KR102104502B1 - A shampoo containing extracts of sword bean and preparing method thereof - Google Patents

Abstract

The present invention relates to a shampoo containing a small bean extract and a method for manufacturing the same, and more specifically, a natural material known as pea bean ( Canavalia gladiata ), which is known to have efficacy and effects such as antioxidant, antibacterial, anti-cancer, anti-inflammatory, and blood circulation promotion. The present invention relates to a shampoo containing peanut extract capable of obtaining a shampoo having a function of maintaining and promoting scalp health by mixing the extract obtained by extraction and a method for manufacturing the same.
The shampoo containing the pea bean extract according to the present invention is characterized in that the pea bean extract is added to the lysate in which the detergent raw material is dissolved in purified water and mixed.

Description

Shampoo containing pea extract and its manufacturing method {A SHAMPOO CONTAINING EXTRACTS OF SWORD BEAN AND PREPARING METHOD THEREOF}

The present invention relates to a shampoo containing a small bean extract and a method for manufacturing the same, and more specifically, a natural material known as a small bean ( Canavalia gladiata ) that has efficacy and effects such as antioxidant, antibacterial, anti-cancer, anti-inflammatory, and blood circulation promotion. The present invention relates to a shampoo containing peanut extract capable of obtaining a shampoo having a function of maintaining and promoting scalp health by mixing the extract obtained by extraction and a method for manufacturing the same.

The shampoo that is widely used today is originally a hair-washing cosmetic that removes contaminants from the scalp and hair to maintain cleanliness and beauty, but in the meantime, it goes beyond simple functions to suit the various needs of consumers, and is selected by consumers according to the condition of the hair and scalp. Research into the development of functional products that are more specialized and subdivided for use has been actively conducted.

As a result, products with functional substances added to improve the scalp and hair, that is, oil and cream moisturizing shampoo, anti-dandruff shampoo to prevent dandruff and itchiness, and conditioning to prevent hair damage during washing Shampoos, hypoallergenic shampoos for hair and scalp, and color protection shampoos for dyed hair have been developed and are widely available.

However, most of these products are chemical products, so consumers have anxiety about safety. Therefore, companies have registered with Korea Patent No. 10-1580216 (a shampoo containing a scalp protection and hair improvement composition and its manufacturing method) or a Republic of Korea Patent No. 10-1108710 (an herbal chrysanthemum composition and a method for manufacturing body and scalp cleanser using the same) In order to resolve consumer anxiety, such as the product disclosed in), efforts are made to develop products using natural materials with excellent safety and eco-friendliness.

However, it is still limited to products using some materials, such as green tea, Eoseongcho, cypress, and ginger, so the development and marketing of products using various eco-friendly materials are urgently needed to maintain and promote scalp health of mankind. Trend.

Meanwhile, cana beans gladiata ) is the largest variety, and the shape of soybean pods is similar to that of small beans, and is also called small beans. The flowering period is from June to July, and the fruiting period is from August to October. The length of the pods is about 10-30 cm. There are about 10 beans in one pod and classified into red and white species.

Pea beans contain various physiologically active ingredients such as urease, hemagglutinine, canavanine, and canavalia gibberellin Ⅰ and Ⅱ, providing excellent efficacy, effectiveness, and palatability. Therefore, it has been used as a special medicine to treat purulent inflammation such as sinusitis, hemorrhoids, and boils in Korea since ancient times. It was developed and sold as a health supplement and health tea in China and Japan. Recently, it has been reported to have efficacy and effects such as anti-cancer, anti-inflammatory, chronic nephritis and anemia prevention, anti-oxidation, antibacterial action, anti-diabetes, anti-allergic (anti-allergic, acne, etc.), skin regeneration.

As described above, small beans have a variety of excellent efficacy and effects such as antioxidant, antibacterial, anti-cancer, anti-inflammatory, anemia prevention, skin regeneration, and blood circulation, so that the cultivation is increasing in Korea, but the utilization is still insignificant.

