KR101322244B1 - The manufacturing method of mixed beverages having cypress extract - Google Patents

Abstract

PURPOSE: A production method of mixed drink containing a retinispora leaf extract is provided to use a mixed solvent of ethyl alcohol and active water. CONSTITUTION: Dried retinispora leaves are steamed for 5-10 minutes at 100°C for blanching for 1-10 seconds in 100°C water (1). The dried retinispora leaves are crushed, and 1.0-3.0 %(w/v) of crushed retinispora leaves is mixed with 80-100°C of hot water for extracting for 5-7 hours to obtain a retinispora leaf extract (2). Purified water is passed through an active water producing device, and active water is obtained in which the nuclear magnetic resonance spectral half width value is changed to less than 80 Hz using an NMR spectrometer (3). The active water producing device includes a ceramic ball and a yellow soil ball filtering layer. The active water and ethyl alcohol are mixed in a volume ratio of 2-6:8-4 to obtain an extract solution. 5-20 v% of retinispora leaf extract is mixed with the extract solution, and residues are removed from the mixture. The vacuum condition of the mixture is controlled at 33-35°C for evaporating and removing the ethyl alcohol, and the mixture is transferred to a centrifuge for removing residues. [Reference numerals] (1) Steaming dried retinispora leaves; (2) Extracting dried retinispora leaves; (3) Active water; (4,AA) Ethyl alcohol; (5) Blend extractor; (6) Centrifuge; (7) Fermenting tank; (8) Concentration tank; (9) Retinispora leave extract; (BB) Recovery; (CC) Water

Description

The manufacturing method of mixed beverages containing cypress leaf extract and active water

The present invention relates to a method for producing a mixed beverage provided by containing cypress leaf extract component and active water.

Phytoncide, named by Russian biochemist Tokin in 1937, is a substance that plants exhale or secrete to resist pathogens, pests, and fungi. Drinking phytoncide through a forest bath relieves stress and intestinal and cardiopulmonary function. Since this enhanced and bactericidal activity has been confirmed, attempts have been made to exploit the efficacy of phytoncide in many food and beverage products.

However, phytoncide is an oil component extracted from a small amount of natural plants such as cypress leaves, and phytoncide has been found to contain phenolic compounds such as terpenes, alkaloids, and glycosides, but most of these components are not water-soluble and volatile. Because of its strength, it is only used for spray formulations, cosmetics, and medical use, and it does not dissolve well in water, so it is not easily dispersed when used as a drink or bath water. Because of the problem of volatilization of the powder, the current phytoncide is in the form of being mixed with vegetable oil, honey, milk, cream, and the like.

In the present application, the cypress leaf extract component is not easily dissolved in water, so it was intended to change the cypress leaf extract component into water-soluble by making a mixed solution of ethyl alcohol and active water as a means for converting it into water-soluble and providing it as a mixed drink. As used herein, the term active water means the following.

In general, the water is much research has consisted came bars, a water molecule H ₂ O to water and very important to the major constituents that make up most of the human body with food at the same time, the things of the origins enough to be recognized as the things of origin It cannot exist as a single molecule, is bound together by an electrical force acting between water molecules, maintains a hydrogen bonding state, and is formed in several groups, which are usually clustered or clustered of water (hereinafter, It is called a cluster), and it is determined that water is delicious or tasteless according to the size of the cluster, and when the size of the cluster is small, the water feels more delicious than when the size of the cluster is large.

However, the clusters of water are not kept constant by hydrogen bonding, but continue for a very short period of time, usually 1x10 ^-12 (one peak second) or one trillion seconds, depending on the degree of energy absorption or relaxation. As a result, it is known that the reconstruction and disassembly of the water cluster structure continue, and the fact that the cluster of water has a large or small cluster structure on an average, is an important factor.

In other words, when the energy is sensitized to water, the nucleus of the water in a stable state absorbs energy and is excited at a high energy level. In this case, the phenomenon of absorbing energy is called resonance. While the energy absorbs energy from the state and rises to a high energy level, the water molecules undergo vibration, rotation, stretching or micro brown movement, and the energy from the vibration, rotation, stretching or micro brown movement of these water molecules. The energy absorbed by the nucleus is extremely weak, so the water nucleus in the resonance state is transferred to the vibration, rotation, stretching, or micro-brown movement of water molecules, which is called relaxation of energy. Mitigation is always happening.

