KR101296153B1 - Cosmetic composition for pore-minimizing using scoria - Google Patents

Abstract

The present invention relates to a cosmetic composition for shrinking pores using Jeju clusters, and Jeju clusters are effective in shrinking pores and excellent in improving keratin, because they have high far-infrared emissivity and radiation energy helps maintain moisture when used as a cosmetic.
In addition, by adding a variety of moisturizing ingredients to stabilize the moisture as well as made of a pack using purified water using an anion exchange resin. Therefore, after applying the composition for pore contraction using Jeju clusters, the user not only gave a fresh feeling, but also obtained a positive answer in the subjective evaluation of the exfoliation effect.
As confirmed through simple clinical results when using the cosmetic composition for pore contraction using Jeju clusters as described above, it may be a solution to those who are suffering from intractable skin diseases such as atopic dermatitis or severe acne. .

Description

Cosmetic composition for pore contraction using Jeju clusters {COSMETIC COMPOSITION FOR PORE-MINIMIZING USING SCORIA}

The present invention relates to a cosmetic composition for pore contraction, and more particularly, the use of cosmetics mixed with Jeju clusters maintains the stratum corneum that can prevent drying of the skin, and pores contraction using Jeju clusters to induce pores shrinkage phenomenon. It is about the cosmetic composition for.

The most important function of the skin is to protect the body from external physical and chemical factors. These skins have oil glands called sebaceous glands, from which sebum is secreted and discharged through the pores to the skin surface. The sebum thus released prevents the evaporation of water from the skin surface and serves to protect the body from bacteria.

The skin is divided into the epidermis, the dermis and the subcutaneous fat layer from the outermost layer, and at the bottom of the epidermis is the basal layer (keratinocyte), where cell differentiation continues, and the differentiated cells are eliminated through the stratum corneum, the granular layer, and the dead stratum corneum. This process is usually repeated every 28 days. If this cycle does not progress smoothly, the stratum corneum becomes thick and the skin becomes rough. Also around the pores, these keratin blocks the entrance of the pores and secreted sebum does not go out, but hardens in the pores, passing through the white head and the black head to develop acne. It can also cause infections with purulent bacteria. This repeated pore trouble affects the dermal layer around the pores, causing the pores to widen.

One of the skin's most important functions is to act as a defense against physicochemical irritation and microbial invasion between the external environment and the living organs in the body.

Dividing the factors that weaken the skin's defense function into internal and external factors include internal diseases such as disease, genetic defects, aging, etc. External factors include soap or detergent, UV (ultraviolet) rays, temperature of bad condition , Prolonged exposure in a humid environment, and poor eating habits. Due to these internal and external factors, the stratum corneum, which acts as a barrier, structurally and physiologically degenerates, thus weakening the defense function. Therefore, maintaining proper moisture so that the moisture of the stratum corneum does not fall below the proper level is essential and essential to skin physiology. The stratum corneum is composed of keratinocytes and scaffolds, and the structure of keratinocytes is mainly composed of cytoplasm consisting of keratin macromolecules and keratinocyte membranes surrounding the cytoplasm. As keratinocytes differentiate, the nucleus disappears and becomes flatter, causing the organelles to disappear and become keratinocytes. Of the substances that make up keratinocytes, the most is keratin.

Keratin accounts for 80-90% of keratinocytes and crosslinks with the keratinocyte membrane to form macrofibrils. The sebum secreted from the sebaceous glands is known to give moisture to the skin by preventing evaporation of the stratum corneum. Lipids in the stratum corneum exist in several layers between keratinocytes, and the components are ceramides, free fatty acids, cholesterol and cholesterol sulfates. Excessive sebum secretion can cause the skin to become greasy, inflamed and acne-prone, and folliculitis caused by bacterial infection. On the other hand, when the lipid on the skin surface is reduced, the skin becomes dry, and the skin disease occurs due to the dry skin.

The secretion of sebum is pores, and the appearance of pores varies depending on factors such as sex, heredity, aging, chronic UV exposure, acne, etc.