Republic of Korea Patent Registration No. 10-1580216: Shampoo containing a composition for protecting the scalp and improving hair and a method for manufacturing the same Republic of Korea Patent No. 10-1108710: Herbal chrysanthemum composition and method for manufacturing body and scalp cleanser using the same

The present invention was devised by recognizing the above points, and the object of the present invention is a natural material known as pea bean ( Canavalia) , which is known to have efficacy and effects such as antioxidant, antibacterial, anticancer, anti-inflammatory, and blood circulation promotion. It is to provide a shampoo containing a small bean extract that can obtain a shampoo having a function of maintaining and promoting scalp health by mixing the extract obtained by extracting gladiata ) and a method for manufacturing the same.

In order to achieve the above object, the shampoo containing the peanut extract according to the present invention is characterized in that the peanut extract is added to the lysate in which the detergent raw material is dissolved in purified water and mixed.

In addition, the shampoo containing the small bean extract according to the present invention, the detergent raw material is sodium lauroyl sacosinate 35% by weight relative to the total weight of the shampoo, cocamidopropylbetaine-sodium chloride mixture 15%, lauramide die 4%, Polyquaternium-7 2%, Glycerin 5%, Fiji-120 methyl glucose dioleate 1%, Citric Acid 0.5%, Sodium Benzoate 0.25%, Polyquaternium-10 0.2%, Disodium ID 0.1 %, Consisting of 0.05% panthenol, and the small bean extract is concentrated to 20brix% of solid content, so that 2% of the total weight of the shampoo is added to the lysate in which the detergent raw material is dissolved in purified water, and polysorbate based on the total weight of the shampoo as an additive. 20 0.5% and flavoring 0.7% is characterized in that the detergent raw material is added to the lysate dissolved in purified water.

In addition, the manufacturing method of the shampoo containing the small bean extract according to the present invention includes a dissolution step of dissolving the detergent raw material in purified water, an adding step of adding the small bean extract to the lysate in which the detergent raw material is dissolved in purified water, and the small bean extract. It characterized in that it comprises a stirring step of stirring the added melt.

In addition, in the method for preparing a shampoo containing the pea extract according to the present invention, in the dissolving step, the detergent raw material is 35% sodium lauroyl sacosinate, 15% cocamidopropyl betaine, sodium chloride mixture, based on the total weight of the shampoo, Lauramide DJ 4%, Polyquaternium-7 2%, Glycerin 5%, Fiji-120 methyl glucose dioleate 1%, Citric Acid 0.5%, Sodium Benzoate 0.25%, Polyquaternium-10 0.2% , Consisting of 0.1% disodium ID, 0.05% panthenol, and in the adding step, the small bean extract is concentrated to 20brix% of solid content, so that 2% of the total weight of the shampoo is added to the lysate in which the cleaning material is dissolved in purified water. In the adding step, 0.5% of polysorbate 20 and 0.7% of fragrance relative to the total weight of the shampoo as an additive are characterized in that the detergent raw material is further added to the dissolved material in purified water.

In addition, the method for producing a shampoo containing the pea extract according to the present invention, the pea extract is a boiled step of boiling the pea by adding water to the pea, and a static step of adding water and ethanol to the boiled pea to settle and It is characterized in that it is extracted from peanuts through a filtration step of filtering out the liquid substance containing solids, and a concentration step of concentrating the liquid substance containing solids that has passed through the filtration step until the solid content is 20 brix%. .

The shampoo containing the pea bean extract according to the present invention and the manufacturing method according to the above configuration are natural materials known as pea beans ( Canavalia) , which are known to have efficacy and effects such as antioxidant, antibacterial, anti-cancer, anti-inflammatory, and blood circulation. gladiata ) has the advantage of obtaining a shampoo having a function of maintaining and promoting scalp health by mixing the extract obtained by extracting it.

1 is a flow chart showing a method of manufacturing a shampoo containing a small bean extract according to an embodiment of the present invention
Figure 2 is a flow chart showing the manufacturing process of the pea extract in a method for producing a shampoo containing pea extract according to an embodiment of the present invention
Figures 3a to 3h is a photograph of the process of manufacturing the small bean extract in the manufacturing method of the shampoo containing the small bean extract according to an embodiment of the present invention

Hereinafter, a method of manufacturing a shampoo containing a pea extract according to the present invention will be described in more detail with reference to Examples.

