KR101444493B1 - 감소된 수의 밸브 및 라인을 갖는 모사이동층 분리 방법 및 장치 - Google Patents

감소된 수의 밸브 및 라인을 갖는 모사이동층 분리 방법 및 장치 Download PDF

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KR101444493B1
KR101444493B1 KR1020097019463A KR20097019463A KR101444493B1 KR 101444493 B1 KR101444493 B1 KR 101444493B1 KR 1020097019463 A KR1020097019463 A KR 1020097019463A KR 20097019463 A KR20097019463 A KR 20097019463A KR 101444493 B1 KR101444493 B1 KR 101444493B1
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plate
column
sector
valve
network
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KR20100014458A (ko
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제라르 오띠에
필리베르 르플레브
실벵 루레
프레데릭 오지에
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아이에프피 에너지 누벨르
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/1842—Simulated moving beds characterised by apparatus features
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0423—Beds in columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/06—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/26—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only halogen atoms as hetero-atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C07C15/067—C8H10 hydrocarbons
    • C07C15/08—Xylenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7027—Aromatic hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/414—Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141—Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B01D2259/4145—Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
    • B01D2259/4148—Multiple layers positioned apart from each other
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Sustainable Development (AREA)
  • Water Supply & Treatment (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020097019463A 2007-03-09 2008-02-14 감소된 수의 밸브 및 라인을 갖는 모사이동층 분리 방법 및 장치 Expired - Fee Related KR101444493B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0701772A FR2913345B1 (fr) 2007-03-09 2007-03-09 Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits
FR07/01772 2007-03-09
PCT/FR2008/000204 WO2008125751A1 (fr) 2007-03-09 2008-02-14 Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits

Publications (2)

Publication Number Publication Date
KR20100014458A KR20100014458A (ko) 2010-02-10
KR101444493B1 true KR101444493B1 (ko) 2014-10-07

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ID=38616443

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KR1020097019463A Expired - Fee Related KR101444493B1 (ko) 2007-03-09 2008-02-14 감소된 수의 밸브 및 라인을 갖는 모사이동층 분리 방법 및 장치

Country Status (7)

Country Link
US (1) US7582208B2 (enExample)
JP (1) JP5401326B2 (enExample)
KR (1) KR101444493B1 (enExample)
CN (1) CN101636210B (enExample)
BR (1) BRPI0808681B1 (enExample)
FR (1) FR2913345B1 (enExample)
WO (1) WO2008125751A1 (enExample)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1775001A1 (en) 2005-10-13 2007-04-18 Xendo Holding B.V. Device for chromatographic separations
FR2904776B1 (fr) * 2006-08-08 2009-01-23 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes reduit
FR2907021B1 (fr) * 2006-10-16 2009-02-06 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre reduit
FR2913346B1 (fr) 2007-03-09 2009-04-24 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre et volume de lignes reduits
FR2913345B1 (fr) * 2007-03-09 2010-06-11 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits
US8211312B2 (en) * 2009-03-27 2012-07-03 Uop Llc Separation system and method
FR2944215B1 (fr) * 2009-04-10 2011-04-01 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule comportant des lignes de derivation d'un lit sur deux et a debit de fluide de derivation module
FR2956037B1 (fr) * 2010-02-11 2012-02-17 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule comportant des lignes de derivation d'un lit sur deux avec debits de balayage controles lors des injections et des soutirages
JP5709974B2 (ja) * 2010-03-30 2015-04-30 エクソンモービル・ケミカル・パテンツ・インク 分離システム
US9943781B2 (en) 2010-06-03 2018-04-17 Ge Healthcare Bioprocess R&D Ab Parallel assembly of chromatography column modules
US9950277B2 (en) 2010-06-03 2018-04-24 Ge Healthcare Bioprocess R&D Ab Parallel assembly of chromatography column modules
CN101972558B (zh) * 2010-11-30 2013-01-02 顾雄毅 一种用于生化分离过程的膨胀床色谱分离柱及工艺流程
WO2012072029A1 (zh) * 2010-11-30 2012-06-07 Gu Xiongyi 一种用于生化分离过程的膨胀床色谱分离柱及工艺流程
US8329975B2 (en) * 2010-12-20 2012-12-11 Uop Llc Elimination of residual transfer line raffinate from feed to increase normal paraffin separation unit capacity
CN102671427B (zh) * 2011-03-11 2014-07-30 阮立昂 用于色谱层析装置的模拟移动床
FR2976500B1 (fr) * 2011-06-16 2013-05-31 IFP Energies Nouvelles Procede et dispositif de sepation chromatographique a contre-courant simule a faible perte de charge et nombre de zones eleve.
CN102895799B (zh) * 2011-07-28 2015-09-23 中国石油化工股份有限公司 控制阀数量减少的模拟移动床吸附分离方法和设备
US9328041B2 (en) 2013-09-24 2016-05-03 Uop Llc Methods and systems for separating para-xylene using a radial flow simulated moving bed chamber
CN106310712B (zh) * 2015-06-30 2018-06-15 中国石油化工股份有限公司 一种降低吸附分离装置吸附塔与旋转阀间床层管线残余液体影响的方法
KR20190013101A (ko) 2017-07-31 2019-02-11 이호석 흉터의 예방 또는 치료를 위한 조성물
FR3072885B1 (fr) * 2017-10-27 2019-11-15 IFP Energies Nouvelles Nouveau systeme de distribution par panneaux meridiens pour un procede de separation en lit mobile simule utilisant n-colonnes en serie
FR3082755B1 (fr) * 2018-06-20 2022-12-30 Ifp Energies Now Procede et dispositif de separation en lit mobile simule a nombre de lits reduit avec debit de fluide de derivation
US11027221B2 (en) 2018-10-19 2021-06-08 Uop Llc Process for a dual extract flush
CN118437031A (zh) * 2023-02-03 2024-08-06 中国石油化工股份有限公司 一种分离装置和方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4434051A (en) * 1982-06-07 1984-02-28 Uop Inc. Multiple valve apparatus for simulated moving bed adsorption processes
US6149874A (en) * 1996-07-11 2000-11-21 Institut Francais Du Petrole Rinsing apparatus in a simulated moving bed adsorption unit, and the use thereof
US6261458B1 (en) * 1998-07-31 2001-07-17 Institut Francais Du Petrole System for alternately merging at least four fluids and its application in a separation process in a simulated moving bed
US20030127394A1 (en) 2001-12-19 2003-07-10 Institut Francais Du Petrole Device for injecting a diverted fluid into a simulated moving bed separation process