Therefore, inducing such shrinkage of the pores prevents the drying of the skin described above and becomes an essential element for the preservation and maintenance of the stratum corneum, which is a layer for maintaining sebum, but cosmetics for pore shrinkage and maintenance of the stratum corneum have not been developed.

The present invention has been made in order to solve the above problems, by using the Jeju pine clusters excellent in moisturizing, cortex and keratin improving effect as a mixture to improve the keratin, in addition to pore shrinkage by using anion firing performance and far-infrared emission effect It is an object of the present invention to provide a composition which can be obtained.

The cosmetic composition for pore contraction using the Jeju cluster according to the present invention for achieving the above object, in the cosmetic composition for shrinking pores, contains 0.1 to 80% by weight of Jeju cluster, kaolinite, montmorillonite, illite, zeolite and ocher It is heated to a temperature of 120 ~ 180 ℃ using natural ceramic mineral material, and sieved with a mesh of 300 ~ 600 mesh to saturate water-soluble ionic metal salts in a solution of organic acid and inorganic acid or mixed acid of two or more organic and inorganic acids. After the solution was prepared, 10 to 80% by weight of purified water, 0.1 to 3% by weight of propylene glycol, 0.1 to 3% by weight of butylene glycol, sodium high was removed by exchanging anions of water-soluble ionic metal salts using an anion exchange resin. 0.1 to 3% by weight of allulonate, 0.1 to 3% by weight of glycerin, 0.1 to 3% by weight of betaine, 0.1 to 3% by weight of methyl glutes-20 and 0.1 to 3% by weight of biosaccharide gum A pore shrinkage cosmetic composition for with Jeju cluster, characterized in that the.

The Jeju cluster, silicon dioxide (SiO ₂ ) 45-48% by weight, aluminum oxide (Al ₂ O ₃ ) 16-18% by weight, iron oxide (Fe ₂ O ₃ ) 11-13% by weight, Na 1-5% by weight , K may be 1 to 5% by weight, Ca 1 to 5% by weight, Mg 1 to 5% by weight and may contain 1 to 5% by weight of Ti.

The cosmetic composition for pore contraction using the Jeju clusters, Dandelion root 0,1-2 wt%, March extract 0.1-2 wt%, brown seaweed extract 0.1-2 wt%, Centella extract 0.1-2 wt%, Panthenol 0.1- 2% by weight, methyl paraffin 0.1 ~ 2% by weight, allantoin 0.1 ~ 2% by weight, tocopheryl acetate 0.1 ~ 2% by weight, disodium idiate 0.1 ~ 2% by weight, citric acid 0.1 ~ 2% by weight, sodium citrate It may further comprise any one or more components selected from 0.1 to 2% by weight.

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The Jeju pine may have a far-infrared emissivity of 0.9 or more and a radiant energy of 350 to 400 W / m 2.

According to the cosmetic composition for pore contraction using the Jeju cluster according to the present invention, since the Jeju cluster is a main component, all the advantages of the Jeju cluster can be utilized. Jeju pine volcanic stone is made of porous structure including many fine holes, so it has strong natural adsorption and sterilizing power, like charcoal baked with oak. Also, since it is composed of weak alkaline natural mineral component, it has a function of emitting a large amount of far infrared rays like ocher.

When using Jeju Mt. volcanic stone as described above, there is a large amount of far-infrared radiation effect, and has antibacterial, purifying and detoxifying functions. In addition, since it is made of a fine porous material, it has an excellent moisturizing effect, and has excellent functionality as a cosmetic by improving the unique function of keratin along with shrinkage of pores.

1 is a photograph showing an analysis image of the pores according to the present invention.
2A and 2B are graphs showing the area of the pores and the number of pores of the subject applying the cosmetic composition for shrinking pores according to the present invention on the face.
3A and 3B are graphs showing that the cosmetic composition for pore contraction using Jeju clusters according to the present invention is applied to the face of a subject.
4 is a graph showing the degree of skin scaling.
5A and 5B are scanning electron microscope (SEM) micrographs showing pore contraction before and after using the cosmetic composition for pore contraction using Jeju clusters according to the present invention.
Figure 6 is a graph showing the results of testing the subject's subjective evaluation of the subject for the cosmetic composition for pores contraction using Jeju clusters according to the present invention.