1 is a flow chart showing a method of manufacturing a shampoo containing a small bean extract according to an embodiment of the present invention, Figure 2 is a small bean extract in a method of manufacturing a shampoo containing the small bean extract according to an embodiment of the present invention It is a flow chart showing the manufacturing process, Figures 3a to 3h is a photograph of the manufacturing process of the small bean extract in the manufacturing method of the shampoo containing the small bean extract according to an embodiment of the present invention.

In particular, FIG. 3A is a photograph of raw peas, raw material of FIG. 3B is a photograph of boiled peas through a boiling step (S21), and FIG. 3C is a photograph of adding ethanol in a stationary step (S22), and FIG. 3D Is a photograph of the state in which the ethanol is added in the stationary step, and FIG. 3e is a photograph of the state being filtered with a strainer in the filtration step (S23), and FIG. 3f is a photograph of the pea extract extracted through the filtration step (S23). , Figure 3g is a photograph of the process of concentrating the pea extract in the filtration step (S24), Figure 3h is a photograph of the pea extract concentrated through the filtration step (S24).

The shampoo containing the pea extract according to the present invention according to the present invention is characterized in that the detergent raw material constituting the shampoo is mixed by adding the pea extract to the lysate dissolved in purified water.

At this time, the detergent raw material is sodium lauroyl sacosinate 35% based on the total weight of the shampoo, cocamidopropyl betaine-sodium chloride mixture 15%, lauramide die 4%, polyquaternium-7 2%, glycerin 5%, It is composed of 1% PG-120 methyl glucose dioleate, 0.5% citric acid, 0.25% sodium benzoate, 0.2% polyquaternium-10, 0.1% disodium IDA, and 0.05% panthenol, compared to the total weight of the shampoo. It is used for 33.70% of purified water.

In addition, the small bean extract has a solid content of 20 brix%, so that 2% of the total weight of the shampoo is added to the lysate in which the detergent raw material is dissolved in purified water, and 0.5% of the total weight of the shampoo as an additive and 0.5% of the fragrance 0.7% A The raw material for the cleaning agent is added to the lysate dissolved in purified water.

The manufacturing method for preparing the shampoo containing the peanut extract according to the present invention as described above is a dissolving step (S10) of dissolving the detergent raw material in purified water, and adding the peanut extract to the melt of the detergent raw material dissolved in purified water It comprises a step (S20) and a stirring step (S30) of stirring the lysate to which the small bean extract is added.

In addition, the small bean extract boils the small beans by adding water to the small beans (S21), and the stationary step (S22) of adding water and ethanol to the boiled small beans, and filtering the liquid material containing solids. Filtration step (S23), and the filtration step (S23) through the concentration step (S24) to concentrate the liquid material containing the solid content until the solid content is 20 brix% is extracted from the peas.

Hereinafter, a specific example of the shampoo containing the peanut extract according to the present invention as described above and a method of manufacturing the same will be described.

<Example 1: Extract of oil-soluble substance of peanut>

1. Materials

For the production of scalp cleansing sampu, which is good for scalp health, peanuts from 2017 were used in Goseo Nonghyup, Jeollanam-do (see Fig. 3a). In order to remove foreign substances, the purchased peas were washed clean with water and then dried.

2. Extraction and filtration

The extraction of oil-soluble substances of peanuts is carried out by mixing hot water and solvent extraction.

After adding 20kg of the peas to the kiln, add 1.5 times the weight of the peas, raise the temperature to 100 ℃ and cook it completely (see Fig. 3b), and then add ethanol to the ratio of 7: 3 between water and ethanol (Fig. 3c). Thereafter, the mixture was allowed to stand for 6 hours while maintaining at 60 ° C (see FIG. 3D), and then a liquid substance was separated and filtered through a strainer (see FIG. 3E) to obtain an extract having a solid content of 11 brix% (see FIG. 3F).

