JP5401326B2 - 減らされた数のバルブおよびラインを有する擬似移動床分離のための方法および装置 - Google Patents

減らされた数のバルブおよびラインを有する擬似移動床分離のための方法および装置 Download PDF

Info

Publication number
JP5401326B2
JP5401326B2 JP2009553174A JP2009553174A JP5401326B2 JP 5401326 B2 JP5401326 B2 JP 5401326B2 JP 2009553174 A JP2009553174 A JP 2009553174A JP 2009553174 A JP2009553174 A JP 2009553174A JP 5401326 B2 JP5401326 B2 JP 5401326B2
Authority
JP
Japan
Prior art keywords
plate
column
sector
valve
network
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2009553174A
Other languages
English (en)
Japanese (ja)
Other versions
JP2010520809A5 (enExample
JP2010520809A (ja
Inventor
ジェラール オチエ
フィリベール ルフレーヴ
シルヴァン ルーレ
フレデリック オージエ
Original Assignee
イエフペ
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by イエフペ filed Critical イエフペ
Publication of JP2010520809A publication Critical patent/JP2010520809A/ja
Publication of JP2010520809A5 publication Critical patent/JP2010520809A5/ja
Application granted granted Critical
Publication of JP5401326B2 publication Critical patent/JP5401326B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/1842—Simulated moving beds characterised by apparatus features
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0423—Beds in columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/06—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/26—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only halogen atoms as hetero-atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C07C15/067—C8H10 hydrocarbons
    • C07C15/08—Xylenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7027—Aromatic hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/414—Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141—Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B01D2259/4145—Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
    • B01D2259/4148—Multiple layers positioned apart from each other
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Sustainable Development (AREA)
  • Water Supply & Treatment (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2009553174A 2007-03-09 2008-02-14 減らされた数のバルブおよびラインを有する擬似移動床分離のための方法および装置 Expired - Fee Related JP5401326B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0701772A FR2913345B1 (fr) 2007-03-09 2007-03-09 Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits
FR07/01772 2007-03-09
PCT/FR2008/000204 WO2008125751A1 (fr) 2007-03-09 2008-02-14 Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits

Publications (3)

Publication Number Publication Date
JP2010520809A JP2010520809A (ja) 2010-06-17
JP2010520809A5 JP2010520809A5 (enExample) 2013-10-17
JP5401326B2 true JP5401326B2 (ja) 2014-01-29

Family

ID=38616443

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009553174A Expired - Fee Related JP5401326B2 (ja) 2007-03-09 2008-02-14 減らされた数のバルブおよびラインを有する擬似移動床分離のための方法および装置

Country Status (7)