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5635072A (en) * 1995-01-31 1997-06-03 Uop Simulated moving bed adsorptive separation process
FR2751888B1 (fr) * 1996-07-31 1998-09-11 Inst Francais Du Petrole Dispositif et procede de rincage en lit mobile simule comportant au moins deux lignes de distribution de fluides
FR2772634B1 (fr) * 1997-12-22 2000-02-18 Inst Francais Du Petrole Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule
FR2774310B1 (fr) * 1998-02-02 2000-02-25 Inst Francais Du Petrole Dispositif d'injection discontinue d'un fluide f2 dans une zone z1 ou d'extraction discontinue d'un fluide f1 depuis une zone z1
FR2777798B1 (fr) * 1998-04-27 2000-06-02 Inst Francais Du Petrole Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule comprenant une recirculation forcee de fluide
FR2782657B1 (fr) * 1998-09-02 2000-09-29 Inst Francais Du Petrole Systeme distributeur-collecteur de fluides et son procede
FR2782656B1 (fr) * 1998-09-02 2000-09-29 Inst Francais Du Petrole Distributeur-melangeur-extracteur de fluides et procede associe
FR2794836B1 (fr) * 1999-06-09 2001-08-03 Inst Francais Du Petrole Vanne rotative amelioree
FR2794663B1 (fr) * 1999-06-09 2001-07-13 Inst Francais Du Petrole Systeme d'injection d'un fluide devie dans un procede de separation en lit mobile simule
FR2843893B1 (fr) * 2002-08-28 2004-10-15 Inst Francais Du Petrole Methode pour optimiser le fonctionnement d'une unite de separation de xylenes par contre courant simule
FR2870751B1 (fr) * 2004-05-25 2006-08-04 Inst Francais Du Petrole Procede et dispositif perfectionne de separation en lit mobile simule
FR2904776B1 (fr) * 2006-08-08 2009-01-23 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes reduit
FR2907021B1 (fr) * 2006-10-16 2009-02-06 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre reduit
FR2913345B1 (fr) * 2007-03-09 2010-06-11 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4434051A (en) * 1982-06-07 1984-02-28 Uop Inc. Multiple valve apparatus for simulated moving bed adsorption processes
US6149874A (en) * 1996-07-11 2000-11-21 Institut Francais Du Petrole Rinsing apparatus in a simulated moving bed adsorption unit, and the use thereof
US6261458B1 (en) * 1998-07-31 2001-07-17 Institut Francais Du Petrole System for alternately merging at least four fluids and its application in a separation process in a simulated moving bed
US20030127394A1 (en) 2001-12-19 2003-07-10 Institut Francais Du Petrole Device for injecting a diverted fluid into a simulated moving bed separation process

Also Published As

Publication number Publication date
FR2913345B1 (fr) 2010-06-11
WO2008125751A1 (fr) 2008-10-23
BRPI0808681A2 (pt) 2015-08-04
US20080237132A1 (en) 2008-10-02
JP5401326B2 (ja) 2014-01-29
CN101636210B (zh) 2013-05-29
FR2913345A1 (fr) 2008-09-12
JP2010520809A (ja) 2010-06-17
KR20100014458A (ko) 2010-02-10
US7582208B2 (en) 2009-09-01
CN101636210A (zh) 2010-01-27
BRPI0808681B1 (pt) 2018-10-23

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