3. Concentration

The pea extract obtained by mixing the hot water and solvent extraction method is concentrated using a reduced pressure concentrator (NE-1001, EYELA) until the solid content is 20 brix% at 60 ° C (see FIGS. 3g and 3h).

4. Physical properties analysis of extract quality

(1) Appearance

As a result of visual observation of the pea extract extract, the color was yellow, and it was found to be suitable for the production of scalp cleanser products such as shampoo by exhibiting the (slightly savory) odor of soybean oil.

(2) pH of substance

As a result of measuring the acidity of the pea extract extract with a pH meter (pHTestr 30, OAKTON, USA), the pH value was 6.2, indicating weak acidity.

5. Understanding the efficacy and effectiveness of extract quality

(1) Antibacterial power

Staphylococcus aureus ATCC 8739 strain, which is the most widely present on troubled skin (especially atopic skin), was used to measure the antibacterial activity of the extract of pea extract. Liquid medium was prepared by mixing the extracts of peas with Tryptic Soy (Difco) at concentrations of 0%, 1%, 2%, 3%, and 5%, respectively. Thereafter, 0.2 ml of Staphylococcus aureus is inoculated by 0.2 ml to be 2.0 x 10 ⁷ CFU per 1 g of the sample, and then cultured at 37 ° C to measure the number of viable bacteria that periodically survive until 1, 7, 14, 21, and 28 days. The observed changes were observed.

As a result of the test, bacteria that survive up to 28 days containing less than 1% of pea extract extract were detected. However, in the medium containing 2%, the initial strain number was maintained, and gradually decreased after 21 days, and in the medium containing 5%, the bacteria were initially killed.

Therefore, when used for antibacterial purposes, it is preferable to use it at a high concentration in consideration of the effect on the shampoo product by the addition of the pea extract.

(2) antioxidant power

The antioxidation degree of pea extract extract was evaluated for reducing power to DPPH (1,1-diphenyl-2-picrylhydrazyl, Sigma-Aldrich, St. Louis, Mo, USA). That is, 1 ml of samples with different concentrations of 0 µg / ml, 20 µg / ml, 40 µg / ml, 60 µg / ml, 80 µg / ml, and 100 µg / ml and 1 ml of 400 uM DPPH solution in ethanol solvent 2 It was treated to a final 4 ml by adding ml. The blank test was conducted with 1 ml of 90% ethanol instead of the sample. After reacting for 30 minutes at room temperature, the absorbance was measured at 517 nm, and the activity of the sample was expressed as the concentration (SC ₅₀ , 50% Scavenging Concentration) necessary for 1/2 reduction of the absorbance of the control, and the sample of the control was a- Tocopherol was used.

As a result of the test, the DPPH radical-scavenging activity of the pea extract extract was lower than that of the control, but showed a tendency to be proportional to the increase in concentration. In particular, at a high concentration of 100 μg / ml, the DPPH radical-scavenging activity was very high. Table 1 summarizes the DPPH radical-scavenging activity according to the concentration of pea extract.

division 10 μg / ml  20µg / ml 30µg / ml  40µg / ml  50 μg / ml 60µg / ml α-Tocopherol 56 84 89 91 93 93 Small bean extract concentrate 14 31 52 68 79 90

6. Raw material of shampoo of small bean extract concentrate

1,3-Butylene alcohol and 1, which are widely used as cosmetic ingredients today because they have a solvent, antiseptic, and moisturizing effect in order to preserve the pea extract extract for a long time and easily use it as a raw material for the shampoo containing the pea extract according to the present invention: It was blended in a ratio of 1 volume to make cosmetic raw materials.

<Example 2: Product Manufacturing>

1. Manufacture of products with different concentrations of small bean extract concentrate

Eldia Cosmetics Company By obtaining a cooperation, a pre-prescription for the preparation of a shampoo containing a pea extract according to an embodiment of the present invention was constructed, sufficiently dissolved at a temperature of 70 ° C, and then cooled to 50 ° C, so that the blending concentration of the pea extract extract was 0%, 1, respectively. %, 2%, 3%, and 5%. Table 2 summarizes the formulation concentrations of the pre-prescription and the pea extract extract for the preparation of a shampoo containing the pea extract according to an embodiment of the present invention.