Hereinafter, the present invention will be described more specifically.

The present invention comprises a Jeju cluster which is a volcanic stone in the cosmetic composition for pore contraction using Jeju clusters, and preferably contains 0.1 to 80% by weight relative to the total weight of the cosmetic composition for pores contraction.

Jeju volcano, the volcanic stone, is composed of plagioclase, pyroxene, and hematite, and the total content of SiO ₂ + Al ₂ O ₃ + Fe ₂ O ₃ reaches 72 to 79%. . Jeju cluster, which is a porous mineral showing the above properties, contains a lot of minerals, so it can be used as a cluster or various functional cosmetics. In particular, the cluster has a strong affinity with water, and the range of application is varied, and when using the cluster, the pH is 7.2 ~ 7.8, showing a weak alkaline property. The pH of 7.2-7.8 is similar to the body's pH index, so it is very compatible with the human body.

Hereinafter, the physical properties of Jeju clusters will be described first, and how the following physical properties cause pore shrinkage effect and how keratin improvement effect will be described in detail.

Kinds Jeju Songi china clay Zeolite jade Elvan ocher Charcoal Far-infrared emissivity 0.92-0.93 0.93 0.90 0.91 0.90 0.91 0.85 Radiation energy (W / m ² ) 374 - - - 355 353 Hair removal rate 96.7 96.0 85.0 57-72 85 / 4hr - - Antimicrobial activity 99.97 97.0 92.0 67-80 85 - -

Table 1 is a table showing far-infrared emissivity, radiation energy (W / m ² ), deodorization rate and antimicrobial properties of Jeju pine according to the present invention in comparison with other minerals. Judging from Table 1, it can be said that Jeju Mt. has far-infrared emissivity of 0.9 or more and radiation energy of 350-400 W / m 2.

Jeju Song-yi is a red natural porous ceramic made of solidified lava that first erupted when the volcano erupted. When the volcano first erupts, gas and lava that have a higher temperature are ejected first, at the same temperature as when the cider was opened at a higher temperature, with lower carbon dioxide solubility. In this process, it is made of porous structure including many fine holes, so it has strong natural flaw and sterilization power like charcoal roasted oak. Since it contains a weak alkaline natural mineral, it emits a large amount of far-infrared rays like ocher has.

Far infrared rays belong to the category of infrared rays, infrared rays having a longer wavelength than the red region of visible light and having the greatest thermal effect are called far infrared rays. The role of far infrared rays is to promote blood circulation, to promote metabolism, to activate cell function, to promote growth, to activate water molecules and to mature.

Looking at the effect of far infrared rays on the human body keeps the body temperature at an appropriate temperature. It also plays a role in promoting the growth of each organ of the human body. It also balances the supply of nutrients in the human body. In particular, when used as a cosmetic material that emits far-infrared rays plays a role in maintaining the moisture that is easily lacking in the keratin. It also promotes the excretion of wastes from human activities and neutralizes odors.

In the case of the cosmetic composition for pores shrinkage using the Jeju clusters according to the present invention, Jeju clusters 0.1 to 80% by weight, purified water 10 to 80% by weight, propylene glycol 0.1 to 3% by weight, butylene glycol 0.1 to 3% by weight, sodium It comprises 0.1 to 3% by weight of hyaluronate, 0.1 to 3% by weight of glycerin, 0.1 to 3% by weight of betaine, 0.1 to 3% by weight of methyl glutes-20 and 0.1 to 3% by weight of biosaccharide gum. It is done.

