KR102134538B1 - Manufacturing method of shampoo having function of preventing hair lose and stimulating hair sprouting - Google Patents

Abstract

The present invention provides a method of preparing a medicinal shampoo having hair loss-preventing and hair growth-promoting functions, the method comprising: a step of mixing fish mint, perilla, green tea, and goji berry in a weight ratio of 5-7 : 2-3.5 : 2-3.5 : 0.5-1.5 and extracting therefrom a medicinal herb component using an alcohol; a step of heating hop and filtering the same; a step of extracting beer yeast using an alcohol; a step of mixing bentonite with water, letting the mixture stand still, and collecting overlying water therefrom; a base layer preparation step of mixing the medicinal herb component extract, the hop filtrate, the beer yeast extract, and the overlying water in a weight ratio of 6-8 : 0.1-2 : 0.1-2 : 0.1-2; a first composition preparation step of mixing a base layer, a thickener, and a surfactant in a weight ratio of 2.5-3.5 : 0.2-0.4 : 3.0-4; and a second composition preparation step of adding a preservative in a weight ratio of 0.6-1.3 with respect to a weight ratio of the base layer in the first composition of 2.5-3.5.

Description

Manufacturing method of pharmacological shampoo having the function of preventing hair loss and promoting hair growth{Manufacturing method of shampoo having function of preventing hair lose and stimulating hair sprouting}

The present invention relates to a method for manufacturing a shampoo having a pharmacological component, and more specifically, while effectively exhibiting the efficacy of natural extracts such as Eoseongcho, Jasobul, green tea, goji berry, etc. It relates to a method of manufacturing a pharmacological shampoo that can promote hair growth.

Shampoo is a kind of detergent for washing off foreign substances such as dust, oil, and sweat on the scalp and hair. In general, shampoo contains surfactants and fragrances, as well as nutrients and moisturizing substances to improve hair condition. Contains a back.

These shampoos need to choose a product that has adequate irritation while having little irritation to the skin as much as possible considering the degree of sebum of the hair.In recent years, various types including pharmacological ingredients that are beneficial to hair or scalp in place of the existing rinse-based shampoo 'S shampoo is being introduced one after another.

Among them, as in Korean Patent Publication No. 2016-0069953, there are many cases of using natural extracts such as Eoseongcho, Jasobul, and green tea. Eoseongcho, Jasobul, green tea, etc. are known to have a function of preventing hair loss as well as promoting hair growth, but these extracts themselves have a drawback of making hair stiff, so there are certain limitations in using shampoos containing these ingredients.

Republic of Korea Registered Patent No. 1802961 Republic of Korea Patent Publication No. 2016-0069953

The present invention has been proposed to improve the problems of the prior art, and the object of the present invention is to produce a shampoo that can prevent hair loss and promote hair growth without sacrificing the flexibility of the hair while the efficacy of the natural extract is fully exhibited. Propose a method.

In order to achieve this object, the present invention comprises the steps of mixing the weight ratio of Eoseongcho, Jasobul, green tea and goji berries to 5~7:2~3.5:2~3.5:0.5~1.5, followed by alcohol extraction of the herbal ingredients; Heating the hop and then filtering; Alcohol extraction of beer yeast; Mixing bentonite and water, standing still, and recovering the upper water; A base layer preparation step of mixing the weight ratio of the herbal ingredient extract, the hop filtrate, the beer yeast extract, and the upper layer water in a ratio of 6 to 8: 0.1 to 2: 0.1 to 2: 0.1 to 2; A primary composition preparation step of mixing the weight ratio of each of the base layer, the thickener, and the surfactant to 2.5 to 3.5: 0.2 to 0.4: 3.0 to 4; Based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition, the secondary composition manufacturing step of adding a preservative from 0.6 to 1.3 weight ratio; is characterized by its technical characteristics, including.

In the primary composition, the thickener is made of guar chloride and glucanade, and the weight ratio of guarchloride and glucanade each has 0.1 to 0.2 based on the weight ratio of the base layer; In the primary composition, the surfactant is made of glucoside and coco betaine, and the weight ratio of each of the glucoside and coco betaine may be 1.5 to 2 based on the weight ratio of the base layer.

In addition, based on the weight ratio of the base layer, the nettle extract, iris extract, silk amino acid, keratin, espinozilia, ceramide, and tocopherol may each be added in a weight ratio of 0.1 to 0.5.

In addition, in the secondary composition, the preservative is composed of a water-soluble preservative and a fat-soluble preservative, and the weight ratio of each of the water-soluble preservative and the fat-soluble preservative is 0.5 to 0.8: 0.1 to based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition. 0.2.