After adding the extract concentrate, the mixture was stirred until it was sufficiently mixed at 3,000 rpm using a stirrer (2.5VER., TOKUSHU KIKA KOGYO CO. LTD, JAPAN), and then cooled to room temperature to prepare a product having a different blending concentration of pea extract. . After that, the physical properties, acidity, temperature stability, and usability of the contents were investigated.

No. Last name Content (% by weight) One Sodium lauroyl sarcosinate 35.000 2 Cocamidopropylbetaine / sodium chloride 15.000 3 Lauraamide D 4.000 4 Polyquaternium-7 2.000 5 glycerin 5.000 6 PG-120 methyl glucose dioleate 1.000 7 Citric Acid 0.500 8 Sodium benzoate 0.250 9 Polyquaternium-10 0.200 10 Polysorbate 20 0.500 11 Pea Bean Extract 0-5 12 Purified water To make 100

2. Appearance and physical properties of the product according to the blending concentration of small bean extract concentrate

As a result of examining the physical properties by preparing the contents by varying the concentration of the extract extract of peas, there was no difference in color (light brown) and odor in all concentration conditions, but the viscosity showed a large difference depending on the concentration.

The viscosity of the contents was measured at 10 rpm using 2 spindles with a viscometer (DV2T, Brookfield, USA). As a result, the contents containing the pea extract extract at a concentration of 2% or less showed a difference from the standard product, especially containing a concentration of 3% or more. In one content, the viscosity was greatly reduced, which was unsuitable for application to a product. Table 3 summarizes the viscosity according to the blending concentration of the extract extract of small beans.

Concentration of extract of small bean extract concentrate 0% One% 2% 3% 5% Viscosity by compounding concentration (cp) 2,030 1,550 1,220 630 230

3. Acidity (pH) of the product according to the blending concentration of small bean extract concentrate

As a result of measuring the acidity of the contents containing the pea extract extract, the pH value was similar to 5.72 ~ 5.76 regardless of the blending concentration of pea extract extract.

4. Temperature stability of the product according to the blending concentration of small bean extract concentrate

5%, 25 ℃ (room temperature), 40 ℃, and 8-hour cycle (-4 ℃ → 25 ℃ → 50 ℃ → -4 ℃) cycled for 3 months with different concentrations of the extract concentration of pea extract, 2% concentration In the contents containing up to, there was almost no change in viscosity compared to the initial stage, but contents contained in a concentration of 3% or more showed a phenomenon in which the contents were separated due to low viscosity, which was difficult to use as a shampoo formulation, especially at a high temperature of 40 ° C.

5. Investigation of the usability of the product according to the blending concentration of small bean extract concentrate

As a result of investigating the feeling of use using contents with different concentrations of the extract concentration of pea extract, the higher the concentration added, the lower the viscosity, and the contents easily flowed out when used, and the foamability and cleaning properties were low.

6. Selection of optimal prescription containing small bean extract concentrate

According to the investigation of physical properties, temperature stability, and usability of the product according to the blending concentration of the extract extract of peanuts, the blending concentration of peanut extract concentrate was found to be limited, and extracting peanuts for the production of products suitable for optimal conditions according to the results of the survey The concentration of the concentrate was determined to be 2%, and then the final prescription was selected. Table 4 summarizes the optimal prescription for the production of shampoo containing peanut extract according to an embodiment of the present invention.

The raw materials (prescriptions 1 to 12 in Table 4) were weighed according to the prescription, placed in a kiln, dissolved at 70 ° C, and then cooled to 50 ° C to add low-temperature extracts, including pea extract extract (Table 4, Prescription 13- 15). Thereafter, the mixture was stirred until sufficiently mixed at 3,000 rpm using a stirrer, and then the product was manufactured by cooling to room temperature while removing air bubbles.

