KR101961476B1 - Manufacturing method of natural composition contained natural minerals and saururus chinensis, and natural composition therefrom - Google Patents

Abstract

The present invention relates to a method of preparing a natural composition including natural minerals and Saururus chinensis. The method comprises: a step (S1) performed by a step (S1a) in which 31-37 parts by weight of germanium, 14-20 parts by weight of diatomite, 1-3 parts by weight of platinum, 19-25 parts by weight of zeolite, and 10-15 parts by weight of loess are mixed and pulverized, and a step (S1b) in which natural mineral solution is prepared by mixing and stirring the pulverized natural minerals obtained in the step (S1a) with purified water; a step (S2) of mixing 1 kg of dried Saururus chinensis powder with 1,000 ml of purified water in order to prepare a natural antibacterial solution; a step (S3) of mixing 85-95 wt% of the natural mineral solution obtained in the step (S1) with 5-15 wt% of the natural antibacterial solution obtained in the step (S2) in a stirring device; and a step (S4) of fermenting the mixed material obtained in the step (S3) by an aging process while rotating the mixed material. According to the present invention, the natural composition is prepared by mixing the natural mineral materials with vegetable raw materials, thereby being harmless to the human body and preventing environmental pollution.

Description

TECHNICAL FIELD The present invention relates to a natural composition containing natural minerals and saururus chinensis, and a natural composition prepared by the same. BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a natural composition,

The present invention relates to a method for producing a natural composition comprising natural minerals and Saururus chinensis, and to a natural composition produced thereby. More particularly, to a technique of mixing a solution of natural minerals containing germanium, diatomaceous earth, platinum, zeolite and loess with a solution of saururus and fermentation by aging.

As the environmental pollution becomes more and more serious in modern life, various kinds of rooms, internal and external air pollution sources are directly or indirectly damaged, and personal diseases caused by moisture are becoming serious. A deodorant or a dehumidifying agent is used to remove or reduce such a pollution source. Most of the conventional deodorant, dehumidifier, and fragrance are chemically synthesized or used by using charcoal or the like to process environmentally harmful or environmentally friendly materials. Thus, the dehumidifying agent, the fragrance agent, and the deodorant, which are the main components of the chemical component, are harmful to the human body and cause environmental pollution.

Accordingly, natural minerals have been proposed as materials that are harmless to the human body and prevent environmental pollution. In general, natural minerals are powerful dehumidifying, deodorizing and antibacterial air purifying agents that simultaneously solve moisture and odor antimicrobial problems. These natural minerals are natural mineral materials that emit far-infrared rays and can function to purify polluted environment space by decomposing bad odor, moisture and bacteria in the air.

Natural minerals are materials made by activating the nano-scale pores by selecting the lightest layer of the far-infrared ray out of the stratum of the clean area. In particular, they contain a large amount of aluminum oxide (Al ₂ O ₃ ) and calcium oxide (CaO). As a result, the adsorption power is stronger than that of the other products, and the decomposition ability of the malodor is excellent, and it is possible to decompose even the cause of the odor, thereby preventing the odor from being generated again.

Conventional volcanic rocks were the main component of SiO ₂ , which only had a large effect on dehumidification. However, natural minerals are getting a lot of attention because they release odor and odor as well as decompose carbon monoxide by far-infrared radiation and help air purification.

Accordingly, an eco-friendly deodorization and dehumidifying agent has been developed. Korean Patent Laid-Open Publication No. 10-2012-0026260 discloses a microbial deodorization and dehumidifying agent using opal and diatomaceous earth. Korean Patent Registration No. 10-0636825 Mud, charcoal, bentonite, cornstarch, and starch are mixed in a mortar.

However, although the above-mentioned prior art is biodegradable including starch, other physical properties such as hardness and strength shaping property are lowered and only a specific component of a polymer is used.