The energy relaxation phenomenon of such water can be visually confirmed by measuring the change in linewidth by nuclear magnetic resonance or nuclear magnetic resonance (NMR), nuclear magnetic resonance spectroscopy (NMR) The fact that the half-width measurement of the NMR spectrum is long indicates that the relaxation time is long and the half-width measurement is wide indicates that the relaxation time is short, and the fact that the relaxation time is long, It means to be fast, and the wide half - width measurement means that the movement of the water molecule is slow.

In general, there may be some deviations depending on the sampling position and the object of water, but for example, the measurement of the half-width of the 0 ¹⁷ nuclear magnetic resonance spectrum of rainwater is about 119 Hz, the tap water is about 117 Hz, and the minerals of Japan's longest village The hot spring water is known to be 79 Hz, and human serum is reported to show about 140 Hz. The hot spring water in the longest village in the world consumes water with a narrow half-width measurement, resulting in a long energy relaxation time. Molecular movements are active, resulting in a small cluster structure, and hot spring water containing a large amount of minerals contributes to longevity because the fine sodium, calcium, and magnesium contained in the water molecules are metal ionized and active in the living body. On the other hand, because tap water, rainwater, and human serum that have large half-width values have a wide half-width measurement, The screen time is short, and thus the movement of water molecules failed to actively and have a large cluster structure so did not ionize the trace metals that are relatively contained water molecules can be predicted to be active in vivo does not.

The term active water used herein is O ¹⁷ Refers to water whose nuclear magnetic resonance spectral half-width measurements are provided in the 70 to 90 Hz range, compared to those provided in the range of 117 ± 3 Hz, when tap water is generally measured with O ¹⁷ nuclear magnetic resonance spectral half-width measurements. Is expressed as active water.

When applied to humans, phytoncide extracted from cypress leaves is expected to have beneficial effects such as stress relief, antibacterial, deodorization and neutralization of harmful substances, sedative and comfort effects, improvement of allergic and skin diseases and enhancement of immune function. It is one of the materials that is expected to be used by modern people suffering from the disease.

In the prior art, a number of techniques for obtaining a drink using a leaf extract of a plant are disclosed. For example, Korean Patent Publication No. 1997-0009306 discloses a beverage composition containing a pine bud extract. Korean Patent Laid-Open Publication No. 1998-030115 describes a composition for preventing geriatric diseases using white berries and a method for preparing the beverage. Korean Patent Laid-Open Publication No. 2004-0091969 discloses a method for preparing a beverage containing cactus extract. It is.

In addition, Korean Patent No. 803342 describes a method for preparing a beverage containing cypress leaf extract, steaming dried leaves of cypress leaves at 100 ° C. for 5-10 minutes or blanching for 5-10 seconds at 100 ° C. hot water. ) And the cypress dry leaves of the above step were added 1.0% to 3.0% (w / v) to hot water at 80 to 100 ° C. and leached for 30 minutes to 5 hours to obtain a cypress leaf extract and undergo a filtration process to remove foreign substances. After adding sodium hydrogen carbonate or calcium carbonate to the cypress leaf extract, adding antioxidant to the cypress leaf extract, which was subjected to the above step, filled with nitrogen, and then sterilized by heating at 90 to 110 ° C. for 10 to 20 minutes. Through the means for cooling the sterilizing solution through a method for producing a beverage containing cypress leaf extract is disclosed.

However, in order to prevent volatilization of the cypress leaf extract, artificially adding sodium hydrogen carbonate or calcium carbonate, and additionally adding an antioxidant and filling with nitrogen, it is necessary to obtain a beverage containing the cypress leaf extract. It has a limit to it.

Techniques disclosed as methods for obtaining phytoncide in the prior art include steam distillation, compression, extraction, fat adsorption, and volatile organic solvent extraction. And supercritical fluid extraction (SFE) are disclosed.

The present invention is a means for solving the disadvantage that the phytoncide extracted from cypress or leaves is not well dissolved in water and the problem that the active ingredient is volatilized when using it as drinking water and the volatilization of the active ingredient early, ethyl alcohol and activity It is an object to obtain a mixed beverage stock solution in which the mixed beverage stock solution containing cypress leaf extract component is changed to water solubility using a mixed solvent of water.

In addition, in order to provide a mixed beverage obtained by the present invention as a mixed beverage, the food additives and sugars are added and the fruit functional ingredient or vitamins are added to provide a mixed beverage with improved functionality.