Ingredients that can be added as optional components here are 0,1-2 wt% of Dandelion root, 0.1-2 wt% of brown seaweed extract, 0.1-2 wt% of Portulaca oleracea extract, 0.1-2 wt% of Centella extract, Panthenol 0.1 ~ 2 wt%, methyl paraffin 0.1-2 wt%, allantoin 0.1-2 wt%, tocopheryl acetate 0.1-2 wt%, disodium ethane, 0.1-2 wt%, citric acid 0.1-2 wt%, sodium sheet It may be one containing any one or more components selected from the rate of 0.1 to 2% by weight. In this case, the mixing ratio of the Jeju cluster, purified water, propylene glycol, butylene glycol, sodium hyaluronate, glycerin, betaine, methyl gluses-20 and biosaccharide gum is limited as described above. It is because the optimum prescription range is less than the minimum value according to the function of each raw material, it is difficult to properly exhibit the function of the raw material, and when the maximum value is exceeded, the formulation is not stable or the feeling of use decreases.

Skin can be said to perform the barrier function of the human body. However, the defense function of the skin is performed by the stratum corneum, the outermost layer of the skin, and the fat film of the skin assists in maintaining this moisture function. Maintaining an appropriate amount of moisture in the stratum corneum is very important for maintaining the elasticity and flexibility of the skin. Normal skin contains about 30% water or water-soluble components. If the water content in the stratum corneum falls below 10%, dry skin may develop, resulting in cracked or rough skin.

The mechanism by which keratinocytes are eliminated from the skin is not fully understood, but lipids, hydrolases, glycoprotein layers, and corneodesmosomes in the stratum corneum are all involved.

In order to maintain healthy skin, lipids between sebum and keratinocytes must be balanced with natural moisturizing factor (NMF). The pores that secrete sebum are present throughout the skin of the face, and the nose and cheeks in particular can be visually identified.

The composition of the cosmetic composition for pore contraction using the Jeju cluster according to the present invention for balancing the lipids between the sebum and keratinocytes as described above is as follows.

In the case of Jeju cluster according to the present invention, the constituents are 45 to 48 wt% of silicon oxide (SiO ₂ ), 16 to 18 wt% of aluminum oxide (Al ₂ O ₃ ), and 11 to 13 wt% of iron oxide (Fe ₂ O ₃ ). 1 to 5 wt% of Na, 1 to 5 wt% of K, 1 to 5 wt% of Ca, 1 to 5 wt% of Mg, and 1 to 5 wt% of Ti.

Mn 1-5 weight% or P 1-5 weight% may be included here.

0.1-80 wt% of purified water is added to the Jeju cluster having the composition described above. The outline of the purified water added is as follows.

Purified water, also called mineral water, refers to inorganic salts, and refers to the inorganic components of organisms other than the three elements such as carbon, hydrogen, and oxygen. Also known as minerals, it is one of the five nutrients along with protein, fat, carbohydrates and vitamins. It participates in various physiological activities in the human body. Among inorganic salts, elements such as Ca, P, K, Na, Cl, Mg, Fe, I, Cu, Zn, Co, and Mn, which constitute the human body, are sufficient in small amounts but are indispensable. Therefore, insufficient intake of the inorganic salts cause various deficiencies.

As a raw material used in the production of purified water of the present invention, natural minerals such as kaolinite, montmorillonite, illite, zeolite, loess and the like may be used as the main raw materials. The natural ceramic is a natural inorganic material collected naturally from soil, mine, etc., except for the special minerals of soils in Korea and around the world, most of which are present in the form of metal oxides or elements. For example, metals in the form of oxides such as silicon oxide, aluminum oxide, iron oxide, titanium oxide, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, zinc oxide, manganese oxide, sulfur, cobalt, copper, molybdenum, nickel, It exists in the form of about 20 kinds of elements such as zinc selenium and germanium. The mineral powder (ceramic powder), which is a collection of these metal oxides or metal elements, is heated and dried for about 1 hour or more at a temperature of 120 to 180 ° C, sieved through a 300 to 600 mesh sieve, and pulverized into a fine powder. The smaller the powder particles, the higher the solubility and mineral content.

After pulverizing into fine powder, a saturated aqueous solution of ionic metal salt is prepared in a solution of one or two or more mixed acids of organic acids such as acetic acid and hydrochloric acid, nitric acid, phosphoric acid, hydrofluoric acid and perchloric acid. At this time, the concentration of the acid may be selected from the range of 1N solution in concentrated acid (Conc Acid). Meanwhile, dissolution and extraction in alkali dissolve metal oxides and elements in inorganic alkali solutions such as potassium hydroxide, ammonium hydroxide, sodium carbonate and potassium carbonate to prepare a water-soluble saturated ionic metal salt solution.

Acid and alkali can also be used together as needed. This is because the physical properties of the metal that are dissolved or salts may vary depending on the type of metal.

The anion exchange resin used here was used as Amberlite IRA 410 chloride foam and hydroxide foam of Aldrich, USA, and Samlite's Trilite SAR 10 chloride foam and hydroxide were used as domestic products. Foam was used.

The anion of the ionic water-soluble metal salt of the anion exchange resin using _{^{Cl -, NO 3-, SO 4}} 2-, PO 4 3-, OH - removed by exchanging the anions of the like, and cations of a metal ion, that is, mineral ions Silver extraction is facilitated, and the solution treated as described above is prepared with a purified water stock solution that contains various kinds of minerals evenly depending on the type of mineral material.

By adjusting the purified water stock solution with distilled water, it is possible to prepare non-toxic natural pure purified water which can be diluted and added as necessary for food additives or drinking water, beverages and various foods or cosmetics, mineral fertilizers for crop cultivation, animal feed, etc. according to the use. Do.

Propylene glycol is a chemical formula C ₃ H ₈ O ₂ , specific gravity is 1.036 ~ 1.040, boiling point is 185 ~ 189 ℃. It is mixed with water, alcohol, acetone, ethyl acetate, chloroform, ether and the like and dissolves gasoline and is not mixed with petroleum ether and paraffin. Hygroscopic, but not volatile. Stable to heat and sunlight, but flammable (flash point 104 ℃).

Compared with glycerin, it has excellent solubility, prevents the growth of mold and prevents fermentation and can be used as a food solvent. It is used as a solvent for dissolving pigments, essential oils and resins and mixing them into water again. The aqueous solution is used as an antifreeze solution. It is used as an agent for bread and moisturizer and for shortening, and as a softener for food, cellophane and cork. It is also used for emulsifying fragrances, emulsion stabilizers, preservatives, air sterilization, and also for the extraction of natural flavors such as vanilla and soybeans.

Butylene glycol is an organic molecule consisting of two alcohol groups.

Originally, alcohol evaporates moisture quickly from the skin, but butyleneglycol, a large-sized organic alcohol, has the ability to attract moisture, which is less dangerous to the skin. Butylene glycol is particularly dangerous to the skin because it has the ability to attract moisture.

In other words, butylene glycol is a highly absorbent moisturizer, and is used because it is less sticky with a fresh feeling than glycerin.

Butylene glycol (BG or 1,3-butylene Glycol) is a viscous liquid with almost no smell and a sweet taste. It is a type of polyol having two hydrophilic hydroxyl groups (-OH), which is moisturizing. It is found in non-wine, aged cheese, rat liver, soil yeast, corn oil, sunflower oil, and fish liver oil. It is also found in alcoholic fermentation and lactose fermentation products.

Moisturizers, solvents, etc. for various creams, lotions, aerosol products, toothpastes, etc., as they have moderate wettability, good solubility and antibacterial properties, less irritation and toxicity to the skin, and less stickiness with a clean feeling than glycerin. It is widely used as a perfume retention agent.

Sodium hyaluronate is a sodium salt of hyaluronic acid. Hyaluronic acid is a type of acidic mucopolysaccharide formed by combining N-acetylglucosamine and gluconic acid, and one molecule attracts 214 water molecules. It creates bound water that does not evaporate easily at high temperatures and does not freeze well even at low temperatures, stores moisture in intercellular spaces, and maintains the structure of cells. It is widely distributed in mammalian connective tissues with chondroitin sulfate, etc., and its function in connective tissues retains moisture in cell gaps, and forms a gel-like matrix in tissues to maintain cells and have lubricity and flexibility of skin. do. It also functions to prevent external forces and bacterial infections. Among the above-mentioned functions, the greatest function helps to keep the skin smooth by enhancing the moisturizing power.