No. ingredient  persons Content (% by weight) One Purified water 33.700 2 Sodium lauroyl sarcosinate 35.000 3 Cocamidopropylbetaine, sodium chloride 15.000 4 Lauraamide D 4.000 5 Polyquaternium-7 2.000 6 glycerin 5.000 7 PG-120 methyl glucose dioleate 1.000 8 Citric Acid 0.500 9 Sodium benzoate 0.250 10 Polyquaternium-10 0.200 11 Disodium LED 0.100 12 Panthenol 0.050 13 Pea Bean Extract 2.000 14 Polysorbate 20 0.500 15 Spices 0.700 100.000

6. Product specification according to the optimal prescription containing the pea extract extract

The product was standardized as summarized in Table 5 below for thorough quality control of the shampoo containing the pea extract according to the present invention.

Item standard Product test results Appearance and color Brown slime Suitability Scent / usability Same as standard product Suitability importance 0.95 ~ 1.05 0.991 / conformity pH 4.50 ~ 6.50 5.71 / conformity Viscosity 1,000 ~ 1,800cps (2/20, 25 ℃, 60sec, one point) 1,374 / conformity Solubilization status Standard sample or more Suitability Cycling test -5 ~ 45 ℃ There should be no abnormality when cycling 3 times Suitability stability When stored at 50 ℃ for 3 days or longer, there should be no abnormality Suitability microbe Total aerobic bacteria 100cfu / g (ml) or less, specific bacteria (-) Suitability Capacity 300ml or more 302.36 Notation Same as standard sample Suitability Container status Standard sample or more Suitability

The shampoo containing the pea bean extract described above and shown in the drawings and a method for manufacturing the same are only one example for carrying out the present invention and should not be interpreted as limiting the technical spirit of the present invention. The protection scope of the present invention is defined only by the matters described in the following claims, and the improved and modified embodiments without departing from the gist of the present invention are obvious to those skilled in the art to which the present invention pertains. It will be said that it belongs to the protection scope of the present invention.

Claims (5)

In the shampoo mixed with the small bean extract is added to the lysate in which the detergent material is dissolved in purified water,
The detergent raw material is sodium lauroyl sacosinate 35% by weight of the total shampoo, cocamidopropyl betaine / sodium chloride mixture 15%, lauramide die 4%, polyquaternium-7 2%, glycerin 5%, page -120 methyl glucose dioleate 1%, citric acid 0.5%, sodium benzoate 0.25%, polyquaternium-10 0.2%, disodium IDT 0.1%, panthenol 0.05%,
The small bean extract has a solid content of 20 brix%, and 2% of the total weight of the shampoo is added to the lysate in which the cleaning material is dissolved in purified water.
Shampoo containing pea bean extract, characterized in that 0.5% of polysorbate 20 and 0.7% of fragrance relative to the total weight of the shampoo as an additive are added to the lysate in which the detergent raw material is dissolved in purified water. delete delete Dissolution step of dissolving the detergent raw material in purified water,
And the step of adding a small bean extract to the lysate in which the detergent material is dissolved in purified water,
Including the stirring step of stirring the lysate to which the small bean extract is added,
In the dissolving step, the detergent raw material is 35% sodium lauroyl sacosinate, 15% cocamidopropyl betaine / sodium chloride, 4% lauramiddiei, 2% polyquaternium-7, glycerin 5 %, Fiji-120 methyl glucose dioleate 1%, citric acid 0.5%, sodium benzoate 0.25%, polyquaternium-10 0.2%, disodium IDT 0.1%, panthenol 0.05%,
In the adding step, the small bean extract has a solid content of 20 brix%, and 2% of the total weight of the shampoo is added to the lysate in which the cleaning material is dissolved in purified water.
In the step of adding, 0.5% of polysorbate 20 and 0.7% of fragrance relative to the total weight of the shampoo as an additive, a method of manufacturing a shampoo containing a small bean extract, characterized in that the detergent raw material is further added to a lysate dissolved in purified water. According to claim 4,
The small bean extract,
Boiling step of boiling small beans by adding water to the small beans,
A political step of adding water and ethanol to the boiled peas to settle,
Filtration step to filter out the liquid substance containing solids,
Method for producing a shampoo containing peanut extract characterized in that it was extracted from peanuts through a concentration step of concentrating the liquid substance containing the solid content that has undergone the filtration step until the solid content becomes 20 brix%.

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