KR102095601B1 - 총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치 - Google Patents

총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치 Download PDF

Info

Publication number
KR102095601B1
KR102095601B1 KR1020130127179A KR20130127179A KR102095601B1 KR 102095601 B1 KR102095601 B1 KR 102095601B1 KR 1020130127179 A KR1020130127179 A KR 1020130127179A KR 20130127179 A KR20130127179 A KR 20130127179A KR 102095601 B1 KR102095601 B1 KR 102095601B1
Authority
KR
South Korea
Prior art keywords
xylene
adsorber
layers
zone
para
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020130127179A
Other languages
English (en)
Korean (ko)
Other versions
KR20140053785A (ko
Inventor
필리베르 르플레브
르 꼬끄 다미앵 레네뀌젤
Original Assignee
아이에프피 에너지스 누벨
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 아이에프피 에너지스 누벨 filed Critical 아이에프피 에너지스 누벨
Publication of KR20140053785A publication Critical patent/KR20140053785A/ko
Application granted granted Critical
Publication of KR102095601B1 publication Critical patent/KR102095601B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/12Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814Recycling of the fraction to be distributed
    • B01D15/1821Simulated moving beds
    • B01D15/1828Simulated moving beds characterised by process features
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02Monocyclic hydrocarbons
    • C07C15/067C8H10 hydrocarbons
    • C07C15/08Xylenes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/12Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
KR1020130127179A 2012-10-26 2013-10-24 총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치 Active KR102095601B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR12/02869 2012-10-26
FR1202869A FR2997396B1 (fr) 2012-10-26 2012-10-26 Procede et dispositif de production de paraxylene en contre-courant simule constitue de deux adsorbeurs en serie a nombre total de lits inferieur ou egal a 22

Publications (2)

Publication Number Publication Date
KR20140053785A KR20140053785A (ko) 2014-05-08
KR102095601B1 true KR102095601B1 (ko) 2020-03-31

Family

ID=47739331

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020130127179A Active KR102095601B1 (ko) 2012-10-26 2013-10-24 총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치

Country Status (6)

Country Link
US (1) US9145343B2 (https=)
JP (1) JP6240466B2 (https=)
KR (1) KR102095601B1 (https=)
CN (1) CN103787821B (https=)
FR (1) FR2997396B1 (https=)
TW (1) TWI579268B (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102309811B1 (ko) * 2015-08-28 2021-10-07 한화테크윈 주식회사 시간 정보 제공 장치 및 방법
FR3066401B1 (fr) * 2017-05-17 2021-04-23 Ifp Energies Now Procede de separation des xylenes en lit mobile simule et conditions operatoires optimisees pour les unites traitant des charges riches en paraxylene
CN116850642B (zh) * 2023-05-23 2025-10-31 潍坊弘润石化科技有限公司 一种用于模拟移动床吸附分离的开工系统及方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100285867B1 (en) * 1991-09-05 2001-01-08 Inst Francais Du Petrole Separation method of p-xylene from c8 aromatic hydrocarbons by simulated moving bed adsorption and crystallization and apparatus thereof

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5824308A (ja) * 1981-08-06 1983-02-14 Tanabe Seiyaku Co Ltd 軟質性吸着剤を用いた多段固定床型吸着塔
FR2693186B1 (fr) * 1992-07-06 1994-09-30 Inst Francais Du Petrole Procédé de séparation du paraxylène dans des hydrocarbures aromatiques en C8 avec une adsorption à contre-courant simulé et une cristallisation.
JPH0779927B2 (ja) * 1992-05-22 1995-08-30 川崎重工業株式会社 擬似移動床式液体クロマトオリゴ糖分離装置
FR2757507B1 (fr) * 1996-12-20 1999-01-29 Inst Francais Du Petrole Procede de separation de paraxylene comprenant une adsorption avec injection d'eau et une cristallisation
FR2772634B1 (fr) 1997-12-22 2000-02-18 Inst Francais Du Petrole Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule
FR2795407B1 (fr) * 1999-06-22 2001-10-05 Inst Francais Du Petrole Procede de production d'au moins un isomere des xylenes comprenant une etape d'adsorption et une etape d'isomerisation avec un catalyseur de type structural euo
KR100845665B1 (ko) * 2001-12-18 2008-07-10 유오피 엘엘씨 분별 증류에 의한 흡착 분리 생성물 회수
KR100741750B1 (ko) * 2005-12-26 2007-07-23 삼성토탈 주식회사 로터리 밸브의 스위칭 타임이 비균일한 유사 이동층 흡착 분리 방법
FR2915481B1 (fr) * 2007-04-26 2012-09-21 Inst Francais Du Petrole Procede de production de metaxylene a haute purete comprenant une adsorption en lit mobile simule et une cristallisation
FR2919604B1 (fr) 2007-07-30 2012-09-21 Inst Francais Du Petrole Procede et dispositif de separation ameliore de metaxylene en lit mobile simule
FR2919603B1 (fr) 2007-07-30 2012-09-21 Inst Francais Du Petrole Procede et dispositif de separation ameliore de paraxylene en lit mobile simule
FR2956037B1 (fr) * 2010-02-11 2012-02-17 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule comportant des lignes de derivation d'un lit sur deux avec debits de balayage controles lors des injections et des soutirages
US8841503B2 (en) * 2011-05-26 2014-09-23 Uop Llc Product recovery from adsorption-separation purge fluids
FR2976501B1 (fr) * 2011-06-16 2013-05-31 IFP Energies Nouvelles Procede et dispositif de separation chromatographique a contre-courant simule utilisant deux adsorbeurs en parallele pour la production optimisee de paraxylene.
FR2979252B1 (fr) * 2011-08-26 2013-08-16 IFP Energies Nouvelles Procede et dispositif de production de paraxylene en contre-courant simule a grande flexibilite