Glycerin is a formula C ₃ H ₅ (OH) ₃ , molecular weight 92.10 and is also called glycerol. As can be seen from the acidic formula, it is a trihydric alcohol, and hydrolysis of glyceride, a main component of triglycerides, results in fatty acids and glycerin.

The properties of glycerin are colorless and transparent. It is a slightly viscous liquid. Melting point is crystallized at low temperature to 17 ℃. The boiling point boils at high temperature to 290 ° C. Hygroscopicity is strong and mixed with water and ethanol arbitrarily.

In order to produce glycerin, it may be produced by hydrolysis of fats and oils or may be synthesized using propylene as a raw material.

Betaine is an amino acid with three methyl groups. The methyl donation promotes the synthesis of methionine, which acts as anti-interstitial and blood pressure lowering, anti-glycemic, visual acuity, detoxification, and cell replication.

A white crystal with the chemical formula C ₅ H ₁₁ NO _{2. It} has a slight odor and sweet taste. Betaine is a natural amino acid betaine obtained by separating and purifying molasses of Myeongju and beets when used as a food additive. Soluble in water, pH of aqueous solution is 5.0 ~ 7.0. Used as a seasoning in processed fish products with squid and octopus.

Betaine is widely distributed in the flora and fauna, but less than 0.1% in the muscles of fish, but invertebrates such as squid, octopus, shrimp, etc. are contained more than fish, in addition to beet, legumes, radish, wolfberry.

Methyl Gluses-20 is a substance used as an ingredient in anti-sticking and moisturizing agents. It is known that as the content of methyl glutes-20 increases, the stickiness decreases. However, when the content of methyl glutes-20 is increased to more than 3% by weight, the freshness disappears.

Biosaccharide Gum is one of the polysaccharides and is a kind of skin conditioning agent. Polysaccharides are often found in nature in a form conforming to fiber morphology. Polysaccharides as described above include cellulose, hemicellulose, chitin, chitosan, guargirl, pectin, alginate, radish, xanthan, starch, amylose, amylopectin, alternane, gellan and the like.

A mixing operation for the cosmetic composition for pore shrinkage having a composition as described above is required. As additional ingredients, Dandelion root 0,1-2 wt%, brown seaweed extract 0.1-2 wt%, portulaca extract 0.1-2 wt%, centella extract 0.1-2 wt%, panthenol 0.1-2 wt%, methyl paraffin 0.1 ~ 2% by weight, Allantoin 0.1-2% by weight, Tocopheryl acetate 0.1-2% by weight, Disodium IDT 0.1-2% by weight, Citric acid 0.1-2% by weight, Sodium citrate 0.1-2% by weight It may include any one or more components.

Taraxacum rootic acid (taraxacum Officinale rhizome) is used as a skin conditioning agent in cosmetics. Algae extract (algae extract) is an ingredient extracted from seaweed contains a large amount of minera, vitamins, amino acids, etc., and also has excellent moisturizing power.

Centella asiatica extract is extracted from the outpost of Centella alatica. Centella asiatica extract contains a component called madecaic acid, which is a component that has been spotlighted as a skin regeneration effect in modern medicine, and is excellent in wound healing, blood circulation promoting effect, and anti-wrinkle effect.

Machi Prefecture Extract is a substance extracted from Machi Prefecture. Machi-hyun is because the leaf shape of the grass resembles the teeth of a horse, so people called it Machi-hyun and we call it purslane. Machi prefecture is called Jangmyeongchae because it is healthy for a long time.