(Document 1) Korean Published Patent Application No. 10-2012-0026260 (March 19, 2012) (Document 2) Korean Patent Registration No. 10-0636825 (Oct. 13, 2006)

The natural composition and the natural composition comprising the natural mineral and the Saururus chinensis according to the present invention have the following problems.

First, it is intended to provide a composition for mixing a natural mineral material and a vegetable raw material.

Second, it is intended to provide a composition excellent in natural antibacterial, deodorizing, dehumidifying, and far-infrared ray releasing functions.

Third, the implementation is suitable for automation process.

The solution of the present invention is not limited to those mentioned above, and other solutions not mentioned can be clearly understood by those skilled in the art from the following description.

The present invention relates to a method for producing a natural composition comprising natural minerals and saururus chinensis comprising 31 to 37 parts by weight of germanium, 14 to 20 parts by weight of diatomaceous earth, 1 to 3 parts by weight of platinum, 19 to 25 parts by weight of zeolite and 10 to 15 parts by weight of loess Mixing the natural minerals with the purified water, and mixing the natural minerals with the purified water, and mixing the natural minerals with the purified water to obtain a natural mineral solution; Step S2: mixing 1 kg of the dried powder of Saururus chinensis with 1000 ml of purified water and making the solution soluble to prepare a natural antibacterial solution; Step S3 of mixing 85 to 95% by weight of the natural mineral solution in step S1 and 5 to 15% by weight of the natural antibacterial solution in step S2 into a stirrer; And S4 in order to allow the fermentation by aging to proceed while rotating the mixture of step S3.

In the step S1a of the present invention, the natural mineral may be pulverized into a powder of 1,000 to 3,500 mesh by a dry process using an air impact pulverizer.

In the stirring step of step S1b according to the present invention, the mixing and stirring temperature is preferably 38 ° C to 45 ° C.

In the grinding step of step S2 according to the present invention, the above-mentioned three hundred seconds may be pulverized into a powder of 150 mesh.

In the lyophilizing process of step S2 according to the present invention, the natural antimicrobial solution can be obtained by filtering and separating the precipitate after boiling in the state of maintaining the temperature of 20 to 45 DEG C in the above-mentioned three hundred seconds of the mixed water.

The fermentation process of step S4 according to the present invention can naturally ferment the mixture of step S3 while rotating at room temperature.

The present invention is a natural composition, preferably a natural composition comprising natural minerals and saururus prepared according to the method of the present invention.

The natural composition and the natural composition comprising the natural mineral and Saururus chinensis according to the present invention have the following effects.

First, it is a natural composition for mixing a natural mineral material and a vegetable raw material, and is harmless to the human body and has an effect of preventing environmental pollution.

Second, there is an excellent effect of natural antimicrobial, deodorizing, dehumidifying, and far-infrared radiation.

Third, there is an effect that it can be easily implemented in an automated process.

The effects of the present invention are not limited to those mentioned above, and other effects not mentioned can be clearly understood by those skilled in the art from the following description.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a flowchart showing a method for producing a natural composition containing natural minerals and Saururus chinensis according to the present invention.

Hereinafter, embodiments of the present invention will be described with reference to the accompanying drawings so that those skilled in the art can easily carry out the present invention. It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit or scope of the invention. Wherever possible, the same or similar parts are denoted using the same reference numerals in the drawings.

The terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. The singular forms as used herein include plural forms as long as the phrases do not expressly express the opposite meaning thereto.

Means that a particular feature, region, integer, step, operation, element and / or component is specified and that other specific features, regions, integers, steps, operations, elements, components, and / It does not exclude the existence or addition of a group.

All terms including technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. Predefined terms are further interpreted as having a meaning consistent with the relevant technical literature and the present disclosure, and are not to be construed as ideal or very formal meanings unless defined otherwise.

In order to facilitate the description of the features of the present invention, it should be understood that the drawings may be exaggerated in some cases, or only necessary portions may be extracted and shown. That is, the drawings are merely a means for easily expressing the technical feature of the present invention, and the technical composition of the present invention is not necessarily interpreted as shown in the drawings.