In addition, an aromatic oil is added to the secondary composition, and the aromatic oil added to the secondary composition may be formed in a 0.5 to 1 weight ratio based on a 2.5 to 3.5 weight ratio of the base layer contained in the primary composition.

The present invention not only can maintain the pharmacological components contained in Eoseongcho, Jasobul, green tea, goji berry intact in shampoo, but also does not cause deterioration of the flexibility of the hair by these pharmacological components, and further, when used continuously for a long time, the scalp state It can be improved to prevent hair loss and promote hair growth.

1 and 2, respectively, test reports analyzing the embodiments according to the present invention

The preferred embodiment according to the present invention will be described in detail with reference to the accompanying drawings. In the detailed description of the embodiment of the present invention, there is no direct relevance to the technical features of the present invention, or in the technical field to which the present invention pertains Details that are apparent to those who have knowledge of will be omitted.

The present invention relates to a method of manufacturing a pharmacological shampoo, characterized by comprising a herbal ingredient extraction step, hop filtration step, beer yeast extraction step, upper layer water recovery step, base layer production step and primary and secondary composition composition steps . Hereinafter, each of these steps will be described in detail.

First, prepare Eoseongcho, Jasobul, green tea, and goji berries. Eoseongcho contains a quercitrin component that expands the capillaries, allowing blood circulation of the scalp pores to be well performed, and is known to be effective in alleviating hair loss and improving hair loss by removing various inflammations, toxins and waste products. .

In addition, it further suppresses the growth of dihydrotestosterone and hair follicles as hair loss enzymes, which have been pointed out as the main causes of hair loss, helps inflammatory hair loss, and has a function of preventing hair loss by increasing female hormones due to the richness of polyphenols.

Cotyledon, also known as perilla, improves blood circulation without specific side effects, and is especially rich in vitamins B1, B2, B6, C, E, K and iron, potassium, magnesium and minerals, and also contains vitamin B3. It is known to maintain the scalp. In addition, it is known that when the lobule is mixed with green tea, it has a positive function in preventing hair loss and promoting hair growth.

Green tea is an epigallocatechin gallate or catechin, which is known as a powerful antioxidant, and has an effect of delaying hair loss as well as suppressing hair loss, and is known to help treat hair loss. Goji berries are rich in phosphorus and calcium, and betaine, especially in goji berries, is known to impart excellent moisturizing effects to the scalp.

When Eoseongcho, Jasobul, green tea, and goji berries are prepared, the weight ratio of each of them is 5 to 7: 2 to 3.5: 2 to 3.5: 0.5 to 1.5, mixed, and then extracted with herbal ingredients.

In the case of Eoseongcho, the effect of expanding the capillaries of the scalp is reduced when mixed in an amount of less than 5% by weight, and does not completely inhibit the hair loss enzyme dihydrotestosterone. On the other hand, if the weight ratio of Eoseongcho exceeds 7, the scalp may be stimulated due to the increased pharmacological composition of Eoseongcho.

In the case of the cotyledon, when it is mixed under 2 weight ratio, the content of useful ingredients such as vitamins is insignificant, making it difficult to maintain the moisture of the scalp, and it is difficult to achieve a smooth blending ability with green tea, and thus the function of preventing hair loss and promoting hair growth is significantly reduced. On the other hand, when the weight ratio of cotyledon exceeds 3.5, the contents of useful ingredients such as vitamins, potassium, and minerals become abundant, but the likelihood of a headache may increase.

In the case of green tea, when it is mixed under 2 weight ratio, the antioxidant power is weakened, and the function of retarding or suppressing hair loss is weakened. When the weight ratio exceeds 3.5, it is not possible to improve blood circulation of the scalp due to poor mixing ability with the lobule. Adverse effects may occur.

In the case of wolfberry, when the weight ratio is less than 0.5, the hair loss prevention and reversion function is weakened, and the moisturizing component is small, making it difficult to impart shine and flexibility to the hair. On the other hand, if the goji berries are mixed in excess of 1.5 weight ratio, the rejection reaction of the scalp may occur.

Herbal ingredient extraction may be achieved through alcohol extraction within a range of 20 to 28 hours. The alcohol is preferably made of any one or more of methanol, ethanol, isopropyl alcohol, and isobutanol, but is not limited thereto.

When the extraction is performed in less than 20 hours, all of the fat-soluble pharmacological components contained in each herb may not be extracted, and when extraction is performed for more than 28 hours, the pharmacological components may be modified in the extraction process.

When all the fat-soluble pharmacological components contained in each of Eoseongcho, Jasobul, green tea, and goji berries are extracted using alcohol, purified water is added to the extracted alcohol and then heated. In the heating process, when the boiling point is reached, the temperature is lowered and heating is continued until the total amount is 1/2, so that herbal extracts can be obtained. It is preferable that each of herbal medicine and alcohol is mixed in a weight ratio of 1:1.5 to 2.5.

Next, prepare hops. Hop is a plant used as the main raw material for beer. Humulon contained in hops has a bitter taste and antimicrobial activity, and beta acid, lupulon, is a polypeptide antibiotic, and is known to have excellent effects on mold and bacteria.

In addition, myrcene and polyphenols contained in hops contain fragrance components, and polyphenols also have antibacterial properties. Due to these ingredients, hops have excellent effects in suppressing hair loss and preventing dandruff, and can function as a very effective scalp care agent by acting as a natural preservative.

When the hops are ready, the hops are heated in the range of 5-10 minutes and then filtered to obtain a liquid hop filtrate. When heating is performed in less than 5 minutes, all useful components of the hops are not extracted, and when heated for 10 minutes or more, useful components of the hops may be eluted, resulting in component changes. The hop is heated in a mixed state with purified water, and it is preferable that the hop and purified water are mixed in a weight ratio of 0.1 to 0.3: 1 to 3.

At this time, when filtering the heated hops, it is preferable to filter only particles of 300 mesh or more. Because particles less than 300 mesh are too large to be usable, they are filtered out during the filtration process.

Next, prepare brewer's yeast. The key ingredient of brewer's yeast is selenium, which has strong antioxidant power. In particular, selenium is known to have an inhibitory effect on free radicals, which is the main cause of hair loss, about 31 times that of barley and 100 times that of garlic, and it is known to activate stem cells to increase the content of growth factors derived from hair follicle stem cells. have.

In addition, brewer's yeast contains minerals such as chromium and zinc, and beta-glucan, which helps immunity. Among them, beta-glucan has a function of activating immune cells in the human body, and has higher content than beef or milk. The protein contained in is similar to the protein in hair, and is known to help strengthen hair while absorbing quickly.

When the brewer's yeast is ready, it is extracted with alcohol. The alcohol used for extraction is roughly the same as in the case of extracting the above-mentioned pharmacological components, and when the useful component of beer yeast is extracted, it is filtered through a filter. It is preferable to filter only particles of 300 mesh or more. At this time, it is preferred that the beer yeast and alcohol are mixed in a weight ratio of 1 to 2: 1 to 5 and an extraction process is performed.

Next, the upper water is recovered. The upper layer water is recovered after mixing bentonite and water. Bentonite is a mineral with excellent heavy metal adsorption properties, and contains a large amount of natural minerals such as calcium, iron, and germanium.

The recovery of the upper water can be done as follows. After mixing bentonite and water, let stand for about a week. In this case, the bentonite layer is formed by sinking coarse particles of bentonite in the lower layer portion, and the transparent and clear upper layer water separated from the bentonite layer floats in the upper portion. The work is terminated by recovering this very supernatant containing a large amount of useful components of bentonite.

At this time, bentonite and water may be mixed in a weight ratio of 0.1 to 2: 4 to 6. If the weight ratio of bentonite is less than 0.1, the upper layer water does not contain enough minerals contained in bentonite, and when the bentonite weight ratio exceeds 2, there is a problem that the absolute amount of the recovered upper layer water itself decreases.

Conversely, if the weight ratio of water is less than 4, the amount of the upper layer water recovered is small and productivity decreases. When the weight ratio of water exceeds 6, the amount of useful components derived from bentonite contained in the upper layer water is insignificant, so that the utilization of useful components of bentonite decreases. do.

When each of herbal extracts, hops, beer yeast extract, and upper water is prepared, the weight ratio of each of them is mixed in the range of 6-8: 0.1-2: 0.1-2: 0.1-2. Accordingly, base layers containing various types of pharmacological components and useful components are prepared.

At this time, in the case of the herbal ingredient extract, when the mixture is less than 6 weight ratio, it is difficult to exert the function of the pharmacological component, and when the weight ratio exceeds 8, it is necessary to mix more each of the hop filtrate, beer yeast extract, and upper layer water, resulting in a decrease in productivity. There is.

In the case of a hop filtrate, when mixed below 0.1 weight ratio, it is difficult to suppress the occurrence of dandruff, as well as the function as a natural preservative may be weakened, and when the weight ratio exceeds 2, the effect of suppressing dandruff is increased, but other extracts, etc., by hop filtrate It can change the properties of useful components.

In the case of the beer yeast extract, when the mixture is less than 0.1 weight ratio, the aging of the hair can be accelerated, and the strength of the hair can also be weakened. If the weight ratio exceeds 2, the strength of the hair is dramatically increased and the hair itself is very rigid. May occur.

In the case of upper layer water, when mixed in an amount of less than 0.1 weight ratio, it is difficult to expect efficacy by various types of minerals derived from bentonite, and there is a problem in that a function of removing harmful substances remaining on the scalp is reduced due to a decrease in adsorption with heavy metals. On the other hand, if the weight ratio exceeds 2, the elasticity and nutritional supply of the scalp is improved, but each composition to be described later may adversely affect physical properties.

When the base layer is prepared, a primary composition is prepared by mixing each of a thickener and a surfactant in the base layer. At this time, the thickener to be mixed may be made of guar chloride to enhance the cleaning power and gluca maid to improve the adhesion to the scalp.

The surfactant can consist of glucoside and cocobetaine. However, the present invention is not limited to this, and does not exclude a case consisting of a surfactant selected from natural surfactants or naturally occurring surfactants.

At this time, the weight ratio of each of the base layer, the thickener, and the surfactant is preferably mixed in a range of 2.5 to 3.5: 0.2 to 0.4: 3.0 to 4, and when the thickener is made of guar chloride and glucamade, guar chloride is based on the base layer weight ratio. And it is preferable that the weight ratio of each of glucamade is 0.1 to 0.2, and when the surfactant is made of glucoside and coco betaine, the weight ratio of glucoside and coco betaine is preferably 1.5 to 2 based on the weight ratio of the base layer.

In the case of the base layer, if the weight ratio is less than 2.5, the shampoo formulation may feel a little stiff, and if the weight ratio exceeds 3.5, the shampoo formulation itself may feel too thin. In the thickener, when the weight ratio of guar chloride is less than 0.1, the cleaning effect decreases, and on the contrary, when the weight ratio of guar chloride exceeds 0.2, there is a fear of irritating the scalp.

It is known that gluca maid is used only with guar chloride, which is a cation constituting a thickener as an anion, to improve the cleaning effect.

When too little surfactant is added, since foaming is not easily generated and the cleaning effect may be reduced, it is preferable that each of the glucoside and cocobetaine constituting the surfactant is added in a weight ratio of 1.5 to 2 based on the weight ratio of the base layer.

In preparing the primary composition, a thickener can be used by mixing with glycerin. That is, after heating glycerin in a range of 58 to 60° C. and then adding and melting guar chloride, gluca maid is melted in a mixed solution of glycerin and guar chloride.

At this time, the thickener and glycerin are preferably mixed in a 1:1 weight ratio. That is, it is preferable that the combined weight of guar chloride and glucamade and the weight of each of glycerin are mixed in a ratio of 1:1.

Further, when each of guar chloride and glucan maid is mixed with glycerin, it is preferable that the weight ratio of guar chloride and glucan maid is 1:2. This is because it can irritate the scalp when it contains a lot of guar chloride.

On the other hand, the present invention does not exclude the case where, when the primary composition is prepared, nettle extract, iris extract, silk amino acid, keratin, espinozilia, ceramide, and tocopherol are each added.

The nettle extract has the effect of boosting blood circulation of the scalp, the iris extract has the effect of providing shine and flexibility to the hair, and each of the silk amino acids and keratin is effective in restoring damaged hair, and ispinozilia has antibacterial and Anti-inflammatory has the effect of preventing hair loss and promoting hair growth, and ceramide has the effect of moisturizing.

Each of nettle extract, iris extract, silk amino acid, keratin, espinozilia, ceramide, and tocopherol is preferably added in a weight ratio of 0.1 to 0.5 based on the weight ratio of the base layer in the primary composition. Each of the nettle extract and the iris extract may use commercially available products.

When the primary composition is prepared, a secondary composition is prepared by adding a preservative thereto. The preservative is to prevent mold growth, to prevent rancidity of the shampoo, and to soften the scalp, based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition, is preferably added in a weight ratio of 0.6 to 1.3.

At this time, the preservative may be made of a water-soluble preservative and a fat-soluble preservative. As the water-soluble preservative, 1,2hexanediol or naphri may be used, and Vit E may be used as the fat-soluble preservative.