Country Link
US (1) US7582208B2 (enExample)
JP (1) JP5401326B2 (enExample)
KR (1) KR101444493B1 (enExample)
CN (1) CN101636210B (enExample)
BR (1) BRPI0808681B1 (enExample)
FR (1) FR2913345B1 (enExample)
WO (1) WO2008125751A1 (enExample)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1775001A1 (en) 2005-10-13 2007-04-18 Xendo Holding B.V. Device for chromatographic separations
FR2904776B1 (fr) * 2006-08-08 2009-01-23 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes reduit
FR2907021B1 (fr) * 2006-10-16 2009-02-06 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre reduit
FR2913346B1 (fr) 2007-03-09 2009-04-24 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre et volume de lignes reduits
FR2913345B1 (fr) * 2007-03-09 2010-06-11 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits
US8211312B2 (en) * 2009-03-27 2012-07-03 Uop Llc Separation system and method
FR2944215B1 (fr) * 2009-04-10 2011-04-01 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule comportant des lignes de derivation d'un lit sur deux et a debit de fluide de derivation module
FR2956037B1 (fr) * 2010-02-11 2012-02-17 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule comportant des lignes de derivation d'un lit sur deux avec debits de balayage controles lors des injections et des soutirages
JP5709974B2 (ja) * 2010-03-30 2015-04-30 エクソンモービル・ケミカル・パテンツ・インク 分離システム
US9943781B2 (en) 2010-06-03 2018-04-17 Ge Healthcare Bioprocess R&D Ab Parallel assembly of chromatography column modules
US9950277B2 (en) 2010-06-03 2018-04-24 Ge Healthcare Bioprocess R&D Ab Parallel assembly of chromatography column modules
CN101972558B (zh) * 2010-11-30 2013-01-02 顾雄毅 一种用于生化分离过程的膨胀床色谱分离柱及工艺流程
WO2012072029A1 (zh) * 2010-11-30 2012-06-07 Gu Xiongyi 一种用于生化分离过程的膨胀床色谱分离柱及工艺流程
US8329975B2 (en) * 2010-12-20 2012-12-11 Uop Llc Elimination of residual transfer line raffinate from feed to increase normal paraffin separation unit capacity
CN102671427B (zh) * 2011-03-11 2014-07-30 阮立昂 用于色谱层析装置的模拟移动床
FR2976500B1 (fr) * 2011-06-16 2013-05-31 IFP Energies Nouvelles Procede et dispositif de sepation chromatographique a contre-courant simule a faible perte de charge et nombre de zones eleve.
CN102895799B (zh) * 2011-07-28 2015-09-23 中国石油化工股份有限公司 控制阀数量减少的模拟移动床吸附分离方法和设备
US9328041B2 (en) 2013-09-24 2016-05-03 Uop Llc Methods and systems for separating para-xylene using a radial flow simulated moving bed chamber
CN106310712B (zh) * 2015-06-30 2018-06-15 中国石油化工股份有限公司 一种降低吸附分离装置吸附塔与旋转阀间床层管线残余液体影响的方法
KR20190013101A (ko) 2017-07-31 2019-02-11 이호석 흉터의 예방 또는 치료를 위한 조성물
FR3072885B1 (fr) * 2017-10-27 2019-11-15 IFP Energies Nouvelles Nouveau systeme de distribution par panneaux meridiens pour un procede de separation en lit mobile simule utilisant n-colonnes en serie
FR3082755B1 (fr) * 2018-06-20 2022-12-30 Ifp Energies Now Procede et dispositif de separation en lit mobile simule a nombre de lits reduit avec debit de fluide de derivation
US11027221B2 (en) 2018-10-19 2021-06-08 Uop Llc Process for a dual extract flush
CN118437031A (zh) * 2023-02-03 2024-08-06 中国石油化工股份有限公司 一种分离装置和方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4434051A (en) * 1982-06-07 1984-02-28 Uop Inc. Multiple valve apparatus for simulated moving bed adsorption processes
US5635072A (en) * 1995-01-31 1997-06-03 Uop Simulated moving bed adsorptive separation process
FR2750886B1 (fr) * 1996-07-11 1998-09-25 Inst Francais Du Petrole Dispositif de rincage dans une unite d'adsorption en lit mobile simule et son utilisation
FR2751888B1 (fr) * 1996-07-31 1998-09-11 Inst Francais Du Petrole Dispositif et procede de rincage en lit mobile simule comportant au moins deux lignes de distribution de fluides
FR2772634B1 (fr) * 1997-12-22 2000-02-18 Inst Francais Du Petrole Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule
FR2774310B1 (fr) * 1998-02-02 2000-02-25 Inst Francais Du Petrole Dispositif d'injection discontinue d'un fluide f2 dans une zone z1 ou d'extraction discontinue d'un fluide f1 depuis une zone z1
FR2777798B1 (fr) * 1998-04-27 2000-06-02 Inst Francais Du Petrole Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule comprenant une recirculation forcee de fluide
FR2781860B1 (fr) * 1998-07-31 2000-09-01 Inst Francais Du Petrole Systeme de mise en communication alternee d'au moins quatre fluides et son application dans un procede de separation en lit mobile simule
FR2782657B1 (fr) * 1998-09-02 2000-09-29 Inst Francais Du Petrole Systeme distributeur-collecteur de fluides et son procede
FR2782656B1 (fr) * 1998-09-02 2000-09-29 Inst Francais Du Petrole Distributeur-melangeur-extracteur de fluides et procede associe
FR2794836B1 (fr) * 1999-06-09 2001-08-03 Inst Francais Du Petrole Vanne rotative amelioree
FR2794663B1 (fr) * 1999-06-09 2001-07-13 Inst Francais Du Petrole Systeme d'injection d'un fluide devie dans un procede de separation en lit mobile simule
FR2833499B1 (fr) * 2001-12-19 2004-08-20 Inst Francais Du Petrole Dispositif d'injection d'un fluide devie dans un procede de separation en lit mobile simule
FR2843893B1 (fr) * 2002-08-28 2004-10-15 Inst Francais Du Petrole Methode pour optimiser le fonctionnement d'une unite de separation de xylenes par contre courant simule
FR2870751B1 (fr) * 2004-05-25 2006-08-04 Inst Francais Du Petrole Procede et dispositif perfectionne de separation en lit mobile simule
FR2904776B1 (fr) * 2006-08-08 2009-01-23 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes reduit
FR2907021B1 (fr) * 2006-10-16 2009-02-06 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes de grand diametre reduit
FR2913345B1 (fr) * 2007-03-09 2010-06-11 Inst Francais Du Petrole Procede et dispositif de separation en lit mobile simule a nombre de vannes et volume de lignes reduits