Hereinafter, the present invention will be described with reference to the drawings. BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a flowchart showing a method for producing a natural composition containing natural minerals and Saururus chinensis according to the present invention.

The step S1 of the present invention is a step of S1a mixing and pulverizing 31 to 37 parts by weight of germanium, 14 to 20 parts by weight of diatomaceous earth, 1 to 3 parts by weight of platinum, 19 to 25 parts by weight of zeolite and 10 to 15 parts by weight of loess, And mixing the natural minerals in step S1a with purified water and stirring the resultant mixture to provide a natural mineral solution.

The reason for limiting the content of each natural mineral composition according to step S1a will be described below.

germanium( Ge ) 31 ~ 37 Weight portion

Germanium (Ge) is an off-white mineral, composed of 32 electrons. When a foreign object comes into contact with one of the four outermost electrons, it combines with the electrons of the foreign substance and attracts the foreign substance into the vacant space. give. At this time, pure oxygen is generated to neutralize, neutralize and neutralize contaminants that are acidified by neutralizing, neutralizing, or eliminating the action, converting it into an alkali substance, and combining it with heavy metals to produce other toxic substances. Also, due to its semiconducting properties, the synergistic effect when used with the mixture of the present invention can improve the effects of negative ion emission and far-infrared radiation. In the present invention, it is preferable to use high purity inorganic germanium of 99.999% in order to secure the safety of the solution.

 If the content of germanium is less than 31 parts by weight, there is a problem that the far-infrared radiation effect is lowered and the antibacterial property is reduced, so that it is difficult to sufficiently exhibit its function. If the content of germanium is more than 37 parts by weight, there is a problem that the increase in far-infrared radiation energy and the antimicrobial effect do not show a synergistic effect.

Therefore, the content of germanium according to the present invention is preferably 31 to 37 parts by weight. More preferably, the germanium content may be 32 to 35 parts by weight.

Diatomaceous earth 14 ~ 20 Weight portion

Diatomaceous earth (SiO ₂ ) is a mineral material composed of silicate wastes (diatomaceous earth) of unicellular algae deposited on the bottom of the sea or lake, and more than 90% of it is made of amorphous silica (SiO ₂ ) It is a physicochemically stable inorganic material. It has numerous small pores on its surface, maximizes its surface area, is lightweight, has excellent hygroscopicity and heat insulation, and can be applied as a plastic insulation material. In addition, diatomaceous earth is capable of adsorbing and filtering harmful substances in the air, filtering out impurities in the room air, and emitting far infrared rays deeply inside the body, thereby facilitating the metabolism of the human body. In addition, a large amount of porous structure of the diatomaceous earth absorbs moisture when it is humid, and diverges when it is dried, so that the human absorbs moisture and diverges repeatedly while sleeping, It absorbs various pollutants and protects the human body from harmful electromagnetic waves.

If the content of the diatomaceous earth is less than 14 parts by weight, there is a problem that the moisture absorption and moisture proofing ability can be exhibited properly. If the content of the diatomite exceeds 20 parts by weight, there is a problem that the manufacturing cost increases and the moisture absorption and moisture-proofing ability are deteriorated.

Therefore, the content of the diatomite according to the present invention is preferably 14 to 20 parts by weight. More preferably, the diatomaceous earth content may be 16 to 18 parts by weight.

Platinum 1 ~ 3 Weight portion

Platinum (Pt) is a silvery silver-silver alloy that is harder than silver and has a good ductility and ductility. It is very stable in air and moisture and does not change even when heated to high temperature. It is very strong in acid and alkali and has excellent corrosion resistance and abrasion resistance among all metals. Do. Platinum is the safest of the existing metal materials and has no oxidation phenomenon. It is harmless to the human body, has antibacterial effect against all viruses, has catalytic function, deodorizing function, and has excellent ability to decompose carbon monoxide and volatile organic compounds. Persistence is also permanent and has the effect of emitting far infrared rays.