The present application is a means to solve the problem that the phytoncide is not water-soluble to be used as drinking water, which is extracted from a small amount of natural plants, and that the active ingredient volatilizes if it is not consumed early due to its high volatility. The cypress leaf residual extract obtained by steaming or blanching the cypress leaf is leached in hot water at 80 to 100 ° C. and then filtered to obtain the cypress leaf extract, and the active water group, which is a patent application technology of the present application, in order to make the cypress leaf extract water-soluble. Prepare the active water with O ¹⁷ nuclear magnetic resonance spectrum half-width measurement range of 70 ~ 80 Hz by using, and make the extraction solution mixed with active water and ethyl alcohol at 4 ± 2: 6 ± 2 ratio The residue is separated through a centrifuge, aged in a aging tank, and ethanol is separated in a concentration tank under vacuum. After discharging the remaining residual liquid to the active water, it is discharged by confirming that O ¹⁷ nuclear magnetic resonance spectrum half width value can be obtained containing mixed extract of cypress leaves in the range of 80 ~ 90 Hz. Invention.

Therefore, the technical idea of the present application is a means for obtaining a mixed beverage provided by containing a cypress leaf extract component, a method of preparing a mixed beverage stock solution containing a cypress leaf extract component, the cypress dried leaves at 100 ℃ for 5 to 10 minutes The cypress dried leaves obtained by steaming or blanching for 1 to 10 seconds in hot water at 100 ° C. were added and then 1.0% to 3.0% (w / v) added to hot water at 80 to 100 ° C. to leach for 5 to 7 hours. By the first step to obtain the cypress leaf extract, the purified water is passed through the active water group having a ceramic ball and ocher ball filter layer to obtain active water whose nuclear magnetic resonance spectral half-width value is converted to 80 Hz or less using the NMR Spectrometer. In step 2, the active water and ethyl alcohol obtained in step 2 were mixed, but active water 4 ± 2: ethyl alcohol was prepared in a mixture solution of 6 ± 2 ratio, and the cypress leaf extract obtained in the first step was mixed with the solution. Injected at 5 ~ 20v% The third step of removing the residue after the cypress leaf extract component is dissolved in the mixed extraction solution, the filtrate from which the residue is removed through the above process by adjusting the vacuum degree in the range 33 ~ 38 ℃ under vacuum conditions to evaporate ethyl alcohol The fourth step of obtaining / removing cypress leaf extract component, the cypress leaf extract component passed through the fourth step is passed through the active water production apparatus and the cypress leaf extract component of the active water is mixed in the range of 0.1 ~ 10 wt% It is an invention of the technical concept to obtain a mixed beverage stock solution containing an extract component.

In addition, the present application is to obtain a mixed beverage source containing the cypress leaf extract component through the above process and using the same, at least one selected from sodium citrate, malic acid, silicon dioxide, aromatic aroma in the mixed beverage stock solution obtained from the above manufacturing process Sugar, glucose, microsaccharides, dextrins, fructose, oligosaccharides, propolis, trehalos, sorbitol, xylitol, mannitol after food additives are included in the range of 0.1 to 1 wt% ), Mannitol, rhamnitol, inositol, inositol, erythritol, paratinos, and quercitol. Can be.

In addition, the above-mentioned mixed drinks include 0.5 to 5 t% of one or more functional ingredients or vitamins selected from audi, bokbunja, cherry, red grapes, cherry, strawberry, tangerine peel, guarana fruit, buttercup, plum extract, and lutein. The mixed beverage may be provided in an additional composition.

The application form in which the technical spirit of the present application is specifically implemented will be described in detail in the following detailed description for carrying out the present invention.

The present application can not be provided with a mixed beverage provided by containing a conventional extract of cypress leaves, it is necessary to accompany the cumbersome process such as adding an antioxidant and nitrogen filling to eliminate the constraints to obtain a beverage containing the extract of cypress leaves It has the effect of providing a water-soluble beverage that can enjoy the effect provided by the leaf extract component.

1: Illustrated diagram of an apparatus for producing active water applied herein
Figure 2 is a manufacturing process diagram of the mixed beverage stock solution provided by containing the cypress leaf extract component to which the technical spirit of the present application is applied.
Figure 3 is an illustration of an apparatus for preparing a mixed beverage undiluted solution provided containing a cypress leaf extract component applied to the present application.
4. Example device and extract yield chart for carrying out cypress leaf extraction process herein.

