powder prepared by mixing the base powder with zeolite and elvan stone at a 1:1 weight ratio, firing at a temperature of about 900°C for 30 minutes, and pulverizing to have an average particle size of 1.5 mm ( That is, a deodorant was prepared in the same manner, except for the addition of carbon fiber and transition metal material, omitting the stirring and firing process).

[Comparative Example 2]

In Example 1, a deodorant was prepared in the same manner, except that immersion treatment using mineral-containing complex functional water was not performed.

[Comparative Example 3]

In Example 1, a deodorant was prepared in the same manner, except that the impregnation treatment using the complex natural extract was not performed.

[Experimental Example 1] Deodorizing power measurement

The deodorizing agent of Example 1 was subjected to a deodorizing power test. The deodorizing power test was requested to the Korea Institute of Construction Living Environment Test on August 10, 2020 to investigate the deodorizing power of ammonia, trimethylamine, hydrogen sulfide and methyl mercaptan, and results having a deodorizing effect were obtained as shown in Table 1 below. At this time, the deodorizing power test was conducted under the condition of a sample amount of 10 mL in 1 L of a deodorizing container.

Test Items
(Concentration reduction rate) Test result
(%) Test Methods Remark ammonia 97.5 EL608:2017 (21±0.8)℃
(50.0 ± 1.0)% RH Trimethylamine 98.8 EL608:2017 Hydrogen sulfide 99.8 EL608:2017 Methylmercaptan 98.8 EL608:2017

[Experimental Example 2] Sensory test

A sensory test was performed on the deodorants of the Examples and Comparative Examples. In the sensory test, the deodorant of Examples and Comparative Examples is put in a sealed storage together with a substance generating odor, and taken out after a predetermined time, and 20 adults are selected to determine the odor intensity of the odor of the substance taken out through the sense of smell. It proceeded in a way of measuring. The evaluation is made with a full score of 5 points, but a score closer to 5 points means that the degree of odor is weak (that is, shows an excellent deodorizing effect), and the average value is shown in Table 2 below.

division Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 Comparative Example 2 score 3.7 4.1 3.9 2.9 3.2 3.4

As can be seen from Table 2, in the case of Examples 1 to 3 of the present invention, it can be seen that the deodorizing effect is superior compared to Comparative Examples 1 to 3. Through this, it can be predicted that the base powder according to the embodiments of the present invention, the immersion treatment using the mineral-containing complex functional water, and the impregnation treatment using the complex natural extract have the effect of enhancing the deodorization function. .

In the above, embodiments of the present invention have been described with reference to the accompanying drawings, but those of ordinary skill in the art to which the present invention pertains to implement the present invention in other specific forms without changing the technical spirit or essential features. You can understand that it can be. Therefore, it should be understood that the above-described embodiments and application examples are illustrative in all respects and are not limiting.

Claims (8)

Mixing and stirring the mixed mineral powder including the calcined pulverized product of zeolite, elvanite, vermiculite and water-soluble silicate, carbon fiber, transition metal material, and dispersant to prepare a first mixture;
Performing a firing process to obtain a base powder from the first mixture;
Immersing the base powder using mineral-containing complex functional water;
Coating the immersion-treated base powder using a natural oil mixture containing two or more oils of olive oil, jojoba oil, coconut oil, and shea butter oil; And
Including the step of impregnating the coated base powder using a complex natural extract containing two or more extracts of pomegranate extract, lavender extract, rosemary extract and jasmine extract,
The method for preparing the mineral-containing complex functional water:
Performing a heating process after preparing a second mixture by mixing purified water, dry shell powder, dried plant powder including pulverized products of peach tree, persimmon tree, citrus leaf and Japanese pepper, and alcohol;
Preparing a third mixture by adding an organic acid or its alkali salt and deep sea water to the second mixture in which the heating process is performed, and then performing a low-temperature aging process; And
A method for producing a deodorant using a mineral-containing complex functional water comprising the step of separating and extracting an aqueous solution from the third mixture subjected to the low-temperature aging process to obtain the mineral-containing complex functional water. The method of claim 1,
The first mixture is a mixed mineral powder in which the calcined pulverized product of zeolite, elvan stone, vermiculite, and water-soluble silicate is mixed in a weight ratio of 1:1:0.5 to 1:1 to 2, and 5 to 10% by weight of carbon fiber , Cu(II), Fe(II), Ag(II), Ni(II), Pt(II) and Pd(II) 1 to 3% by weight of a transition metal material containing at least one of Pd(II) and the remaining dispersant Method for producing a deodorant using a mineral-containing complex functional water prepared by mixing and then stirring. The method of claim 1,
The second mixture contains 15 to 30% by weight of dry shell powder mixed with two or more pulverized products among the shells of conch, oyster, cockle, abalone, and scallops, and pulverized products of peach tree, persimmon tree, citrus leaf and pepper Method for producing a deodorant using mineral-containing complex functional water prepared by mixing and stirring after mixing 10 to 25% by weight of dried plant powder, 10 to 20% by weight of alcohol and remaining purified water mixed in a weight ratio of :1 to 2: 0.5 to 1 . The method of claim 3,
The heating process of the second mixture is performed at a temperature of 80 to 100° C. for 60 to 180 minutes,
The third mixture is a deodorant using a mineral-containing complex functional water prepared by adding and stirring 5 to 10 parts by weight of an organic acid or an alkali salt thereof per 100 parts by weight of the second mixture in which the heating process is performed and 1 to 5 parts by weight of deep sea water. Manufacturing method. The method of claim 4,
The low-temperature aging process of the third mixture is performed at a temperature of 10 to 20°C for 24 to 36 hours,
The immersion treatment of the base powder comprises immersing the base powder in the mineral-containing complex functional water, and then heating the base powder at a temperature condition of 25 to 45° C. for 60 to 120 minutes. . The method of claim 1,
In the coating treatment of the immersion-treated base powder, olive oil, jojoba oil, coconut oil, and shea butter oil per 100 parts by weight of the immersion-treated base powder are mixed in a weight ratio of 1:1 to 1.5:0.5 to 1:0.5 to 1 Method for producing a deodorant using a mineral-containing complex functional water performed using 100 to 200 parts by weight of the natural oil mixture. The method of claim 6,
The impregnation treatment of the coated base powder is 25 to 50 composite natural extracts in which pomegranate extract, lavender extract, rosemary extract and jasmine extract are mixed in a weight ratio of 1:1:1:1 per 100 parts by weight of the coated base powder Mixing parts by weight, and a method for producing a deodorant using a mineral-containing complex functional water comprising stirring for 60 to 90 minutes at a temperature of 50 to 70 ℃. Deodorant prepared by using the method of any one of claims 1 to 7.

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