If the content of platinum is less than 1 part by weight, the critical trapping rate is insufficient and the active antibacterial performance is deteriorated. If the content of platinum is more than 3 parts by weight, the control effect of active antimicrobial is remarkably reduced by half, and the manufacturing cost is increased.

Therefore, the content of platinum according to the present invention is preferably 1 to 3 parts by weight.

Zeolite 19-25 Weight portion

Zeolite is a porous material formed by the action of the volcanic ash of the third layer, which is a porous material with excellent adsorption capacity and chemical cation exchange function. It is used for removal and purification of automobile noxious gas components, various heavy metal detoxifiers, gas adsorption and deodorizers, It is a minerals that is used as a catalyst for environmental purification as a land improvement agent. The zeolite is a type of aluminosilicate mineral that is connected in three dimensions to molecular-sized cavities consisting of tetrahedral TO ₄ (T is tetrahedral atom Si or Al) to form a molecular-sized channel. It causes reversible adsorption / desorption of water molecules in the pupil. There are about 40 kinds of natural zeolite and about 130 kinds of synthetic zeolite. The zeolite used in the present invention is not particularly limited, and any known zeolite may be used.

If the zeolite content is less than 19 parts by weight, the deodorizing performance of the zeolite component properties is reduced. If the zeolite content exceeds 25 parts by weight, there is a problem that the effect of improving the deodorizing performance is not further increased, and further, the process and cost efficiency are further reduced.

Accordingly, the content of the zeolite according to the present invention is preferably 19 to 25 parts by weight. More preferably, the zeolite content may be 16 to 18 parts by weight.

Loess 10-15 Weight portion

Yellow loam is a material consisting of silica and soil containing hydrous iron oxide and anhydrous iron oxide, and means sediments composed mainly of silt-sized particles having a diameter of 0.002 to 0.005 mm. The main components of the loess are silica, iron powder, alumina, magnesium, sodium, calcium carbonate and lime. The above-mentioned loess has a large amount of far-infrared rays for shielding electromagnetic waves, and has effects such as humidity control, antibacterial and detoxification.

When the content of the loess is less than 10 parts by weight, the amount of the loess is too small and it is difficult to sufficiently exhibit the functions of the loess such as the far-infrared radiation power, the self-tacking power and the deodorant power. If the content of the loess exceeds 15 parts by weight, there is a problem that the effect of removing the offensive odor and harmful substances by the loess is not increased any more.

Accordingly, the content of the loess according to the present invention is preferably 10 to 15 parts by weight. More preferably from 13 to 15 parts by weight.

Next, the grinding step of step S1a according to the present invention will be described.

In the step S1a according to the present invention, it is preferable that the natural mineral is pulverized into a powder of 1,000 to 3,500 mesh by a dry method using an air impact pulverizer.

Mineral material grinding is classified into grinding, heavy chain, grinding, fine grinding, and ultrafine grinding depending on the size of the desired grinding particles by mechanically manipulating the material by applying external force to subdivide it into smaller sizes and increasing the surface area. The pulverization method of the pulverizer can be pulverized using a ball mill, a rod mill, a roller mill, a Wheeler mill, and a dry air flow impact mill.

In the present invention, in order to further increase the elution efficiency with respect to the main component of the mineral material, the powder is dry-pulverized to a super-fine size due to collision between powders, and the pulverization is carried out by controlling the size of ultrafine particles The surface area was increased by pulverizing the mineral material with ultrafine particles using a dry airflow impact mill. Such a dry milling method has an effect of improving the elution of the main component of the mineral material.

Next, step S1b according to the present invention will be described. In the step S1b according to the present invention, the natural minerals in step S1a may be mixed with purified water and stirred to provide a natural mineral solution. Further, in the stirring step of step S 1 b, the mixing and stirring temperature is preferably 38 ° C to 45 ° C.

In step S1b of the present invention, the pulverized mineral powders are mixed with purified water and mixed in a low-speed stirrer for 5 to 30 days at room temperature, thereby alleviating aggregation of mineral powders, It is a step of homogenizing to maximize fluidity.