Hereinafter, the embodiments of the technical spirit of the present application will be described below, the numbers indicating the upper limit or the lower limit of various reaction conditions or compositions presented to obtain a mixed drink containing the extract of cypress leaves is the purpose of the present application Experimental results by various trial and error methods to achieve the present invention is one example of the application of the range of the inventors achieve the desired expectations, and does not represent all of the technical spirit of the present application, but the upper limit of the numerical values presented herein In the case of deviation from the lower limit or the lower limit, the best physical property is impaired and the problem is departed from the purpose.

In addition, the manufacturing method according to the purity or the blending ratio of various raw materials presented as a means for achieving the object of the present application may have a somewhat influence depending on the blending order, but the scope of rights according to the technical idea of the present invention is described in the claims It should be interpreted and applied equally on the basis of contents.

The present application solves the problem that phytoncide is an oil component extracted from a small amount of natural plants, which does not dissolve well in water and does not disperse when used as drinking water and the volatility is so strong that volatilization of active ingredients does not occur early. In order to obtain a beverage in which the mixed beverage containing cypress leaf extract component is made water-soluble using a mixed solvent of ethyl alcohol and active water.

In the present invention, as a means for obtaining the active water, by using the active water group disclosed in the present patent application No. 2011-119300 of the present inventors, clean purified water is passed through a ceramic ball or an ocher ball media layer to use an NMR Spectrometer. ¹⁷ Nuclear Magnetic Resonance Spectrum Half-width measurements are obtained with active water converted to less than 80 Hz.

Figure 1 shows a side view in the form of an internal perspective so that the internal structure is visible in one application of the active water group 100 applicable here, the active water group 100 is applicable to the upper portion of the body 70 In the body 70, there are 12 kinds of activating materials. The activating materials selected from zeolite, clay, diatomaceous earth, germanium, ocher, illite, and tourmaline are calcined to achieve different compounding ratios. The first contact media layer to the ninth contact media layers 41 to 49 are formed on the first pedestal to the ninth pedestal on a kind of tray-shaped pedestal that is processed in the form of ceramic balls or ocher balls 51 to 59 to induce zigzag flow. 51 to 59) and the water flowing through the channel 31 of the base member 30 is introduced into the active water heater 100 after impurities are removed through the prefilter 10 and the auxiliary filter 20. Jig each contact media layer Circulating in form and converting into active water, three or more contact filter layers (61 GPG ceramic filter layer, 62 palm tree charcoal filter layer, 63 nanosilver filter layer) have a catalyst layer on the filter or diskette structure. It can be applied to.

In FIG. 1, the water flowing into the water channel 31 below the active water group is passed through the prefilter 10 and the auxiliary filter 20, and impurities are removed, and the water flowing into the active water group 100 is the first contact medium layer 41. since from flows to the overflow ninth contact media layer 49 filled with each other to achieve the activation of the different mixing ratios metal forming a ceramic ball or circulate ocher on zigzag passage through the contact media layer flows between 0 ¹⁷ nuclear magnetic It is disclosed in the applicant's prior application publication 2011-119300, in which the half-width measurement of the resonance spectrum is provided in the range of 70 to 80 Hz. Hole, 74 is functional water outlet, 75 is functional water outlet)

The apparatus for producing active water shown in FIG. 1 may have a difference in the measurement result depending on the size and flow velocity of the contact area. In the process of the present application, the active type of diameter (ID) 650 mm × height 3,000 mm The results of Table 1 were obtained as a result of pH measurement when the general tap water was sent at a rate of 50 mm / min to the water manufacturing device, and the results of Table 2 were obtained from the characteristics of ¹⁷ O using the NMR Spectrometer. In the present application, far-infrared active water having a range of 70-80 Hz was obtained by measurement by ¹⁷ O-NMR spectroscopy (nuclear magnetic resonance spectroscopy), which was mixed with ethyl alcohol in a ratio of about 4: 6 to dissolve the cypress leaf extract. It was intended to be used as.

sample pH value measuring equipment tap water 7.02 TOA Electronic
HM-149 pH meter  Water through the active water column of the present invention 7.84

time
sample 19 minutes 50 seconds 39 minutes 4 seconds measuring equipment tap water 105.45 Hz 105.34 Hz Varian's Unit Plus
300NMR Spectrometer  Far infrared ray 72.14 Hz 73.82 Hz

In order to obtain the phytoncide essential oil component from the cypress leaves as a means for obtaining a mixed beverage containing the phytoncide essential oil component herein, steam distillation, expression, extraction, fat adsorption , Volatile organic solvent extraction, supercritical fluid extraction (SFE), and the like may be used, but in the present application, a cypress leaf extract is obtained by the method disclosed in Korean Patent No. 803342 and the technical configuration of the present application. It was intended to be applied to.

