KR102189390B1 - 그리냐르 커플링 반응에서 높은 선택성을 갖는 다이알킬-, 다이아릴- 및 알킬아릴-다이할로실란의 제조 방법 - Google Patents

그리냐르 커플링 반응에서 높은 선택성을 갖는 다이알킬-, 다이아릴- 및 알킬아릴-다이할로실란의 제조 방법 Download PDF

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KR102189390B1
KR102189390B1 KR1020157029859A KR20157029859A KR102189390B1 KR 102189390 B1 KR102189390 B1 KR 102189390B1 KR 1020157029859 A KR1020157029859 A KR 1020157029859A KR 20157029859 A KR20157029859 A KR 20157029859A KR 102189390 B1 KR102189390 B1 KR 102189390B1
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South Korea
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reactor
stream
alkyl
grignard
aryl
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KR1020157029859A
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Korean (ko)
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KR20150131352A (ko
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제임스 리
빈 탄 응우옌
스콧 이. 피더
스티븐 엘. 움프리
한 쉬안 보
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다우 실리콘즈 코포레이션
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/125—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving both Si-C and Si-halogen linkages, the Si-C and Si-halogen linkages can be to the same or to different Si atoms, e.g. redistribution reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/122—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-C linkages

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020157029859A 2013-03-15 2014-03-14 그리냐르 커플링 반응에서 높은 선택성을 갖는 다이알킬-, 다이아릴- 및 알킬아릴-다이할로실란의 제조 방법 KR102189390B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361786750P 2013-03-15 2013-03-15
US61/786,750 2013-03-15
PCT/US2014/027339 WO2014152436A1 (en) 2013-03-15 2014-03-14 A method of preparing dialkyl-diaryl-, and alkylaryl-dihalosilanes with high selectivity in a grignard coupling reaction

Publications (2)

Publication Number Publication Date
KR20150131352A KR20150131352A (ko) 2015-11-24
KR102189390B1 true KR102189390B1 (ko) 2020-12-11

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KR1020157029859A KR102189390B1 (ko) 2013-03-15 2014-03-14 그리냐르 커플링 반응에서 높은 선택성을 갖는 다이알킬-, 다이아릴- 및 알킬아릴-다이할로실란의 제조 방법

Country Status (6)

Country Link
US (1) US9828394B2 (ja)
EP (1) EP2970343B1 (ja)
JP (1) JP6338651B2 (ja)
KR (1) KR102189390B1 (ja)
CN (1) CN105164140B (ja)
WO (1) WO2014152436A1 (ja)

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5206402A (en) * 1992-09-17 1993-04-27 Dow Corning Corporation Process for preparation of Ω-alkenylchlorosilanes
EP0767771B2 (en) * 1994-06-30 2004-05-06 The Dow Chemical Company Chlorohydrin process
US5430168A (en) 1994-10-27 1995-07-04 Dow Corning Corporation Alumimum trichloride catalyzed hydrogenation of high-boiling residue from direct process
WO2003059966A1 (en) 2002-01-03 2003-07-24 Bp Corporation North America Inc. Gas phase olefin polymerizations using dual donor catalyst systems
US7084206B2 (en) * 2002-04-04 2006-08-01 Dow Corning Corporation Process for preparing phenylorganosilicon intermediates
US6541651B1 (en) 2002-04-04 2003-04-01 Dow Corning Corporation Process for chlorosilane intermediates manufacture
CN1281612C (zh) * 2004-11-16 2006-10-25 浙江大学 一种CH3SiCl3转化反应的组合方法
WO2006083665A1 (en) * 2005-02-01 2006-08-10 Dow Corning Corporation Method of making phenyl-containing chlorosilanes with aliphatic or cycloparaffinic hydrocarbon solvents
EP2606053A1 (en) * 2010-08-18 2013-06-26 Momentive Performance Materials Inc. Solventless process to produce aromatic group-containing organosilanes
CN102225949A (zh) * 2011-05-23 2011-10-26 扬州三友合成化工有限公司 一种甲基苯基二氯硅烷的制备方法

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Publication number Publication date
JP6338651B2 (ja) 2018-06-06
CN105164140A (zh) 2015-12-16
CN105164140B (zh) 2018-04-17
EP2970343A1 (en) 2016-01-20
KR20150131352A (ko) 2015-11-24
WO2014152436A1 (en) 2014-09-25
US9828394B2 (en) 2017-11-28
US20160031917A1 (en) 2016-02-04
EP2970343B1 (en) 2017-10-25
JP2016512265A (ja) 2016-04-25

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