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100285867B1 (en) * 1991-09-05 2001-01-08 Inst Francais Du Petrole Separation method of p-xylene from c8 aromatic hydrocarbons by simulated moving bed adsorption and crystallization and apparatus thereof

Also Published As

Publication number Publication date
FR2997396A1 (fr) 2014-05-02
CN103787821B (zh) 2016-09-07
US20140121436A1 (en) 2014-05-01
JP6240466B2 (ja) 2017-11-29
CN103787821A (zh) 2014-05-14
TWI579268B (zh) 2017-04-21
FR2997396B1 (fr) 2015-09-11
TW201422582A (zh) 2014-06-16
KR20140053785A (ko) 2014-05-08
JP2014084323A (ja) 2014-05-12
US9145343B2 (en) 2015-09-29

Similar Documents

Publication Publication Date Title
US9302201B2 (en) Apparatus for conducting simulated countercurrent adsorptive separation of a multi-component feed stream
JP5997946B2 (ja) 最適化されたパラキシレンの製造のための、並列した2基の吸着器を用いる擬似向流クロマト分離のための方法および装置
CN103596654B (zh) 具有低压力降和高区数的模拟逆流色谱分离方法
KR101957521B1 (ko) 파라-크실렌의 시뮬레이팅 역류 생성용 고 유연성 프로세스 및 장치
KR20110093698A (ko) 하나 거른 층마다 우회 라인을 포함하고 주입과 인출 동안 제어된 플러싱 유량을 갖는 모사 이동층 분리를 위한 프로세스 및 장치
US8933288B2 (en) System and process for flushing residual fluid from transfer lines in simulated moving bed adsorption
US20130153500A1 (en) System and process for recovering products using simulated-moving-bed adsorption
US8992779B2 (en) System and process for recovering products using simulated-moving-bed adsorption
US9017558B2 (en) System and process for recovering products using simulated-moving-bed adsorption
KR102095601B1 (ko) 총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치
US20130158335A1 (en) System and process for recovering products using simulated-moving-bed adsorption
US20130153503A1 (en) System and process for recovering products using simulated-moving-bed adsorption
WO2013089920A2 (en) System and process for recovering products using simulated-moving-bed adsorption
US20130153502A1 (en) System and process for recovering products using simulated-moving-bed adsorption
US20130153501A1 (en) System and process for recovering products using simulated-moving-bed adsorption
WO2013089922A1 (en) System and process for recovering products using simulated-moving-bed adsorption
CN110613953A (zh) 具有减少数量的床和旁路流体流动的模拟移动床分离方法与装置
TW202015775A (zh) 具備分流流體之模擬移動床分離方法及裝置

Legal Events

Date Code Title Description
PA0109 Patent application

Patent event code: PA01091R01D

Comment text: Patent Application

Patent event date: 20131024

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20181016

Comment text: Request for Examination of Application

Patent event code: PA02011R01I

Patent event date: 20131024

Comment text: Patent Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20191119

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20200129

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20200325

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20200325

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
PR1001 Payment of annual fee

Payment date: 20230315

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20240312

Start annual number: 5

End annual number: 5