In the present application, as shown in the manufacturing process diagram for obtaining the mixed beverage shown in Figure 2, the cypress leaf residual extract obtained by steaming or blanching the cypress leaf is leached in hot water of 90 to 100 ℃ first and then filtered to extract the cypress leaf extract. In order to make the cypress leaf extract water-soluble, the active water group was used to make active water with O ¹⁷ nuclear magnetic resonance spectrum half-width measurement in the range of 70 to 80 Hz, and the active water and ethyl alcohol were 4 ± 2: 6 ± 2. After extracting the mixed solution in the ratio, inject the cypress leaf extract oil, melt it, separate the residues and residues through the centrifuge, and ripen in the aging tank, and then adjust the vacuum degree in the concentration tank in the range of 33 ~ 35 ℃. After separating it first, the remaining residue is controlled by vacuum degree in the range of 36 ~ 38 ℃, removing ethanol residue and passing through the active water production line again. The shipment yields a phytoncide beverage with an O ¹⁷ nuclear magnetic resonance spectrum half-width converted in the 80-90 Hz range.

2 is a view illustrating a configuration applied in an embodiment with reference to the manufacturing process diagram to which the technical idea of the present application is applied to obtain a mixed beverage, first, the first process will be described for the steaming step (1) of the baekyopberry To compensate for the disadvantage that astringent taste takes precedence over sweet taste when leaching cypress leaves with hot water, 10.0 kg of cypress leaves are filled in upper and lower trays of stainless chamba and steamed to reduce tannin content, which is the main cause of astringent taste. The steaming process of the cypress dry leaves was carried out for 10 minutes at 100 ℃.

In the second step of extracting the cypress dry leaves (2) can be obtained by extracting the cypress leaves, which have been adjusted by the tannin content through the steaming process of the first step under hydrothermal extraction under optimized extraction conditions, extraction conditions Finely cut or crushed cypress dry leaves after the steaming process of the first step was added to hot water (98 ° C.), which is 10 times the weight of the cypress dry weight, and the hydrophilic extract was carried out for 5 to 7 hours. When used by cutting to about 0.21% by weight, when using the crushed cypress dry leaves can obtain a cypress leaf extract oil, in the laboratory to perform the hydrothermal extraction process of cypress dried leaves The applied extraction apparatus is shown in FIG. 4A, and as a result of various experiments performed through the apparatus of FIG. 4A, it is more convenient than the case in which the cypress dried leaves are cut as shown in FIG. 4B. When crushed dried leaves were used to obtain higher protein extract oil, it was confirmed that the extraction time is applied in the range of 5-7 hours through the data of FIG. 4c. About 1Okg of about 30 g of extract protein oil was obtained.

The third step is the active water production process, the O ¹⁷ nuclear magnetic resonance spectrum half-width measurement using the NMR Spectrometer using the active water disclosed in the above-described Patent Publication No. 2011-119300 described above, as shown in Table 2, 72 ~ 73Hz range Active water (3) provided was used.

In the present application, an attempt was made to dissolve the extract of the cypress dried leaves obtained in the second step using only the active water (3) obtained through the third step, but it was confirmed that the solvent was not dissolved. Ethyl alcohol (4) 6 ± 2: active water (3 ) Put the mixture solution into the mixer extractor (5) at 4 ± 2 ratio and inject a small amount of the extracted oil component of the cypress dried leaves obtained in the second step by stirring slowly in the clockwise direction at the speed of 100 ~ 120 rpm and stirring. In one application example of the present application, 30 g of cypress extract oil was slowly added to a mixed solvent of 180 ml of ethyl alcohol and 120 ml of active water, followed by stirring for about 3 hours. .

After the dissolution process, which is the fourth process, is completed, the temperature is gradually increased by using a reaction tank provided as a vacuum evaporation means. The residue was removed by the centrifuge (6), and the filtrate was sent to the aging tank (7) to carry out the aging process as a fifth step in the range of 6 to 12 hours in the range of about 18 ± 2 ℃.