However, when a mixture of a trace amount of a substance such as platinum and a mineral having a high total content ratio, such as germanium, zeolite, diatomaceous earth, and loess, is mixed and stirred or mixed in the mixture, the concentration is locally biased in general.

In order to solve such a problem, Mixing and stirring in an internal temperature range of 38 ° C to 45 ° C to obtain a composition in which all the particles are uniform in composition as a whole and the functional ingredient is saturated and dissolved without breaking the original mineral properties.

If the mixing and stirring temperature is less than 38 占 폚, mineral aggregation may occur. In addition, there is a problem that the silicon dioxide component, which is the main component of germanium minerals, is not properly dissolved and the far-infrared far-infrared ray emissivity and radiant energy are reduced, and the component properties of the mineral materials are not eluted properly.

If the mixing and stirring temperature exceeds 45 ° C, iron and manganese oxides having a large specific surface area and high cation exchange ability among the yellow coal minerals constituting components are destroyed and the ability of adsorbing harmful substances is reduced. Diatomaceous earth is a material composed of a siliceous shell of a single-celled plant and is highly hygroscopic due to its porosity. Such a silicon dioxide component, which is a main component of diatomaceous earth, has a problem that the destruction porous property is decreased and the moisture absorption ability is decreased.

Therefore, the mixing and stirring temperature of the step S1b according to the present invention is such that the composition can be prepared without destroying the properties of the respective minerals when the composition is mixed and stirred at 38 ° C to 45 ° C. Application of such a composition to a variety of products makes it possible to exhibit natural antimicrobial, far-infrared emissivity, deodorization, removal of harmful substances, and no change in target values for dehumidification capability.

Next, step S2 according to the present invention will be described. Step S2 does not necessarily mean that the process of step S1 is performed. That is, it may be performed simultaneously, S2 may be performed in advance, or may be performed in succession. This is because it is sufficient to mix the result of step S1 and the result of step S2 in step S3.

In step S2 according to the present invention, it is preferable that 1 Kg of Saururus chinensis powder is mixed with 1000 ml of purified water and then dissolved in a solution to provide a natural antibacterial solution.

In the milling process of the S2 step, the millbase can be pulverized into a powder of 150 mesh. In the present invention, the plant material Saururus chinensis is dried and can be pulverized into 150 mesh powder using an ultra high-speed blender or the like.

In the solubilization step of step S2, it is preferable to collect the natural antimicrobial solution by filtering and separating the sediment after the water bath in a state where the above-mentioned three-hundred second water mixture water is maintained at a temperature of 20 to 45 캜.

In the solubilization step S2, 1 kg of powdered saururus powder is mixed with 1000 ml of purified water, and then the elution of the active ingredient of the solution is accelerated in a constant temperature water bath. The appropriate temperature for maintaining the elution time is maintained at 20 ° C to 45 ° C, The mixture is heated for 12 to 24 hours, filtered through a filter paper or the like to produce a plant solution.

Next, step S3 of the present invention will be described. Step S3 according to the present invention is characterized in that 85 to 95% by weight of the natural mineral solution in Step S1 and 5 to 15% by weight of the natural antibacterial solution in Step S2 are mixed in a stirrer.

The reason for mixing vegetable raw materials with natural mineral solutions is that Saururus chinensis is currently used for medicinal purposes and has the effect of inhibiting the growth of antibacterial, Staphylococcus aureus and typhoid bacteria. That is, a vegetable solution was added to increase the antimicrobial activity of the natural mineral solution.

In addition, due to the far - infrared radiation energy of the natural mineral solution, the mycelia of organic matter, which is an organic matter, were sufficiently fermented, and the antimicrobial efficacy was improved by improving the elution of the antibacterial component.

Furthermore, when the solution is adsorbed uniformly on the porous inorganic particles of the natural mineral solution component, the antibacterial component of the organic matter, Saururus chinensis, can be displayed for a long period of time.

