KR101991705B1 - 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 - Google Patents

발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 Download PDF

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Publication number
KR101991705B1
KR101991705B1 KR1020147006790A KR20147006790A KR101991705B1 KR 101991705 B1 KR101991705 B1 KR 101991705B1 KR 1020147006790 A KR1020147006790 A KR 1020147006790A KR 20147006790 A KR20147006790 A KR 20147006790A KR 101991705 B1 KR101991705 B1 KR 101991705B1
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South Korea
Prior art keywords
solution
succinic acid
mgcl
hcl
magnesium
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Expired - Fee Related
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KR1020147006790A
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English (en)
Korean (ko)
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KR20140064870A (ko
Inventor
한 안드러 바니르 데
브뢰헐 얀 판
데르 베이더 파울뤼스 로뒤비퀴스 요하너스 판
페터르 파울 얀선
란시스 호세 마리아 비달
바로 아구스틴 세르다
Original Assignee
푸락 바이오켐 비.브이.
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Publication of KR20140064870A publication Critical patent/KR20140064870A/ko
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Publication of KR101991705B1 publication Critical patent/KR101991705B1/ko
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/03—Preparation from chlorides
    • C01B7/035—Preparation of hydrogen chloride from chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/02—Magnesia
    • C01F5/06—Magnesia by thermal decomposition of magnesium compounds
    • C01F5/10—Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/26—Magnesium halides
    • C01F5/30—Chlorides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
KR1020147006790A 2011-08-16 2012-08-16 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 Expired - Fee Related KR101991705B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP11177633.2 2011-08-16
EP11177633 2011-08-16
US201161524353P 2011-08-17 2011-08-17
US61/524,353 2011-08-17
PCT/NL2012/050572 WO2013025105A1 (en) 2011-08-16 2012-08-16 Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up

Publications (2)

Publication Number Publication Date
KR20140064870A KR20140064870A (ko) 2014-05-28
KR101991705B1 true KR101991705B1 (ko) 2019-06-21

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Family Applications (1)

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KR1020147006790A Expired - Fee Related KR101991705B1 (ko) 2011-08-16 2012-08-16 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수

Country Status (14)

Country Link
US (1) US9376364B2 (https=)
EP (1) EP2744745B1 (https=)
JP (1) JP6146922B2 (https=)
KR (1) KR101991705B1 (https=)
CN (1) CN103813977A (https=)
AU (1) AU2012295625B2 (https=)
BR (1) BR112014003379A2 (https=)
CA (1) CA2843696C (https=)
EA (1) EA027269B1 (https=)
IN (1) IN2014CN01924A (https=)
PL (1) PL2744745T3 (https=)
UA (1) UA112991C2 (https=)
WO (1) WO2013025105A1 (https=)
ZA (1) ZA201401748B (https=)

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CN103201395B (zh) 2010-06-26 2016-03-02 威尔迪亚有限公司 糖混合物及其生产和使用方法
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
WO2012137201A1 (en) 2011-04-07 2012-10-11 Hcl Cleantech Ltd. Lignocellulose conversion processes and products
EP3845486A1 (en) 2011-08-16 2021-07-07 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up
CN108148027A (zh) * 2011-08-16 2018-06-12 普拉克生化公司 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法
EP2878614A1 (en) 2012-05-03 2015-06-03 Virdia Ltd. Methods for treating lignocellulosic materials
EP2821368A1 (en) * 2013-07-03 2015-01-07 PURAC Biochem BV Method for processing magnesium chloride solutions
US11078548B2 (en) 2015-01-07 2021-08-03 Virdia, Llc Method for producing xylitol by fermentation
BR112017025322A8 (pt) * 2015-05-27 2022-08-23 Virdia Inc Processos integrados para recuperação de hidrolisato celulósico após hidrólise de polpa de celulose
EP3118185A1 (en) * 2015-07-14 2017-01-18 PURAC Biochem BV Method for manufacturing succinic acid
EP3124434A1 (en) * 2015-07-31 2017-02-01 PURAC Biochem BV Method for providing a succinic acid solution
BR112018014591B1 (pt) * 2016-01-19 2023-04-25 Purac Biochem Bv Método para processamento de soluções de cloreto de magnésio e para fabricação de ácidos carboxílicos
JP7053506B2 (ja) 2016-06-29 2022-04-12 ベーリンゲ、イノベイション、アクチボラグ タングを挿入するための方法及び装置
CN114906812B (zh) * 2022-06-01 2023-06-23 湖南吴赣药业有限公司 一种有机混酸分离纯化方法
WO2024097329A1 (en) 2022-11-02 2024-05-10 Amalgamated Research Llc Smb separator for organic acid purification using a strong acid cation resin