Also Published As

Publication number Publication date
KR101444493B1 (ko) 2014-10-07
FR2913345B1 (fr) 2010-06-11
WO2008125751A1 (fr) 2008-10-23
BRPI0808681A2 (pt) 2015-08-04
US20080237132A1 (en) 2008-10-02
CN101636210B (zh) 2013-05-29
FR2913345A1 (fr) 2008-09-12
JP2010520809A (ja) 2010-06-17
KR20100014458A (ko) 2010-02-10
US7582208B2 (en) 2009-09-01
CN101636210A (zh) 2010-01-27
BRPI0808681B1 (pt) 2018-10-23

Similar Documents

Publication Publication Date Title
JP2010520809A (ja) 減らされた数のバルブおよびラインを有する擬似移動床分離のための方法および装置
CN101143274B (zh) 采用减少的阀数目的模拟移动床分离方法与设备
US7582207B2 (en) Process and device for simulated moving bed separation with a reduced number of large diameter valves
JP5763360B2 (ja) バイパス・ラインを1つ置きの床内に包含し、注入および抜き出しの間におけるコントロールされたフラッシング・フロー・レートを伴う擬似移動床分離のための方法および装置
KR101828899B1 (ko) 모의 이동상 흡착 분리 방법 및 장치
KR101164239B1 (ko) 개선된 모의 이동상 분리 방법 및 장치
JP5343010B2 (ja) 減らされた数の大径バルブおよび低減させられたライン容積を有する擬似移動床分離のための方法および装置
JP2014528907A (ja) 圧力降下が少なくかつ帯域の床数が多い、擬似向流クロマトグラフィー分離のための方法および装置
CN104511184B (zh) 一种吸附分离c8芳烃所用模拟移动床的管线冲洗方法
KR20140053785A (ko) 총 개수 22 개 이하의 층을 갖는 직렬의 2 개의 흡착기로 구성되는, 파라-크실렌의 모의 역류 제조를 위한 방법 및 장치
KR102689602B1 (ko) 감소된 수의 베드들 및 바이패스 유체 유동을 갖는 시뮬레이션된 이동 베드 분리 방법 및 디바이스
KR102689160B1 (ko) 바이패스 유체 유동을 갖는 시뮬레이션된 이동 베드 분리 방법 및 디바이스
CN121944596A (zh) 模拟移动床吸附分离的系统和方法
CN116135278A (zh) 液相模拟移动床吸附分离系统和应用以及混合二甲苯吸附分离抽取间二甲苯的方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20110209

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130604

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20130830

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20131001

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20131028

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

Ref document number: 5401326

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees