KR101972111B1 - Manufacturing method of pear extract - Google Patents

Manufacturing method of pear extract Download PDF

Info

Publication number
KR101972111B1
KR101972111B1 KR1020160082629A KR20160082629A KR101972111B1 KR 101972111 B1 KR101972111 B1 KR 101972111B1 KR 1020160082629 A KR1020160082629 A KR 1020160082629A KR 20160082629 A KR20160082629 A KR 20160082629A KR 101972111 B1 KR101972111 B1 KR 101972111B1
Authority
KR
South Korea
Prior art keywords
extract
weight
parts
water
extractor
Prior art date
Application number
KR1020160082629A
Other languages
Korean (ko)
Other versions
KR20180003152A (en
Inventor
이강삼
Original Assignee
슬로푸드 주식회사 농업회사법인
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 슬로푸드 주식회사 농업회사법인 filed Critical 슬로푸드 주식회사 농업회사법인
Priority to KR1020160082629A priority Critical patent/KR101972111B1/en
Publication of KR20180003152A publication Critical patent/KR20180003152A/en
Application granted granted Critical
Publication of KR101972111B1 publication Critical patent/KR101972111B1/en

Links

Images

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/385Concentrates of non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/72Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2250/00Food ingredients
    • A23V2250/20Natural extracts
    • A23V2250/21Plant extracts
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/14Extraction
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/24Heat, thermal treatment
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/50Concentrating, enriching or enhancing in functional factors

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

본 발명은 배 엑기스 제조방법에 관한 것으로, 보다 상세하게는 배와 부재료인 초석잠, 도라지, 생강, 대추를 포함하는 기능성이 증진된 배 엑기스 제조방법에 관한 것이다.
본 발명에 따른 배엑기스 제조방법은 배를 슬러쉬화하는 제 1단계; 추출기에 상기 슬러쉬한 배, 기능성 부재료, 물을 투입하는 제 2단계; 상기 추출기를 이용하여 열수추출을 수행하는 제 3단계; 상기 열수추출한 추출물을 여과하여 추출액을 얻는 제 4단계; 상기 여과한 추출액을 농축하여 엑기스를 얻는 제 5단계; 상기 농축한 엑기스를 여과하는 제 6단계; 상기 여과한 엑기스를 포장하는 제 7단계;를 포함하되, 상기 기능성 부재료는 초석잠, 도라지, 생강, 대추 중 적어도 어느 하나를 포함하여 구성하는 것을 특징으로 한다.
More particularly, the present invention relates to a method for producing a vinegar having enhanced functionality including a main ingredient such as a pearl bar, a bellflower, ginger, and jujubes.
A method for manufacturing a vinegar extract according to the present invention comprises a first step of making a vessel slush; A second step of injecting the slush vessel, the functional ingredient, and water into the extractor; A third step of performing hot water extraction using the extractor; A fourth step of filtering the extracted hot-water extract to obtain an extract; A fifth step of concentrating the filtered extract to obtain an extract; A sixth step of filtering the concentrated extract; And a seventh step of packaging the filtered extract, wherein the functional material comprises at least one of cornerstone, bellflower, ginger, and jujube.

Description

배 엑기스 제조방법{Manufacturing method of pear extract}Manufacturing method of pear extract "

본 발명은 배 엑기스 제조방법에 관한 것으로, 보다 상세하게는 배와 부재료인 초석잠, 도라지, 생강, 대추를 포함하는 기능성이 증진된 배 엑기스 제조방법에 관한 것이다.More particularly, the present invention relates to a method for producing a vinegar having enhanced functionality including a main ingredient such as a pearl bar, a bellflower, ginger, and jujubes.

근래 급속한 산업화의 영향으로 갈수록 대기 오염문제가 갈수록 심각하게 대두되고 있으며, 이로 인하여 발생하는 직접적인 질병 발생 문제는 인류의 건강을 위협하고 있다. 특히 다양한 호흡기 질환을 호소하는 환자의 발생이 매년 증가 추세이다. In recent years, the problem of air pollution has become more and more serious due to the rapid industrialization, and the problem of direct disease caused by it has threatened human health. In particular, the incidence of patients complaining of various respiratory diseases is increasing every year.

한편, 배는 예로부터 한방의 중요 약재로 활용될 만큼 인체에 유익한 과일로, 본초강목, 동의보감 등에 의하면 배는 맛은 달고 차가우며, 무독하고, 즙을 내어 복용하면 효율성이 뛰어난 것으로 알려져 왔으며, 담, 가래, 기침, 해열, 진통, 이뇨 촉진(다이어트 효과), 숙취해소, 종기 등의 치료에 효능을 나타내고, 식품분야에서는 고기를 연하게 하는 것으로 알려져 있다. 또한, 최근 항암제로서의 효과도 발표되고 있다. On the other hand, it has been known that the pear is useful for human body as it is used as an important medicinal material for a long time, and it is known that the pear is tasteful and cold, unattractive, and excellent in efficiency when taken by juice, It is known that it has efficacy in the treatment of sputum, cough, fever, pain, urinary diuretic (dieting effect), relieving hangover, boil and so on in the field of food. In addition, recently, the effect as an anticancer drug has also been announced.

지금까지 배는 주로 식품 분야에서 설탕과 탄산이 함유된 탄산음료 대신에 천연물을 주재로 한 음료로서 갈아만든 배 등의 캔음료 제품의 형태로 출시되고 있으며, 한국등록특허 제10-0882710호에는 배를 주로 하는 음료의 조성물 및 그의 제조 방법이 개시되어 있다. Until now, the pear has been released in the form of a can drink product such as a pear, which is produced by replacing a carbonated drink containing sugar and carbonic acid in a food field mainly as a beverage based on a natural substance. In Korean Patent No. 10-0882710, And a method for producing the same.

그러나, 배를 적절히 처리하여 건강 기능성을 증대시키거나, 특정 질환 등에 유효한 제품으로 개발하려는 시도는 아직 주목할만한 성과가 없는 실정이다.However, there is no remarkable achievement in attempts to increase the health functionalities by properly treating the fish or to develop them as products effective for specific diseases.

한국등록특허 제10-0882710호Korean Patent No. 10-0882710

본 발명에 따른 목적은 배엑기스 제조 시 기능성 부재료를 첨가하여 보다 건강 기능성이 증대되고, 기호도가 높은 배엑기스를 제조한 것이다.The object of the present invention is to produce a pear extract having a higher degree of health function and a higher degree of preference by adding a functional ingredient in the production of a pear extract.

발명이 해결하고자 하는 기술적 과제들은 이상에서 언급한 기술적 과제들로 제한되지 않으며, 언급되지 않은 또 다른 기술적 과제들은 아래의 기재로부터 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에게 명확하게 이해될 수 있을 것이다.It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory and are not restrictive of the invention as set forth in the accompanying drawings. It will be possible.

본 발명에 따른 배엑기스 제조방법은 배를 슬러쉬화하는 제 1단계; 추출기에 상기 슬러쉬한 배, 기능성 부재료, 물을 투입하는 제 2단계; 상기 추출기를 이용하여 열수추출을 수행하는 제 3단계; 상기 열수추출한 추출물을 여과하여 추출액을 얻는 제 4단계; 상기 여과한 추출액을 농축하여 엑기스를 얻는 제 5단계; 상기 농축한 엑기스를 여과하는 제 6단계; 상기 여과한 엑기스를 포장하는 제 7단계;를 포함하되, 상기 기능성 부재료는 초석잠, 도라지, 생강, 대추 중 적어도 어느 하나를 포함하여 구성하는 것을 특징으로 한다.A method for manufacturing a vinegar extract according to the present invention comprises a first step of making a vessel slush; A second step of injecting the slush vessel, the functional ingredient, and water into the extractor; A third step of performing hot water extraction using the extractor; A fourth step of filtering the extracted hot-water extract to obtain an extract; A fifth step of concentrating the filtered extract to obtain an extract; A sixth step of filtering the concentrated extract; And a seventh step of packaging the filtered extract, wherein the functional material comprises at least one of cornerstone, bellflower, ginger, and jujube.

또한, 상기 본 발명에 따른 배엑기스 제조방법은 상기 제 2단계에서 추출기에 슬러쉬한 배, 기능성 부재료, 물의 투입 시 비율은 슬러쉬한 배 55중량부에 대하여 기능성 부재료 25중량부, 물 20중량부인 것을 특징으로 한다.In addition, in the method for producing a pear extract according to the present invention, the amount of the blended slurry, the functional ingredient, and water added to the extractor in the second step is 25 parts by weight of the functional ingredient and 20 parts by weight of water, .

또한, 상기 본 발명에 따른 배엑기스 제조방법은 상기 제 3단계에서 열수추출은 가열온도 120℃에서 6시간 동안 수행하는 것을 특징으로 한다.In addition, in the method for manufacturing a bait extract according to the present invention, the hot water extraction in the third step is performed at a heating temperature of 120 ° C for 6 hours.

또한, 상기 본 발명에 따른 배엑기스 제조방법은 상기 제 5단계에서 농축은 가열온도 60℃에서 2시간 동안 수행하는 것을 특징으로 한다.In addition, in the method for producing an extract of the present invention, the concentration in the fifth step is performed for 2 hours at a heating temperature of 60 ° C.

상기 과제의 해결 수단에 의해, 본 발명의 배엑기스 제조방법은 배의 담, 가래, 기침, 해열, 진통, 이뇨 촉진(다이어트 효과), 숙취해소, 종기 등의 치료 효능에 초석잠, 도라지, 생강, 대추의 기능성이 포함된 엑기스를 제조할 수 있으며, 배의 단맛으로 인하여 부가적인 추가물 없이도 맛이 우수하여 맛과 기능성이 우수한 배엑기스를 제조할 수 있는 효과가 있다. According to the solution of the above-mentioned problems, the present invention provides a method for producing a vinegar extract of the present invention, which is characterized in that it has a therapeutic effect such as feces, sputum, cough, fever, pain, diuretic (dieting effect), hangover, , And jujube functionalities can be produced, and it is possible to produce a vinegar extract excellent in taste and functionality without any additional additives due to the sweetness of the vinegar.

도 1은 본 발명의 배엑기스 제조방법을 나타내는 순서도이다.1 is a flow chart showing a method for producing a vinegar extract of the present invention.

이상과 같은 본 발명에 대한 해결하려는 과제, 과제의 해결 수단, 발명의 효과를 포함한 구체적인 사항들은 다음에 기재할 일실시예 및 도면들에 포함되어 있다. 본 발명의 이점 및 특징, 그리고 그것들을 달성하는 방법은 첨부되는 도면과 함께 상세하게 후술되어 있는 일실시예를 참조하면 명확해질 것이다.The above and other objects, features and advantages of the present invention will be more apparent from the following detailed description taken in conjunction with the accompanying drawings, in which: FIG. BRIEF DESCRIPTION OF THE DRAWINGS The advantages and features of the present invention and the manner of achieving them will become apparent by reference to an embodiment which will be described in detail below with reference to the accompanying drawings.

하기에서는 상기 제시된 배엑기스 제조방법에 대하여 상세하게 설명한다.Hereinafter, the present invention will be described in detail.

도 1은 본 발명의 배엑기스 제조방법을 나타내는 순서도이다.1 is a flow chart showing a method for producing a vinegar extract of the present invention.

먼저, 제 1단계(S10)에서는 배를 슬러쉬화한다. 구체적으로, 주재료인 배를 세척한 다음 배엑기스 제조 시 엑기스의 균일한 농도와 분포를 위하여 슬러쉬화한다.First, in a first step (SlO), the ship is made into a slush. Specifically, the main raw material is washed and then slushed for uniform concentration and distribution of the extract in the production of a pear extract.

다음으로, 제 2단계(S20)에서는 추출기에 상기 슬러쉬한 배와 기능성 부재료 및 물을 투입한다. 구체적으로, 하기 추출작업을 위하여 추출기에 상기 슬러쉬한 배와 기능성 부재료인 초석잠, 도라지, 생강, 대추 및 물을 혼합, 투입한다.Next, in the second step S20, the slush boat, the functional material and water are introduced into the extractor. Specifically, in order to perform the following extraction operation, the above-mentioned slush boat and the functional materials such as foundation stone, bellflower, ginger, jujube, and water are mixed and injected into an extractor.

상기 초석잠은 국화과에 속하는 여러해살이 풀로, 뇌에 신선한 산소를 공급하여 머리를 총명하게 하고 치매와 뇌경색을 예방하는 약초로, 생리불순이나 생리주기 개선 등의 각종 여성질환에 도움이 된다.The cornerstone sleep is a perennial herb that belongs to the family Asteraceae. It is a medicinal herb that supplies fresh oxygen to the brain to make the head clear and prevent dementia and cerebral infarction. It is useful for various female diseases such as physiological impairment and improvement of menstrual cycle.

상기 도라지는 양치식물 초롱꽃목 초롱꽃과의 여러해살이 풀로, 사포닌이 풍부하게 들어있으며 심혈관계의 질환을 개선하고 면역력을 증진시키는 효능이 있으며, 도라지의 뿌리는 감기, 기침, 거담, 편도선 등의 약재로 이용되고 있다.The bellflower is a perennial herb that is rich in saponin and has the effect of improving the cardiovascular disease and improving the immunity, and the root of the bellflower is a medicinal substance such as cold, cough, geudam, and tonsil .

상기 생강은 외떡잎식물 생강목 생강과의 여러해살이 풀로, 약리작용으로 위액분비촉진, 소화력 증진, 심장흥분 작용, 혈액순환 촉진, 억균 작용 등이 보고되고 있으며, 혈액순환에 좋아서 몸을 따뜻하게 해주는 데 효과적이다.The ginger is a perennial plant of ginger with ginger and ginger. Its pharmacological effect promotes gastric juice secretion, promotes digestive power, stimulates the heart, promotes blood circulation, and inhibits the growth of the blood circulation. It is also effective in warming the body to be.

상기 대추는 대추나무의 열매로 과실을 생식할 뿐 아니라 채취한 후 말려 견과로서 과자, 요리 및 약용으로 쓰인다. 한방에서는 이뇨, 강장, 완화제로 사용되며 발암물질의 배출을 돕고 노화방지, 신경 이완 및 안정, 불면증 완화, 내장기능 회복, 혈액순한 개선, 면역력 증강 등의 효능이 있다.The jujube is the fruit of the jujube, which not only reproduces the fruit, but also extracts and nuts, which are used as confectionery, cooking, and medicine. It is used as a diuretic, tonic, and emollient in the oriental medicine. It helps the release of carcinogens, and has the effects of preventing aging, nervous relaxation and stabilization, relieving insomnia, restoring internal function, improving blood circulation and improving immunity.

상기 슬러쉬한 배와 부재료, 물의 혼합 시 혼합비율은 배 55중량부에 대하여 부재료(초석잠, 도라지, 생강, 대추) 25중량부, 물 20중량부인 것이 바람직하다. It is preferable that the blending ratio of the above blended slurry, the material and water is 25 parts by weight of the material (cornerstone, bellflower, ginger, jujube) and 20 parts by weight of water relative to 55 parts by weight.

상기 배 55중량부에 대하여 부재료가 25중량부를 초과할 경우 부재료인 초석잠, 도라지, 생강, 대추의 맛이 너무 강하게 느껴져 배엑기스의 전체적인 맛을 해칠 수 있으며, 25중량부 미만으로 혼합될 경우 부재료의 기능성이 충분히 배엑기스에 전달되지 않을 수 있다.If the amount of the auxiliary material exceeds 25 parts by weight with respect to 55 parts by weight of the abalone, the taste of the foundation stone, bellflower, bellflower, ginger and jujube as a sub ingredient may feel too strong to harm the overall taste of the vinegar. May not be delivered to the vinegar sufficiently.

또한, 물이 20중량부를 초과할 경우 하기에서 실시할 농축단계가 과도하게 길어질 수 있으며, 20중량부 미만일 경우 추출 시의 용매로 작용하기에 물이 양이 부족하여 원활한 추출이 어려운 문제점이 있다.When the amount of water is more than 20 parts by weight, the concentration step to be carried out below may be excessively long. When the amount of water is less than 20 parts by weight, it acts as a solvent at the time of extraction.

상기 부재료인 초석잠, 도라지, 생강, 대추는 각각의 독성, 맛, 기능성을 고려하여 초석잠 10중량부에 대하여 도라지 5중량부, 생강 5중량부, 대추 5중량부를 혼합하는 것이 가장 바람직하며, 기호 및 기능에 따라 부재료의 종류를 더 추가하여 구성할 수 있다.It is most preferable to mix 5 parts by weight of the bellflower, 5 parts by weight of the ginger and 5 parts by weight of the jujube in 10 parts by weight of the foundation stone in consideration of the toxicity, taste and functionality of the foundation stone, It is possible to further configure the kind of the material to be added according to the symbol and the function.

다음으로, 제 3단계(S30)에서는 상기 추출기를 이용하여 열수추출을 수행한다. 구체적으로, 상기 슬러쉬화한 배, 기능성 부재료 및 물이 투입된 추출기를 이용하여 일정온도에서 열수추출을 진행한다.Next, in the third step S30, hot water extraction is performed using the extractor. Specifically, the hot water extraction is carried out at a predetermined temperature using the slushing boat, the functional material, and an extractor into which water is introduced.

상기 열수추출을 수행할 시 온도는 120℃에서 6시간 동안 진행하는 것이 바람직하다. It is preferable that the temperature is 120 ° C for 6 hours when the hot water extraction is performed.

상기 열수추출 온도가 120℃를 초과하는 경우 높은 온도로 인하여 배 엑기스의 맛이 변질되거나 기능성 부재료의 이로운 성분이 파괴될 수 있으며, 120℃ 미만일 경우 충분히 부재료의 약리성분이 추출되지 않거나 추출 시간이 과도하게 길어지는 문제점이 있다.If the hot water extraction temperature exceeds 120 ° C, the taste of the vinegar extract may be deteriorated or the beneficial component of the functional ingredient may be destroyed due to the high temperature. If the temperature is less than 120 ° C, the pharmacological ingredient of the sub ingredient may not be sufficiently extracted, There is a problem that it becomes longer.

또한, 상기 열수추출 시간이 6시간 미만일 경우 부재료의 약리성분이 충분히 추출되지 않을 수 있으며, 6시간을 초과할 경우 이미 추출이 완료되어 작업의 효율성이 저하될 수 있다.In addition, if the hot water extraction time is less than 6 hours, the pharmacological components of the material may not be sufficiently extracted. If the hot water extraction time exceeds 6 hours, the extraction may be completed and the efficiency of the work may be lowered.

다음으로, 제 4단계(S40)에서는 상기 열수추출한 추출액을 여과한다. 구체적으로, 상기 열수추출을 진행한 후의 추출물에서 추출액만을 얻기 위하여 여과작업을 수행한다.Next, in the fourth step (S40), the extracted liquid extracted by the hot water is filtered. Specifically, filtration is performed to obtain only the extract from the extract after the hot water extraction.

다음으로, 제 5단계(S50)에서는 상기 여과된 추출액을 농축하여 엑기스를 제조한다. 구체적으로, 상기 열수추출한 후 여과한 추출액을 가열, 농축하여 엑기스를 제조한다.Next, in a fifth step (S50), the filtered extract is concentrated to produce an extract. Specifically, an extract is obtained by heating and concentrating the extracted liquid after the hot water extraction.

상기 농축 과정을 수행할 시 가열 온도 60℃에서, 2시간 동안 진행하는 것이 바람직하다.The concentration is preferably carried out at a heating temperature of 60 ° C for 2 hours in the course of performing the concentration process.

상기 농축 시 가열온도가 60℃미만일 경우 농축시간이 과도하게 길어지게 되어 작업의 효율성이 저하되며, 60℃가 초과할 경우 맛이 변질되거나 높은 온도로 인해 점성이 과도하게 높아질 수 있다.When the heating temperature is lower than 60 ° C, the condensation time becomes excessively long and the efficiency of the operation is deteriorated. When the heating temperature is higher than 60 ° C, the taste may deteriorate or the viscosity may become excessively high due to the high temperature.

또한, 상기 농축 시간이 2시간 미만일 경우 충분한 당도와 점성을 얻기 위한 농축이 완료되지 않을 수 있으며, 2시간을 초과할 경우 당도와 점성이 과도하게 높아지고 작업의 효율성이 저하되는 문제점이 있다.If the concentration time is less than 2 hours, the concentration for obtaining a sufficient sugar content and viscosity may not be completed. If the concentration time exceeds 2 hours, the sugar content and viscosity become excessively high and the efficiency of the operation deteriorates.

상기 농축 과정을 수행한 배엑기스의 당도는 소비자 또는 사용자의 기호도를 고려하여 11 내지 12브릭스(Brix)인 것이 바람직하다.It is preferable that the sugar extract of the extract concentrate is 11 to 12 Brix considering the preference of the consumer or the user.

다음으로, 제 6단계(S60)에서는 상기 농축한 엑기스를 여과한다. 구체적으로, 상기 농축 과정을 거쳐 제조한 엑기스에서 침전물, 불순물 등을 걸러내기 위하여 여과 작업을 수행한다.Next, in the sixth step (S60), the concentrated extract is filtered. Specifically, filtration is performed in order to filter precipitates, impurities, and the like from the extract prepared through the concentration process.

다음으로, 제 7단계(S70)에서는 상기 여과한 엑기스를 포장한다. 구체적으로, 상기 여과 과정을 거친 엑기스를 용기(팩, 병 등)에 포장하여 배엑기스의 제조를 완료한다.Next, in the seventh step S70, the filtered extract is packed. Specifically, the filtered extract is packaged in a container (pack, bottle, etc.) to complete the production of the vial extract.

하기에서는 본 발명의 배 엑기스에 기능성 부재료를 첨가하고, 그의 혼합비율을 달리하여 실험을 진행하고 실험 내용을 상세하게 설명한다.In the following, the functional ingredient is added to the extract of the present invention and the experiment is carried out by varying the mixing ratio thereof, and the contents of the experiment will be described in detail.

[비교예 1][Comparative Example 1]

비교예 1은 배엑기스 제조 시 주재료인 배만을 이용하여 추출, 농축한 배엑기스이다.Comparative Example 1 is a vial extract obtained by extracting and concentrating only the main raw material at the time of manufacturing a vulture extract.

[실시예 1][Example 1]

실시예 1은 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료 20중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 1 is a pear extract prepared by mixing 20 parts by weight of a functional ingredient and 20 parts by weight of water with respect to 55 parts by weight of a slushed pear by mixing a pear, a functional ingredient, and water at the time of preparing a pear extract.

[실시예 2][Example 2]

실시예 2는 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료 25중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 2 is a pear extract prepared by mixing a boat, a functional ingredient, and water at the time of preparing a pear extract, and mixing 25 parts by weight of a functional ingredient and 20 parts by weight of water with respect to 55 parts by weight of a slushed pear.

[실시예 3][Example 3]

실시예 3은 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료 30중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 3 is a pear extract prepared by mixing a boat, a functional ingredient, and water at the time of preparing a pear extract, and mixing 30 parts by weight of a functional ingredient and 20 parts by weight of water with respect to 55 parts by weight of a slushed pear.

상기 실시예 및 비교예에서 배엑기스 제조 시 배와 기능성 부재료, 물의 최적 혼합비율을 선정하기 위하여 관능평가를 수행하고, 그 결과를 표 1에 나타내었다.In the above Examples and Comparative Examples, sensory evaluation was carried out in order to select the optimum blending ratio of the abalone, the functional ingredient, and water at the time of preparing the bait extract, and the results are shown in Table 1.

ㄱ. 관능평가 1A. Sensory evaluation 1

배엑기스의 품질 특성을 비교하기 위하여 검사원으로서의 적합성이 인정된 식품공학과 대학원생을 선발하여 본 실험의 목적에 적합한 훈련을 시킨 후에 관능평가를 하였다. 관능검사 항목은 배엑기스의 색, 향, 맛 및 전반적인 기호도(overall acceptability)로 굉장히 좋으면 9점, 매우 나쁘면 1점으로 평가하는 9점 척도법(Liker scale)으로 실시한 후 이를 평균하여 나타내었다.In order to compare the quality characteristics of pear extracts, a graduate student of Food Science and Engineering who was recognized as an examiner was selected and tested for sensory evaluation after training suitable for the purpose of this experiment. The sensory test items were evaluated by a 9 point scoring method (Liker scale) evaluating the color, aroma, taste and overall acceptability of the pear extract as 9 points for very good and 1 point for very poor, and then averaged.

샘플 종류Sample Type 관능 특성Sensory characteristics color incense flavor 전체적인 기호도Overall likelihood 비교예 1Comparative Example 1 4.754.75 3.753.75 3.903.90 4.354.35 실시예 1Example 1 5.005.00 4.104.10 4.354.35 4.504.50 실시예 2Example 2 6.256.25 5.755.75 6.006.00 6.106.10 실시예 3Example 3 5.505.50 5.155.15 5.105.10 5.255.25

상기 표 1에 나타난 바와 같이 기능성 부재료를 첨가하지 않은 일반적인 배엑기스에 비하여 기능성 부재료를 첨가한 본 발명의 배엑기스에 대한 종합적인 기호도가 더 높았으며, 실시예 2의 경우 색상, 향, 맛, 종합적 기호도 전반에 걸쳐 가장 우수한 관능을 나타내었다.As shown in Table 1, the general preference for the extract of the present invention containing the functional ingredient was higher than that of the general extract without the functional ingredient, and in the case of Example 2, the color, flavor, taste, It showed the highest sensory performance throughout the preference.

따라서, 배엑기스에 기능성 부재료를 첨가함에 따라 맛, 식감, 색상 및 종합적 기호도를 증진시킬 수 있으며, 본 발명의 상기 제조방법에서 제시한 혼합비율이 가장 선호도가 높음을 알 수 있다.Therefore, it can be understood that the taste, texture, color, and overall acceptability can be improved by adding the functional ingredient to the vinegar extract, and the mixing ratio suggested by the manufacturing method of the present invention is the most preferable.

본 발명에서는 하기에 나타난 바와 같이 배 엑기스에 기능성 부재료를 첨가하고, 이의 혼합비율을 달리하여 실험한 내용을 상세하게 설명한다.In the present invention, as shown below, the experimental results of adding the functional ingredient to the vinegar extract and the mixing ratio thereof are described in detail.

하기에서는 본 발명의 배 엑기스에 첨가되는 기능성 부재료의 종류를 달리하여 실험을 진행하고 실험 내용을 상세하게 설명한다.In the following, experiments will be carried out with different kinds of functional materials to be added to the extract of the present invention, and the contents of the experiment will be described in detail.

[비교예 1][Comparative Example 1]

비교예 1은 배엑기스 제조 시 주재료인 배만을 이용하여 추출, 농축한 배엑기스이다.Comparative Example 1 is a vial extract obtained by extracting and concentrating only the main raw material at the time of manufacturing a vulture extract.

[실시예 4][Example 4]

실시예 4는 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료로 초석잠 25중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 4 is a pear extract prepared by mixing a boat, a functional ingredient, and water at the time of preparing a pear extract, and mixing 55 parts by weight of a slushed pear with 25 parts by weight of a base stone as a functional material and 20 parts by weight of water.

[실시예 5][Example 5]

실시예 5는 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료로 초석잠 20중량부, 도라지 5중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 5 was prepared by mixing a boat, a functional ingredient, and water at the time of preparing a pear extract, and mixing 55 parts by weight of slurry with 20 parts by weight of ground stone as a functional material, 5 parts by weight of balloon, and 20 parts by weight of water It is a pear extract.

[실시예 6][Example 6]

실시예 6은 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료로 초석잠 15중량부, 도라지 5중량부, 생강 5중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 6 was prepared by mixing a boat, a functional ingredient, and water at the time of preparing a vinegar extract. To 55 parts by weight of a slushed vinegar, 15 parts by weight of ground stone as a functional ingredient, 5 parts by weight of balloon, 5 parts by weight of ginger, Lt; / RTI >

[실시예 7][Example 7]

실시예 7은 배엑기스 제조 시 배, 기능성 부재료, 물을 혼합하여 제조하되, 슬러쉬한 배 55중량부에 대하여 기능성 부재료로 초석잠 10중량부, 도라지 5중량부, 생강 5중량부, 대추 5중량부 및 물 20중량부를 혼합하여 제조한 배엑기스이다.Example 7 was prepared by mixing a boat, a functional ingredient, and water at the time of preparing a vinegar extract. To 55 parts by weight of a slushed vinegar, 10 parts by weight of ground stone as a functional ingredient, 5 parts by weight of gypsum, 5 parts by weight of ginger, And 20 parts by weight of water.

ㄴ. 관능평가 2N. Sensory evaluation 2

배엑기스의 품질 특성을 비교하기 위하여 검사원으로서의 적합성이 인정된 식품공학과 대학원생을 선발하여 본 실험의 목적에 적합한 훈련을 시킨 후에 관능평가를 하였다. 관능검사 항목은 배엑기스의 색, 향, 맛 및 전반적인 기호도(overall acceptability)로 굉장히 좋으면 9점, 매우 나쁘면 1점으로 평가하는 9점 척도법(Liker scale)으로 실시한 후 이를 평균하여 나타내었다.In order to compare the quality characteristics of pear extracts, a graduate student of Food Science and Engineering who was recognized as an examiner was selected and tested for sensory evaluation after training suitable for the purpose of this experiment. The sensory test items were evaluated by a 9 point scoring method (Liker scale) evaluating the color, aroma, taste and overall acceptability of the pear extract as 9 points for very good and 1 point for very poor, and then averaged.

샘플 종류Sample Type 관능 특성Sensory characteristics color incense flavor 전체적인 기호도Overall likelihood 비교예 1Comparative Example 1 4.754.75 3.753.75 3.903.90 4.354.35 실시예 4Example 4 5.165.16 4.884.88 5.115.11 4.964.96 실시예 5Example 5 5.225.22 5.015.01 5.005.00 5.125.12 실시예 6Example 6 5.665.66 5.875.87 5.545.54 5.675.67 실시예 7Example 7 6.256.25 5.755.75 6.006.00 6.106.10

상기 표 1에 나타난 바와 같이 기능성 부재료를 첨가하지 않은 일반적인 배엑기스에 비하여 기능성 부재료를 첨가한 본 발명의 배엑기스에 대한 종합적인 기호도가 더 높았으며, 실시예 7의 경우 색상, 향, 맛, 종합적 기호도 전반에 걸쳐 가장 우수한 관능을 나타내었다.As shown in Table 1, the overall acceptability of the extract of the present invention containing the functional ingredient was higher than that of the common extract without addition of the functional ingredient. In the case of Example 7, color, flavor, taste, It showed the highest sensory performance throughout the preference.

따라서, 배엑기스에 기능성 부재료로 초석잠, 도라지, 생강, 대추를 혼합하는 것이 배엑기스의 맛, 식감, 색상 및 종합적 기호도를 증진시킬 수 있으며, 본 발명의 상기 제조방법에서 제시한 혼합비율이 가장 선호도가 높음을 알 수 있다.Therefore, it is possible to enhance the taste, texture, color, and overall acceptability of the vinegar extract by mixing cornstarch, bellflower, ginger and jujube with a functional ingredient in a vinegar extract. The mixing ratio proposed in the above- The preference is high.

이와 같이, 상술한 본 발명의 기술적 구성은 본 발명이 속하는 기술분야의 당업자가 본 발명의 그 기술적 사상이나 필수적 특징을 변경하지 않고서 다른 구체적인 형태로 실시될 수 있다는 것을 이해할 수 있을 것이다.As described above, it is to be understood that the technical structure of the present invention can be embodied in other specific forms without departing from the spirit and essential characteristics of the present invention.

그러므로 이상에서 기술한 실시예들은 모든 면에서 예시적인 것이며 한정적인 것이 아닌 것으로서 이해되어야 하고, 본 발명의 범위는 상기 상세한 설명보다는 후술하는 특허청구범위에 의하여 나타나며, 특허청구범위의 의미 및 범위 그리고 그 등가 개념으로부터 도출되는 모든 변경 또는 변형된 형태가 본 발명의 범위에 포함되는 것으로 해석되어야 한다.Therefore, it should be understood that the above-described embodiments are to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than the foregoing description, All changes or modifications that come within the scope of the equivalent concept are to be construed as being included within the scope of the present invention.

S10. 배를 슬러쉬화하는 제 1단계;
S20. 추출기에 상기 슬러쉬한 배, 기능성 부재료, 물을 투입하는 제 2단계
S30. 상기 추출기를 이용하여 열수추출을 수행하는 제 3단계
S40. 상기 열수추출한 추출물을 여과하여 추출액을 얻는 제 4단계
S50. 상기 여과한 추출액을 농축하여 엑기스를 얻는 제 5단계
S60. 상기 농축한 엑기스를 여과하는 제 6단계
S70. 상기 여과한 엑기스를 포장하는 제 7단계
S10. A first step of slicing the ship;
S20. A second step of injecting the slush vessel, the functional ingredient, and water into the extractor
S30. And a third step of performing hot water extraction using the extractor
S40. The fourth step of filtering the extracted hot-water extract to obtain an extract
S50. The fifth step of concentrating the filtered extract to obtain an extract
S60. And a sixth step of filtering the concentrated extract
S70. The seventh step of packaging the filtered extract

Claims (4)

배를 슬러쉬화하는 제 1단계;
추출기에 상기 슬러쉬한 배, 기능성 부재료, 물을 투입하는 제 2단계;
상기 추출기를 이용하여 열수추출을 수행하는 제 3단계;
상기 열수추출한 추출물을 여과하여 추출액을 얻는 제 4단계;
상기 여과한 추출액을 농축하여 엑기스를 얻는 제 5단계;
상기 농축한 엑기스를 여과하는 제 6단계;
상기 여과한 엑기스를 포장하는 제 7단계;를 포함하되,
상기 기능성 부재료는 초석잠, 도라지, 생강 및 대추를 포함하고,
상기 제 2단계에서 추출기에 슬러쉬한 배, 기능성 부재료, 물의 투입 시 비율은 슬러쉬한 배 55중량부에 대하여 기능성 부재료 25중량부, 물 20중량부의 비율로 혼합되며,
상기 기능성 부재료는,
초석잠 10중량부, 도라지 5중량부, 생강 5중량부, 대추 5중량부의 비율로 혼합되고,
상기 제 3단계에서 열수추출은 가열온도 120℃에서 6시간 동안 수행하고,
상기 제 5단계에서 농축은 가열온도 60℃에서 2시간 동안 수행하며,
상기 제 5단계에서 엑기스의 당도는 11 내지 12브릭스(Brix)로 하는 것을 특징으로 하는 배엑기스 제조방법
A first step of slicing the ship;
A second step of injecting the slush vessel, the functional ingredient, and water into the extractor;
A third step of performing hot water extraction using the extractor;
A fourth step of filtering the extracted hot-water extract to obtain an extract;
A fifth step of concentrating the filtered extract to obtain an extract;
A sixth step of filtering the concentrated extract;
And a seventh step of packaging the filtered extract,
Wherein the functional material includes cornerstone, bellflower, ginger and jujube,
In the second step, the amount of the blended slurry, the functional ingredient, and the water added to the extractor is mixed at a ratio of 25 parts by weight of the functional material and 20 parts by weight of water to 55 parts by weight of the slush,
The functional sub-
10 parts by weight of cornstarch, 5 parts by weight of ballad, 5 parts by weight of ginger, and 5 parts by weight of jujube,
In the third step, the hot water extraction is performed at a heating temperature of 120 ° C for 6 hours,
In the fifth step, the concentration is carried out at a heating temperature of 60 DEG C for 2 hours,
Wherein the sugar content of the extract in the fifth step is 11 to 12 Brix.
삭제delete 삭제delete 삭제delete
KR1020160082629A 2016-06-30 2016-06-30 Manufacturing method of pear extract KR101972111B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1020160082629A KR101972111B1 (en) 2016-06-30 2016-06-30 Manufacturing method of pear extract

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020160082629A KR101972111B1 (en) 2016-06-30 2016-06-30 Manufacturing method of pear extract

Publications (2)

Publication Number Publication Date
KR20180003152A KR20180003152A (en) 2018-01-09
KR101972111B1 true KR101972111B1 (en) 2019-05-23

Family

ID=61000814

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020160082629A KR101972111B1 (en) 2016-06-30 2016-06-30 Manufacturing method of pear extract

Country Status (1)

Country Link
KR (1) KR101972111B1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20200113435A (en) * 2019-03-25 2020-10-07 슬로푸드주식회사농업회사법인 Manufacturing method of pear concentrate using by-product of pear processing
KR102630382B1 (en) * 2021-01-20 2024-01-29 김상범 Method of manufacturing extraction liquid of pear and balloonflower root

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101195064B1 (en) 2010-07-29 2012-10-29 이혜진 Ginger tea composition and making method thereof

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040087172A (en) * 2003-04-04 2004-10-13 (주)한국나주배 A functional beverage of pear and its manufacturing method
KR100882710B1 (en) 2008-08-18 2009-02-06 조평운 Pear drink

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101195064B1 (en) 2010-07-29 2012-10-29 이혜진 Ginger tea composition and making method thereof

Also Published As

Publication number Publication date
KR20180003152A (en) 2018-01-09

Similar Documents

Publication Publication Date Title
CN101904384B (en) Pu'er antipyretic beverage and preparation method thereof
KR101539864B1 (en) Beverage for curing of hangover
CN104544406A (en) Chinese-date-flavor functional beverage capable of improving sleep quality of spacemen and preparation method of Chinese-date-flavor functional beverage
CN101897361A (en) A bean curd containing Chinese herbal medicines
KR20160065497A (en) Manufacturing method of beverage for relieving hangovers and the beverage
KR101972111B1 (en) Manufacturing method of pear extract
CN106173695A (en) A kind of sapodilla Herba Passiflorae Caeruleae mulse and preparation method thereof
CN106722593A (en) A kind of low sugar green tea Green plum jam and preparation method thereof
KR101721940B1 (en) Beverage including fruit wine and fruit or vegetable and preparation method thereof
CN106360198A (en) Spleen-strengthening and stomach-nourishing health-care beverage and preparation method thereof
CN107519442A (en) A kind of sorrow is escaped careless tea and preparation method thereof
KR101469495B1 (en) Mature Composition Comprising Ginger and Jujube and Preparation Method Thereof
CN104544405A (en) Litchi-flavor functional beverage capable of improving sleep quality of spacemen and preparation method of litchi-flavor functional beverage
CN103815507B (en) A kind of Folium Artemisiae Argyi beverage and production technology thereof
CN107019134A (en) A kind of syrup of plum and preparation method thereof
KR20130003496A (en) A health beverage containing the extract of gastrodiae rhizona
CN114403319A (en) Preparation method of sugar-free bubble water
CN106509532A (en) Health-care beverage for preventing and treating oral ulcer and preparation method of health-care beverage
KR20180037437A (en) Manufacture Method For Green Tea bean curd
KR20170036841A (en) A method of preparing pear beverage using apple
CN110916025A (en) Sea-buckthorn compound fruit juice beverage and preparation method thereof
CN113796417B (en) Matcha latte solid beverage with anti-drunk and sobering-up functions and preparation method thereof
CN108244436A (en) A kind of ginseng and pilose antler beverage and its preparation method and application
KR20030066539A (en) Process for preparing drink type health aid foods
CN107897603A (en) One kind Chinese mugwort fragrance coarse food grain beverage and preparation method thereof

Legal Events

Date Code Title Description
A201 Request for examination
PA0109 Patent application

Patent event code: PA01091R01D

Comment text: Patent Application

Patent event date: 20160630

PA0201 Request for examination
N231 Notification of change of applicant
PN2301 Change of applicant

Patent event date: 20160719

Comment text: Notification of Change of Applicant

Patent event code: PN23011R01D

PG1501 Laying open of application
E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20180122

Patent event code: PE09021S01D

AMND Amendment
E601 Decision to refuse application
PE0601 Decision on rejection of patent

Patent event date: 20180726

Comment text: Decision to Refuse Application

Patent event code: PE06012S01D

Patent event date: 20180122

Comment text: Notification of reason for refusal

Patent event code: PE06011S01I

AMND Amendment
PX0901 Re-examination

Patent event code: PX09011S01I

Patent event date: 20180726

Comment text: Decision to Refuse Application

Patent event code: PX09012R01I

Patent event date: 20180322

Comment text: Amendment to Specification, etc.

E90F Notification of reason for final refusal
PE0902 Notice of grounds for rejection

Comment text: Final Notice of Reason for Refusal

Patent event date: 20180913

Patent event code: PE09021S02D

AMND Amendment
PX0701 Decision of registration after re-examination

Patent event date: 20190118

Comment text: Decision to Grant Registration

Patent event code: PX07013S01D

Patent event date: 20181113

Comment text: Amendment to Specification, etc.

Patent event code: PX07012R01I

Patent event date: 20180824

Comment text: Amendment to Specification, etc.

Patent event code: PX07012R01I

Patent event date: 20180726

Comment text: Decision to Refuse Application

Patent event code: PX07011S01I

Patent event date: 20180322

Comment text: Amendment to Specification, etc.

Patent event code: PX07012R01I

X701 Decision to grant (after re-examination)
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20190418

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20190418

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
PR1001 Payment of annual fee

Payment date: 20220428

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20240213

Start annual number: 6

End annual number: 6