Citations (2)

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WO2000017378A2 (en) 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
JP2009079057A (ja) 2005-04-22 2009-04-16 Mitsubishi Chemicals Corp ポリエステル及びその製造方法

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BE548967A (https=) 1954-12-08 1956-07-14
GB9102393D0 (en) 1991-02-05 1991-03-20 Ici Plc Production of terephthalic acid
AUPP437698A0 (en) * 1998-06-30 1998-07-23 Baumgart, Karl Methods for treatment of coronary, carotid and other vascular disease
US6670505B1 (en) 2000-03-07 2003-12-30 Eastman Chemical Company Process for the recovery of organic acids from aqueous solutions
US6660505B2 (en) 2000-06-22 2003-12-09 Cognis Corporation Isolation of carboxylic acids from fermentation broth
CN100534972C (zh) * 2003-09-30 2009-09-02 味之素株式会社 从发酵液中纯化琥珀酸的方法
US20080223519A1 (en) 2006-12-06 2008-09-18 Locko George A Polyamide polyols and polyurethanes, methods for making and using, and products made therefrom
FR2925068B1 (fr) * 2007-12-13 2010-01-08 Roquette Freres Procedes de production d'acide succinique
CN101550079B (zh) * 2009-05-12 2010-10-27 安徽丰原发酵技术工程研究有限公司 一种连续制备丁二酸的方法
KR101051582B1 (ko) 2009-05-13 2011-07-22 삼성석유화학(주) 발효액으로부터 숙신산을 분리 및 정제하는 방법
US8431372B2 (en) * 2009-06-19 2013-04-30 Mbi International Fermentation method using a magnesium compound containing oxygen
CN101748161B (zh) * 2010-01-19 2012-06-06 南京工业大学 一种厌氧发酵纯化丁二酸的工艺
EP3845486A1 (en) 2011-08-16 2021-07-07 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up

Patent Citations (2)

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Publication number Priority date Publication date Assignee Title
WO2000017378A2 (en) 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
JP2009079057A (ja) 2005-04-22 2009-04-16 Mitsubishi Chemicals Corp ポリエステル及びその製造方法

Also Published As

Publication number Publication date
PL2744745T3 (pl) 2020-05-18
AU2012295625B2 (en) 2016-05-12
JP6146922B2 (ja) 2017-06-14
CN103813977A (zh) 2014-05-21
EA027269B1 (ru) 2017-07-31
JP2014524254A (ja) 2014-09-22
EP2744745B1 (en) 2019-10-30
CA2843696A1 (en) 2013-02-21
KR20140064870A (ko) 2014-05-28
WO2013025105A8 (en) 2014-04-10
US20140200365A1 (en) 2014-07-17
EA201490408A1 (ru) 2014-07-30
IN2014CN01924A (https=) 2015-05-29
US9376364B2 (en) 2016-06-28
BR112014003379A2 (pt) 2017-03-01
EP2744745A1 (en) 2014-06-25
UA112991C2 (uk) 2016-11-25
CA2843696C (en) 2019-09-24
AU2012295625A1 (en) 2014-03-20
ZA201401748B (en) 2015-01-28
WO2013025105A1 (en) 2013-02-21

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