Next, step S4 of the present invention will be described. In the step S4 according to the present invention, fermentation by aging is progressed while rotating the mixture of step S3. Also, The aging step in step S4 is characterized in that the mixture in step S3 is spontaneously fermented while being rotated at room temperature.

In the step S4 according to the present invention, it is preferable that fermentation by aging proceeds while the mixture of step S3 is rotated. In step S3, 85 to 95% by weight of the prepared natural mineral solution and 5 to 15% by weight of the natural vegetable antibacterial solution were mixed in a stirrer to form a mixture. In step S4, the mixture was allowed to ferment at a high temperature while rotating at a high temperature, for example, aging for 45 to 60 days. That is, in step S4, the natural fermentation of the components of the mineral powder is performed.

On the other hand, the present invention includes a natural composition comprising natural minerals and Saururus chinensis prepared according to the above-described manufacturing method.

[ Example ]

First, a natural mineral material is prepared by mixing 34 parts by weight of germanium as a natural mineral material, 17 parts by weight of diatomaceous earth, 2 parts by weight of platinum, 22 parts by weight of zeolite and 15 parts by weight of loess. Also, the natural mineral material was pulverized to prepare a natural mineral material powder having a particle size of 1,000 to 3,500 mesh.

To a reaction vessel equipped with a stirrer, 4,000 ml of purified water was added to 2,000 ml of the natural mineral material powder, and the mixture was stirred. At this time, 1,500 ml of natural mineral solution was prepared by mixing with a low speed stirrer at an internal temperature of 25 ° C to 45 ° C for 5 to 30 days.

1 kg of dried Saururus chinensis was crushed into 150 mesh and then mixed with 1,000 ml of purified water. After maintaining the temperature of the incubation tank at 20 ° C to 45 ° C for 12 to 24 hours, the precipitate was filtered with a filter paper, do. The solution is homogenized by high-speed stirring using a centrifuge, and 100 ml of the supernatant is separated from the precipitate.

1,500 ml of the solution of the natural mineral material and 100 ml of the natural vegetable antibacterial solution were simultaneously introduced into a reaction vessel equipped with a stirrer. At this time, while maintaining the internal temperature of the mixing bath at 25 ° C to 45 ° C, the stirrer is rotated for 50 days to uniformly mix. As a result, the final product was completed.

[ Application example ]

1000 g of the natural composition prepared according to the present invention and 60 g of polyester fabric are prepared. A stainless steel immersion tank to which an electric device is attached is prepared so that the natural composition stably adsorbs to the raw air gap. After the natural composition is filled in the immersion tank, the temperature in the immersion tank is maintained at 25 ° C or more and 40 ° C or less.

The polyester fabric is soaked in the immersion tank such that the natural composition is adsorbed to the polyester fabric. In this case, the polyester fabric dipping time is set to be 30 minutes or less so that the natural composition can stably penetrate evenly between the yarn constituting the polyester fabric and the yarn in a state where the temperature of the natural composition is maintained at 25 ° C to 40 ° C It is immersed within 40 minutes.

Also, the immersion tank temperature is within 25 占 폚 to 40 占 폚 in order that the natural composition can uniformly and stably adsorb the internal voids from the surface of the polyester fabric through the gap. The polyester fabric immersed in the natural composition is dewatered for 1 minute using a dehydrator.

The surface of the polyester fabric on which the natural composition is adsorbed is dried and cooled using hot air. In addition, the composition is stably fixed using an electric warm dryer at 20 ° C to 40 ° C so that the components of the permeation composition penetrating between the yarn constituting the polyester fabric and the yarn can be completely fixed to the polyester fabric.

[ Comparative Example ]

The natural composition extracted according to the present invention was tested for animal safety through animal testing, and applied to polyester fabric to test antibacterial, deodorization and efficacy against far-infrared emissivity.