When the preservative consists of a water-soluble preservative and a fat-soluble preservative, each of these is preferably added in a weight ratio of 0.5 to 0.8: 0.1 to 0.2 based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition. That is, when the preservative is added at a weight ratio of 0.6 to 1.3 based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition, each of the water-soluble preservative and the fat-soluble preservative that constitutes the preservative is added at 0.5 to 0.8: 0.1 to 0.2.

Each of the water-soluble preservative and the fat-soluble preservative decreases the storage effect when the weight ratio is less than 0.5, and even if the weight ratio is added in excess of 0.8, the storage period is not long or the storage effect is not improved. Therefore, it is preferable that the base layer contained in the primary composition is added in a weight ratio within the range of 0.5 to 0.8: 0.1 to 0.2 based on the weight ratio of 2.5 to 3.5.

When a secondary composition is prepared by adding a preservative to the primary composition, the preparation of the pharmacological shampoo according to the present invention is completed. That is, a shampoo capable of preventing hair loss and promoting hair growth is made without deteriorating the flexibility of the hair while the efficacy of the extract derived from nature is fully exhibited.

Meanwhile, the present invention does not exclude the case where an aromatic oil is added to the secondary composition. The aroma oil is intended to impart fragrance to the shampoo, and the aroma oil is preferably added in a 0.5 to 1 weight ratio based on the 2.5 to 3.5 weight ratio of the base layer contained in the primary composition.

In adding the aromatic oil to the secondary composition, the effect of the added fragrance can hardly be expected when added in less than 0.5 weight ratio based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition, otherwise the weight ratio exceeds 1 When added, oil may be deposited on the hair and scalp due to excessive oil.

Each of the attached Figures 1 and 2 is a test report analyzing the shampoo prepared according to the present invention, whereby the shampoo contains hazardous substances such as lead, arsenic, mercury, antimony, cadmium, nickel, methanol, formaldehyde, and phthalates. It can be confirmed that this is not detected at all. Although dioxane was partially detected, it was added as a surfactant for the test results, and it is needless to say that stability can be guaranteed for use in that the detected values are far below the standards.

In the above, the present invention has been described in terms of preferred embodiments, but this is only an example, and the present invention is not limited to this and can be implemented in various ways, and further, based on the disclosed technical idea, separate technical features are provided. It will be apparent that it can be carried out in addition.

Claims (5)

Eoseongcho, Jasobul, green tea and goji each weight ratio of 5 to 7: 2 to 3.5: 2 to 3.5: 0.5 to 1.5, followed by mixing and then extracting the herbal ingredients for alcohol;
Heating the hop and then filtering;
Alcohol extraction of beer yeast;
Mixing bentonite and water, standing still, and recovering the upper water;
A base layer preparation step of mixing the weight ratio of the herbal ingredient extract, the hop filtrate, the beer yeast extract, and the upper layer water in a ratio of 6 to 8: 0.1 to 2: 0.1 to 2: 0.1 to 2;
A primary composition preparation step of mixing the weight ratio of each of the base layer, the thickener, and the surfactant to 2.5 to 3.5: 0.2 to 0.4: 3.0 to 4;
Based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition, a secondary composition manufacturing step of adding a preservative 0.6 to 1.3 weight ratio;
A method of manufacturing a pharmacological shampoo having a function of preventing hair loss and promoting hair growth. According to claim 1,
In the primary composition, the thickener is made of guar chloride and glucanade, and the weight ratio of guarchloride and glucanade each has 0.1 to 0.2 based on the weight ratio of the base layer; In the primary composition, the surfactant is composed of glucoside and coco betaine, and the weight ratio of glucoside and coco betaine is 1.5 to 2 based on the weight ratio of the base layer. Method of manufacturing shampoo. According to claim 1,
The primary composition has a hair loss prevention and hair growth promotion function, characterized in that each of the nettle extract, iris extract, silk amino acid, keratin, espinozilia, ceramide, and tocopherol is added in a weight ratio of 0.1 to 0.5 based on the weight ratio of the base layer. Method of manufacturing pharmacological shampoo. According to claim 1,
In the secondary composition, the preservative is composed of a water-soluble preservative and a fat-soluble preservative, and the weight ratio of each of the water-soluble preservative and the fat-soluble preservative is 0.5 to 0.8: 0.1 to 0.2 based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition. Method for producing a pharmacological shampoo having a function to prevent hair loss and promote hair growth, characterized in that. According to claim 1,
Aroma oil is added to the secondary composition, and the aroma oil added to the secondary composition is hair loss prevention and hair growth, characterized in that it consists of 0.5 to 1 weight ratio based on the base layer weight ratio of 2.5 to 3.5 contained in the primary composition. Method of manufacturing a pharmacological shampoo having an promoting function.

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