KR101744362B1 - １급 히드록실 말단 기를 포함하는 폴리에테르 폴리올의 제조 방법 - Google Patents

１급 히드록실 말단 기를 포함하는 폴리에테르 폴리올의 제조 방법 Download PDF

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KR101744362B1
KR101744362B1 KR1020127000005A KR20127000005A KR101744362B1 KR 101744362 B1 KR101744362 B1 KR 101744362B1 KR 1020127000005 A KR1020127000005 A KR 1020127000005A KR 20127000005 A KR20127000005 A KR 20127000005A KR 101744362 B1 KR101744362 B1 KR 101744362B1
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hydrogen
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aryl
alkyl
koh
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KR20120095338A (ko
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하르트무트 네프츠거
에리카 바우어
외르크 호프만
클라우스 로렌츠
노르베르트 한
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코베스트로 도이칠란드 아게
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4887—Polyethers containing carboxylic ester groups derived from carboxylic acids other than acids of higher fatty oils or other than resin acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/67—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids
    • C07C69/708—Ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/73—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
    • C07C69/734—Ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/74—Esters of carboxylic acids having an esterified carboxyl group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C69/757—Esters of carboxylic acids having an esterified carboxyl group bound to a carbon atom of a ring other than a six-membered aromatic ring having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • C07C69/82—Terephthalic acid esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2615—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen the other compounds containing carboxylic acid, ester or anhydride groups
    • C—CHEMISTRY; METALLURGY
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    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C08G65/2672—Nitrogen or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/329—Polymers modified by chemical after-treatment with organic compounds
    • C08G65/331—Polymers modified by chemical after-treatment with organic compounds containing oxygen
    • C08G65/332—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof
    • C08G65/3324—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof cyclic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/329—Polymers modified by chemical after-treatment with organic compounds
    • C08G65/331—Polymers modified by chemical after-treatment with organic compounds containing oxygen
    • C08G65/332—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof
    • C08G65/3324—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof cyclic
    • C08G65/3326—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof cyclic aromatic

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
KR1020127000005A 2009-07-03 2010-06-30 １급 히드록실 말단 기를 포함하는 폴리에테르 폴리올의 제조 방법 Expired - Fee Related KR101744362B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE200910031584 DE102009031584A1 (de) 2009-07-03 2009-07-03 Verfahren zur Herstellung von Polyetherpolyolen mit primären Hydroxyl-Endgruppen
DE102009031584.5 2009-07-03
PCT/EP2010/003958 WO2011000560A1 (de) 2009-07-03 2010-06-30 Verfahren zur herstellung von polyetherpolyolen mit primären hydroxyl-endgruppen

Publications (2)

Publication Number Publication Date
KR20120095338A KR20120095338A (ko) 2012-08-28
KR101744362B1 true KR101744362B1 (ko) 2017-06-07

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KR1020127000005A Expired - Fee Related KR101744362B1 (ko) 2009-07-03 2010-06-30 １급 히드록실 말단 기를 포함하는 폴리에테르 폴리올의 제조 방법

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US (1) US9029495B2 (enExample)
EP (1) EP2448996B2 (enExample)
JP (1) JP2012531506A (enExample)
KR (1) KR101744362B1 (enExample)
CN (1) CN102471478B (enExample)
BR (1) BRPI1011807A2 (enExample)
CA (1) CA2767040A1 (enExample)
DE (1) DE102009031584A1 (enExample)
ES (1) ES2432501T5 (enExample)
MX (1) MX2011013699A (enExample)
SG (1) SG177282A1 (enExample)
WO (1) WO2011000560A1 (enExample)

Families Citing this family (13)