1. Human safety inspection of functional natural composition

The safety test of the solution was carried out in accordance with the Toxicological Standards of Pharmaceuticals and Notification No. 2009-19 (May 1, 2009) of the Korean Food and Drug Administration Notification No. 2005-60 (October 21, 2005) (CBS-SOP-ACO) of the OECD Test Guideline (No. 420) and the Biosafety Center Standard Work Guideline (CBS-SOP-ACO).

The above test was conducted in order to examine the toxicity of the composition extracted from the above in a single oral administration to 5 male and 5 female Sprague-Dawley (SD) Daily mortality, general symptoms, weight change and autopsy findings were observed.

The test weight and weight range are 7 weeks for male and 7 weeks for male, 13 for female, 13 for male, and 157.1 ~ 173.1g for female and 201.9 ~ 217.7g for male, respectively. At 8 weeks of age and at the start of administration, the number of animals was 8 weeks for each male and female at the start of administration, and the number of animals was 10 for male and 172.1 ~ 179.9g for females and 226.2 ~ 240.7g for males.

The composition and dosage of the test group were grouped by the random method after measuring the weight before the start of administration, and the result of the limit test confirmed that there was no test system that died at 2 ml / kg of test substance and 5 ml / kg of test substance .

The dose of the test substance was administered at a dose of 5 ml / kg once / day based on the body weight measured on the day of administration (see Table 1).

The toxicity index of the test group was compared with the control group through the ANOVA test using the statistical method SPSS 14.OK.

  As a result of the test, no dead animal was observed during the entire period of the test, and no abnormal symptoms related to administration of the test substance were observed even in general symptoms. In addition, there was no significant difference between male and female control group and test group during autopsy. There was no significant difference between test group and control group in male and female.

  As a result of observing the mortality rate, general symptoms, weight change and autopsy findings due to toxic indicators caused by single oral administration of the test substance in the test in the above test, abnormal symptoms and abnormal lesions were not found or confirmed, It was confirmed that the composition was confirmed to have safety.

2. Composition Efficacy  evaluation

 ① Antimicrobial activity test

 The test for antibacterial activity was carried out according to the test method of KS K0693: 2011. Staphylococcus aureus ATCC 6538 and Klebsiella pneumoniae ATCC 4532 were used in the antimicrobial activity test, 0.05% nonionic surfactant was used in the inoculum, and the standard cloth was attached with cotton for KS K 0905 dyeing fastness. As a sample, 0.4 g of polyester fabric immersed in a natural composition was used.

 As shown in Table 2, it was confirmed that the antibacterial activity of the polyester fabric adsorbed on the natural composition within the preferred range of the present invention was 99.9%.

Thus, it can be seen that the natural composition according to the present invention is not harmful to health because there is no difference in antibacterial activity between the organic antibacterial agent used for imparting the antibacterial power to the absorbed fabric.

② Deodorization test

The deodorization test was carried out by injecting 500 ppm of ammonia gas into a deodorizing container (5 liters) according to the test method of KFIA-FI-1004.

 As shown in Table 3, it can be seen that, in the polyester fabric mixed with the natural composition within the preferable range of the invention, there is a deodorizing effect of decomposing odor and bad smell with time. Therefore, it can be seen that the deodorizing effect according to the embodiment is excellent.

  ③ far infrared emissivity test

  The radiant energy was measured using a FT-IR spectrometer at a sample size of 3 cm × 3 cm and a temperature of 37 ° C. according to the KFIA-FI-1005 test method.

As shown in Table 4, in the case of the polyester fabric adsorbed with the natural composition within the preferable range of the invention, far-infrared ray emissivity and far-infrared radiation energy are emitted. In particular, it can be seen that after the natural composition is adsorbed, the radiant energy at the fabric is more increased to 3.41 × 10⁴ W / m2 · ㎛.

On the other hand, before the natural composition is adsorbed, it can be seen that the radiant energy is as low as 3.25 10 4 W / m 2 m.

