KR102017924B1 - 에스테르교환에 의한 2-옥틸 아크릴레이트의 제조 방법 - Google Patents

에스테르교환에 의한 2-옥틸 아크릴레이트의 제조 방법 Download PDF

Info

Publication number
KR102017924B1
KR102017924B1 KR1020147022795A KR20147022795A KR102017924B1 KR 102017924 B1 KR102017924 B1 KR 102017924B1 KR 1020147022795 A KR1020147022795 A KR 1020147022795A KR 20147022795 A KR20147022795 A KR 20147022795A KR 102017924 B1 KR102017924 B1 KR 102017924B1
Authority
KR
South Korea
Prior art keywords
acrylate
octanol
catalyst
column
stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020147022795A
Other languages
English (en)
Korean (ko)
Other versions
KR20140114880A (ko
Inventor
알랭 리옹드
꼬랄리 그레르
마르끄 에쉬
라인하르트 리네만
Original Assignee
아르끄마 프랑스
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 아르끄마 프랑스 filed Critical 아르끄마 프랑스
Publication of KR20140114880A publication Critical patent/KR20140114880A/ko
Application granted granted Critical
Publication of KR102017924B1 publication Critical patent/KR102017924B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/293—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020147022795A 2012-01-23 2013-01-14 에스테르교환에 의한 2-옥틸 아크릴레이트의 제조 방법 Active KR102017924B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
FR1250607A FR2985999B1 (fr) 2012-01-23 2012-01-23 Procede de production d'acrylate de 2-octyle par transesterification
FR1250607 2012-01-23
FR1256471A FR2986000B1 (fr) 2012-01-23 2012-07-05 Procede de production d'acrylate de 2-octyle par transesterification
FR1256471 2012-07-05
PCT/FR2013/050078 WO2013110876A1 (fr) 2012-01-23 2013-01-14 Procede de production d'acrylate de 2-octyle par transesterification

Publications (2)

Publication Number Publication Date
KR20140114880A KR20140114880A (ko) 2014-09-29
KR102017924B1 true KR102017924B1 (ko) 2019-09-03

Family

ID=46634451

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020147022795A Active KR102017924B1 (ko) 2012-01-23 2013-01-14 에스테르교환에 의한 2-옥틸 아크릴레이트의 제조 방법

Country Status (10)

Country Link
US (1) US9018410B2 (https=)
EP (1) EP2807140B1 (https=)
JP (1) JP6030150B2 (https=)
KR (1) KR102017924B1 (https=)
CN (1) CN104053643B (https=)
BR (1) BR112014017366B1 (https=)
FR (2) FR2985999B1 (https=)
MY (1) MY166181A (https=)
SG (1) SG11201404333SA (https=)
WO (1) WO2013110876A1 (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3032198B1 (fr) * 2015-02-04 2017-01-13 Arkema France Valorisation de produits nobles dans un procede de production d'ester (meth)acrylique.
FR3069538B1 (fr) * 2017-07-25 2020-05-15 Arkema France Procede de purification d'esters (meth)acryliques.

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004529202A (ja) 2001-06-08 2004-09-24 ビーエーエスエフ アクチェンゲゼルシャフト （メタ）アクリル酸エステルの製造方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0466555A (ja) * 1990-07-03 1992-03-02 Mitsubishi Gas Chem Co Inc （メタ）アクリル酸エステルの製造法
JPH11222461A (ja) * 1998-02-02 1999-08-17 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
FR2777561B1 (fr) * 1998-04-21 2000-06-02 Atochem Elf Sa Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle
EP1294658B1 (en) 2000-06-28 2005-03-02 ZAMBON GROUP S.p.A. Process for the preparation of nitroalkenes
DE10200171A1 (de) * 2002-01-04 2003-07-10 Roehm Gmbh Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten
DE10301007A1 (de) * 2003-01-13 2004-07-22 Röhm GmbH & Co. KG Verbessertes Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten mit mehrfacher Katalysatorrezyklierung.
FR2934261B1 (fr) * 2008-07-25 2015-04-10 Arkema France Procede de synthese d'esters de l'acide acrylique

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004529202A (ja) 2001-06-08 2004-09-24 ビーエーエスエフ アクチェンゲゼルシャフト （メタ）アクリル酸エステルの製造方法

Also Published As

Publication number Publication date
US9018410B2 (en) 2015-04-28
CN104053643A (zh) 2014-09-17
SG11201404333SA (en) 2014-10-30
FR2985999B1 (fr) 2014-01-31
FR2986000A1 (fr) 2013-07-26
JP2015504084A (ja) 2015-02-05
FR2985999A1 (fr) 2013-07-26
BR112014017366A2 (pt) 2017-06-13
JP6030150B2 (ja) 2016-11-24
EP2807140A1 (fr) 2014-12-03
BR112014017366B1 (pt) 2020-02-18
MY166181A (en) 2018-06-07
FR2986000B1 (fr) 2014-01-31
EP2807140B1 (fr) 2015-10-28
KR20140114880A (ko) 2014-09-29
WO2013110876A1 (fr) 2013-08-01
US20140371482A1 (en) 2014-12-18
BR112014017366A8 (pt) 2017-07-04
CN104053643B (zh) 2015-12-30

Similar Documents

Publication Publication Date Title
US9403750B2 (en) Method for producing 2-octyl acrylate by direct esterification
CA2761707C (en) The production of n,n-dialkylaminoethyl(meth)acrylates
KR102079840B1 (ko) 알킬 아크릴레이트의 제조 방법
KR19990083363A (ko) 디알킬아미노알킬(메트)아크릴레이트의연속제조방법
US9776946B2 (en) Process for producing 2-propylheptyl acrylate by transesterification
US9296679B2 (en) Method for the production of 2-octyl acrylate by means of transesterification
US20170267624A1 (en) Improved method for producing alkyl (meth)acrylates
KR102017924B1 (ko) 에스테르교환에 의한 2-옥틸 아크릴레이트의 제조 방법
CN1244189A (zh) (甲基)丙烯酸与链烷醇的酯化方法
KR20250161631A (ko) 경질 알킬 아크릴레이트의 정제 방법

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20140814

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20171222

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20190515

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20190816

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20190828

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20190828

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
FPAY Annual fee payment

Payment date: 20220718

Year of fee payment: 4

PR1001 Payment of annual fee

Payment date: 20220718

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20230718

Start annual number: 5

End annual number: 5

PR1001 Payment of annual fee

Payment date: 20240722

Start annual number: 6

End annual number: 6