After completion of the aging process is sent to the vacuum concentration tank (8) under vacuum conditions to gradually increase the temperature first to adjust the degree of vacuum in the 35 ~ 36 ℃ range to go through the process of evaporation accompanied by a small amount of ethyl alcohol and a little water to extract the protein It is possible to obtain a mixed solution containing the active water + protein extract oil containing the component in the range of about 20 ± 1 wt%, the mixed solution is reactivated to pass through the active water production line shown in Figure 3 ( Cyclone leaf extract component converted to O ¹⁷ nuclear magnetic resonance spectrum half-width value in 80-90 Hz range by passing through active water so as to contain cypress leaf extract component in the range of 0.1-5 wt% through the 6th process) A mixed beverage stock solution containing can be obtained.

3 is a unit active water groups (110, 120, 130, 140) is installed in a plurality of parallel structure to form a structure in which the four active water groups (110, 120, 130, 140) is fixed to the outer frame 150 and the auxiliary frame 151 and the baekbyeon side extract components as desired herein An example of the use that can be applied to the apparatus containing the mixed beverage raw material liquid contained in the storage tank 200, for example, selected from the first contact media layer to the ninth contact media layers 41 to 49 as shown in FIG. In the active water group of the parallel structure filled with contact media, the tap water is introduced into the active water through the active water groups 1 and 2 (110,120) and is introduced into the active water group 3 (130) as described in FIG. When the cypress leaf extract component is introduced into the active water + 130, the active solution + cypress extract oil-containing mixed solution through the valve V3 in the position B of FIG. When the inflow of the changed active water flows through the valve V2 through the yellow water phase (110,120), the cypress leaf extract component is finally contained in the range of 0.1 to 5 wt% by means of controlling the amount of A and B sent. It may be provided as a liquor-containing mixed beverage raw material liquid.

Example 1 to the composition of Table 3 as a mixed drink desired by the inventors of the present invention using the raw ingredient adjusted so that the extract of the cypress leaf in the active water in the blended beverage manufacturing process through the Figure 3 apparatus of 3.0 wt% range In the composition of Example 5, in the comparative example, the cypress leaf extract ingredient is added to the amount of 5.0 wt% of active water instead of 5.0 wt% of the raw ingredients, which are adjusted to form a range of 3.0 wt%, instead of the amount of the active ingredient. A mixed drink was made and a panel test was conducted.

 ingredient Example 1
(wt%) Example 2
(wt%) Example 3
(wt%) Example 4
(wt%) Example 5
(wt%) Comparative Example
(wt%)  3 wt%  5.0  5.0  5.0  5.0  5.0  -  Citric Acid Na  0.8  0.8  0.8  0.8  0.8  0.8  Malic acid  0.5   0.5   0.5   0.5   0.5   0.5  Silicon dioxide  0.5   0.5   0.5   0.5   0.5   0.5  glucose  32.7  32.7  32.7  32.7  32.7  32.7  Bokbunja  1.5  Audi  1.5  Cherry  1.5  Red grapes  1.5  Plum Extract  1.5  Cherry  1.5  Active water  59  59  59  59  59  64  Sum  100  100  100  100  100  100

Sensory tests such as taste, aroma, preference, etc. were performed on the mixed drinks of Example 1 to Comparative Example, and the results are shown in Table 2 below. Fifteen males and females were subjected to five-point scales of taste, aroma and preference to average / calculate the aggregates. The results in Table 2 were obtained.

 division  flavor  incense  Likelihood  Example 1  4.5  4.5  4.3  Example 2  4.4  4.4  4.4  Example 3  4.4  4.3  4.3  Example 4  4.5  4.4  4.5  Example 5  4.5  4.4  4.4  Comparative Example  3.6  3.5  3.4

From the results of the panel test test of Table 4, the technical idea of the present invention is that sensory soybeans can be clearly distinguished in sensory evaluation between the use of the raw ingredient adjusted to make the range of 3.0 wt% range and the mixed beverage not used It could be confirmed that the excellent functional beverage can be provided.