Therefore, the far infrared ray radiated energy of the absorbed raw material of the natural composition according to the embodiment is much emitted, so that the warmth penetrates directly into the body to promote blood circulation, thereby warming the body and improving the odor It can be seen that the effect of purifying is excellent.

As shown in the above experimental results, it was confirmed that the composition of the present invention has not only remarkable effects on natural antimicrobial, deodorizing, dehumidifying, far-infrared ray emitting function, but also human safety.

As described above, the present invention provides a functional natural composition having an effect on natural antibacterial, deodorizing, dehumidifying and far-infrared ray releasing functions, and a pharmaceutical composition containing the functional natural composition.

④ Heavy metal detection confirmation test

The heavy metal detection test on the natural composition was carried out on a polyester fabric by proceeding the processing of immersion and drying of the natural composition with the following measurement standards.

For the detection of heavy metals, the sample pretreatment was measured by EPA 3052: 1996 for Cd, Pb, Hg and EPA 3060: 1996 for CrVl. The analyzing instruments were Cd, Pb, Hg for lCP / AES, CrVl for UV / VlS was used

As shown in Table 5, it was confirmed that the natural composition contained no heavy metals in the natural composition.

Therefore, it can be seen that the natural composition according to the examples is harmless to the human body since it does not contain a heavy metal harmful to the human body .

⑤Deep test

The dehumidifying power test for the natural composition was carried out by processing the natural composition on the polyester fabric by the above immersion and drying process and then by the following test method in the Department of Health and Biotechnology of Kyungwoon University in Gumi City, Table 6 confirms.

The humidity was adjusted to 80% using a humidifier in a 30 cm x 30 cm x 30 cm transparent box. Then, a fabric having a size of 8 cm x 0.1 cm was dipped into a polyester fabric dipped and dried with a hygrometer and a natural composition, the box was sealed, and humidity change was measured with time.

As shown in Table 6, it can be seen that the polyester fabric mixed with the natural composition within the preferred range of the present invention has an effect of removing moisture as time elapses.

The embodiments and the accompanying drawings described in the present specification are merely illustrative of some of the technical ideas included in the present invention. Accordingly, the embodiments disclosed herein are for the purpose of describing rather than limiting the technical spirit of the present invention, and it is apparent that the scope of the technical idea of the present invention is not limited by these embodiments. It will be understood by those of ordinary skill in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (7)

31 to 37 parts by weight of germanium, 14 to 20 parts by weight of diatomaceous earth, 1 to 3 parts by weight of platinum, 19 to 25 parts by weight of zeolite and 10 to 15 parts by weight of loess, And S1b comprising the step of mixing and stirring with purified water to provide a natural mineral solution;
Step S2: mixing 1 kg of the dried powder of Saururus chinensis with 1000 ml of purified water and making the solution soluble to prepare a natural antibacterial solution;
Step S3 of mixing 85 to 95% by weight of the natural mineral solution in step S1 and 5 to 15% by weight of the natural antibacterial solution in step S2 into a stirrer; And
And (S4) allowing the fermentation by aging to proceed while rotating the mixture of step (S3). The method according to claim 1,
Wherein the natural mineral is pulverized into a powder of 1,000 to 3,500 mesh by a dry method using an air impact pulverizer in the step of pulverizing the natural mineral in step S1a. The method according to claim 1,
Wherein the temperature of mixing and stirring in the stirring step of step S1b is 38 ° C to 45 ° C. The method according to claim 1,
Characterized in that in the milling step of step S2, the three hundred milligrams are ground into a powder of 150 mesh. The method according to claim 1,
In the step of lyophilizing in step S2, the water of the three hundred seconds of the mixture is maintained at a temperature of 20 to 45 DEG C, and the precipitate is filtered and separated to obtain a natural antimicrobial solution. ≪ / RTI > The method according to claim 1,
Wherein the aging step of step S4 is a step of spontaneously fermenting the mixture of step S3 while rotating the mixture at room temperature. A natural composition comprising natural minerals and Saururus chinensis prepared according to the method of any one of claims 1 to 6.

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