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Publication number Priority date Publication date Assignee Title
WO2011075343A1 (en) * 2009-12-17 2011-06-23 Dow Global Technologies Inc. Ethylene oxide capping of secondary hydroxyl polyols
DK2794798T3 (en) 2011-12-20 2016-02-29 Medical Adhesive Revolution Gmbh HYDROXY AMINO POLYMER AND USE THEREOF IN POLY-UREA / POLYURETHAN-tissue adhesives
EP2617748A1 (de) 2012-01-23 2013-07-24 Basf Se Polyetherester-Polyole und Verfahren zu deren Herstellung
EP3209706B1 (en) 2014-10-22 2018-09-05 Dow Global Technologies LLC Dual catalyst system for high primary hydroxyl polyols
KR102603117B1 (ko) * 2017-09-14 2023-11-17 노쓰웨스턴유니버시티 폴리올을 제조하는 방법
CN109180928B (zh) * 2018-09-14 2021-02-02 湖北工业大学 一种高纯度单羧基封端的聚乙二醇的制备方法
EP3670571A1 (de) 2018-12-21 2020-06-24 Covestro Deutschland AG Verfahren zur herstellung eines polyester-polyetherpolyol-blockcopolymers
EP3670568A1 (de) 2018-12-21 2020-06-24 Covestro Deutschland AG Verfahren zur herstellung eines polyesters
EP3670557A1 (de) * 2018-12-21 2020-06-24 Covestro Deutschland AG Verfahren zur herstellung eines polyoxyalkylenpolyesterpolyols
CN110540640A (zh) * 2019-09-19 2019-12-06 福建省天骄化学材料有限公司 一种鞋材专用分散剂的制备方法
EP3875510A1 (de) * 2020-03-03 2021-09-08 Covestro Deutschland AG Verfahren zur herstellung eines etheresterols
EP3889204A1 (de) 2020-04-02 2021-10-06 Covestro Deutschland AG Verfahren zur herstellung eines polyoxyalkylencarbonatpolyols
CN114369236B (zh) * 2021-11-30 2024-04-12 山东一诺威新材料有限公司 高性能聚酯醚多元醇及其制备方法和应用

Citations (1)

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US20060105188A1 (en) 2004-11-12 2006-05-18 Simons James B Laminating adhesives based on primary hydroxyl-containing curatives

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US3941849A (en) 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
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US4487853A (en) 1983-12-27 1984-12-11 Basf Wyandotte Corporation Low ethylene oxide/high primary hydroxyl content polyether-ester polyols and polyurethane foams based thereon
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US5627120A (en) 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
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US5763642A (en) * 1997-06-19 1998-06-09 Arco Chemical Technology, L.P. Low monol polyoxy (higher) alkylene polyols with primary hydroxyl content
US6066683A (en) 1998-04-03 2000-05-23 Lyondell Chemical Worldwide, Inc. Molded and slab polyurethane foam prepared from double metal cyanide complex-catalyzed polyoxyalkylene polyols and polyols suitable for the preparation thereof
DE19905611A1 (de) 1999-02-11 2000-08-17 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
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DE102007002555A1 (de) * 2007-01-17 2008-07-24 Bayer Materialscience Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
WO2011075343A1 (en) * 2009-12-17 2011-06-23 Dow Global Technologies Inc. Ethylene oxide capping of secondary hydroxyl polyols
PL2563834T3 (pl) * 2010-04-29 2019-07-31 Dow Global Technologies Llc Hybrydowe poliestropolieteropoliole

Patent Citations (1)

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Publication number Priority date Publication date Assignee Title
US20060105188A1 (en) 2004-11-12 2006-05-18 Simons James B Laminating adhesives based on primary hydroxyl-containing curatives

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BRPI1011807A2 (pt) 2016-05-31
MX2011013699A (es) 2012-02-22
EP2448996B1 (de) 2013-08-28
WO2011000560A1 (de) 2011-01-06
US9029495B2 (en) 2015-05-12
JP2012531506A (ja) 2012-12-10
SG177282A1 (en) 2012-02-28
CA2767040A1 (en) 2011-01-06
US20120196999A1 (en) 2012-08-02
ES2432501T5 (es) 2017-09-11
DE102009031584A1 (de) 2011-01-05
EP2448996A1 (de) 2012-05-09
CN102471478B (zh) 2016-03-09
KR20120095338A (ko) 2012-08-28
EP2448996B2 (de) 2017-04-12
CN102471478A (zh) 2012-05-23
ES2432501T3 (es) 2013-12-03

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