10: pre filter 20: auxiliary filter
30: base member 41 ~ 49: contact medium layer
51 ~ 59: Pedestal layer 61 ~ 63: Filter layer
70: active water body
100,110,120,130,140: Active Water 150: Outer Frame
151: auxiliary frame 200: raw material storage tank

Claims (3)

In the method for producing a mixed beverage stock solution containing a cypress leaf extract component,
1.0% to 3.0% (w) in hot water at 80 to 100 ° C by crushing the cypress dried leaves obtained by steaming cypress dried leaves at 100 ° C for 5 to 10 minutes or by blanching at 100 ° C hot water for 1 to 10 seconds. / v) the first step of obtaining a cypress leaf extract by adding and leaching for 5-7 hours;
A second step of passing purified water through an active water group having a ceramic ball and an ocher ball filtration layer to obtain active water having a nuclear magnetic resonance spectral half-width converted to 80 Hz or less using an NMR Spectrometer;
Mixing the active water and ethyl alcohol obtained in the second step, but the active water 4 ± 2: ethyl alcohol 6 ± 2 volume ratio of the extraction solution was made and the cypress leaf extract obtained in the first step 5 ~ of the mixed extraction solution A third step of dissolving the cypress leaf extract component in a mixed extract solution by injecting at 20v% to remove the residue;
After the third step, the residue was removed from the filtrate under vacuum condition, and the degree of vacuum was adjusted in the range of 33 to 35 ° C. to evaporate / remove the ethyl alcohol and send the contents to a centrifuge to remove the residue. A fourth step of carrying out a aging process in a range of 6-12 hours in a range of 18 ± 2 ° C .;
The aging solution passed through the fourth step was sent to a vacuum concentration tank to adjust the vacuum degree in the range of 35 to 36 ° C., followed by evaporation with the remaining amount of ethyl alcohol and water. A fifth step of obtaining a mixed solution;
The mixed solution obtained through the fifth step is passed through the active water producing apparatus, the method for producing a mixed beverage stock solution containing a cypress leaf extract component mixed in the range of 0.1 to 5.0 wt% cypress leaf extract component of the active water. In the mixed beverage provided by containing the cypress leaf extract component,
1.0% to 3.0% (w) in hot water at 80 to 100 ° C by crushing the cypress dried leaves obtained by steaming cypress dried leaves at 100 ° C for 5 to 10 minutes or by blanching at 100 ° C hot water for 1 to 10 seconds. / v) the first step of obtaining a cypress leaf extract by adding and leaching for 5-7 hours;
A second step of passing purified water through an active water group having a ceramic ball and an ocher ball filtration layer to obtain active water having a nuclear magnetic resonance spectral half-width converted to 80 Hz or less using an NMR Spectrometer;
Mixing the active water and ethyl alcohol obtained in the second step, but the active water 4 ± 2: ethyl alcohol 6 ± 2 volume ratio of the extraction solution was made and the cypress leaf extract obtained in the first step 5 ~ of the mixed extraction solution A third step of dissolving the cypress leaf extract component in a mixed extract solution by injecting at 20v% to remove the residue;
After the third step, the residue was removed from the filtrate under vacuum condition, and the degree of vacuum was adjusted in the range of 33 to 35 ° C. to evaporate / remove the ethyl alcohol and send the contents to a centrifuge to remove the residue. A fourth step of carrying out a aging process in a range of 6-12 hours in a range of 18 ± 2 ° C .;
The aging solution passed through the fourth step is sent to the vacuum concentration tank to gradually increase the temperature and adjust the degree of vacuum in the range of 35 to 36 ° C., followed by evaporation with the remaining amount of ethyl alcohol and water. A fifth step of obtaining a mixed solution contained in a range;
Passing the mixed solution obtained through the fifth step through the active water producing apparatus and obtaining a mixed beverage stock solution provided by containing the cypress leaf extract component mixed with the cypress leaf extract component in the range of 0.1 ~ 5.0 wt% of active water step;
Sugar, glucose, microsaccharides, dextrins, fructose, sugar, glucose, microsaccharides, dextrins, fructose, citric acid, malic acid, silicon dioxide, and edible additives selected from the range of 0.1 to 1 wt% Oligosaccharides, propolis, trehalos, sorbitol, xylitol, mannitol, mantitol, rhamnitol, inositol, erythritol, A mixed beverage containing a cypress leaf extract, characterized in that the addition of at least one sugar selected from paratinos (paratinos) and quercitol (quercitol). 3. The method of claim 2,
In the mixed drink, one or more functional ingredients or vitamins selected from audi, bokbunja, cherry, red grapes, cherry, strawberry, tangerine peel, guarana fruit, buttercup, plum extract, and lutein are in the range of 0.5 to 5 wt%. Mixed beverage containing cypress leaf extract, characterized in that the additional provided.

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