March's outpost contains large amounts of noradrenaline and large amounts of potassium salt. It also contains alkaloids, coumarins, flavonoids, cardiac glycosides and anthraquinone glycosides (anthraquinone), which not only help prevent antioxidants but also help prevent and soothe dryness of the skin. Moisturizing

Panthenol is a provitamin of pantothenic acid (vitamin B), a substance that turns into vitamins in the body. Improves skin's moisturizing function and stimulates skin regeneration, leaving dry skin soft and elastic. It is also widely used to prevent inflammation and itching. Panthenol turns into pantothenic acid when it is absorbed into skin cells. This pantothenic acid promotes the growth of new cells and binds moisture to act as a moisturizer.

Methyl paraffin is a basic preservative in cosmetics. Allantoin is the final product of purine and pyrimidine targets and is found in the ureters and urine of certain mammals, gastropods, and insects. Tocopheryl acetate is an ester of tocopherol and acetic acid. Used as an antioxidant and skin conditioning agent.

Disoium EDTA is called a metal ion sequestrant. It plays a role in preventing metal from being rancid. It is also found in natural minerals, and it is necessary to block metals such as magnesium and sodium to ensure stability (degradation of composition, oxidation and bacterial infection). Citric acid is also called citric acid as an exfoliant.

Sodium citrate is the sodium salt of citric acid. It is also used as a pH regulator and as a metal ion sequestrant.

Hereinafter, the action and effect of the cosmetic composition for pore contraction using the Jeju cluster according to the present invention will be described in detail.

First, it is heated at 120 ~ 180 ° C, and the iron oxide component is removed with a magnetic remover for the Jeju cluster where fine particles are extracted through sieving. Jeju clusters with iron oxide components removed are sterilized and used as cosmetic ingredients.

10-80% by weight of purified water containing various kinds of minerals prepared using anion exchange resin is mixed with 0.1-80% by weight of Jeju pine mushroom, in which the iron oxide component is enhanced. In addition, 0.1 to 3% by weight of propylene glycol, 0.1 to 3% by weight of butylene glycol, 0.1 to 3% by weight of sodium hyaluronate, 0.1 to 3% by weight of glycerin, beta 0.1 to 3% by weight phosphorus, 0.1 to 3% by weight methylgluse-20, and 0.1 to 3% by weight biosaccharide gum are added.

The cosmetic composition for pore shrinkage using the thus prepared Jeju clusters is prepared in various forms. The various types of preparation methods include emulsions, lotions, creams (water droplets, oil droplets, multiphase), solutions, suspensions (anhydrous and water based), anhydrous products (oil and glycle), gels, mask packs, distributions. And other formulations.

In the present invention, the cosmetic composition comprising the Jeju matsutake powder and the cosmetic composition does not contain the Jeju matsutake powder in the conventional cosmetic ingredients, and the two compositions are clinically administered to patients with atopic dermatitis or acne symptoms The experiment was conducted to compare the degree of improvement of the diseases.

Here, the improvement of atopic dermatitis was confirmed by how low the atopic dermatitis index (EASI score) is (the higher the atopic dermatitis index is lower, the better the effect of atopic dermatitis), and the acne improvement is the clinical improvement and acne. The antimicrobial effect on the bacteria (propionibacterium acnes) and the inhibitory activity of 5a-reductase, which is known to be involved in the production of excess sebum, were confirmed.

Acne detailed in the present invention is defined to include diseases classified as acne in the art regardless of a direct cause of the occurrence. As shown in the following examples of the present invention, a clinical trial was conducted on 60 subjects with a randomly selected acne disease, and the clinical trial results showed that the case of the subject using the composition for pore contraction using Jeju cluster according to the present invention. Acne symptoms showed a tendency to improve.

Acne as used herein refers to collective acne, acne caused by bromide, congoblate acne, acne by using cosmetics, acne by using detergent, teat acne acne, youth acne, glare acne (acne fulminans) ), Acne furunculoid, halogenated acne, cleansing acne, keloid acne, physical stimulus acne, drug acne, necrotic acne, lip acne, neonatal acne (acne nconatorum), oily acne ( It is understood to include acne oil, pomade acne, premenstrual acne, acne rowacea, tropical acne, addictive acne, vulgar acne and the like.

In addition, atopic dermatitis referred to herein is defined to include diseases classified as atopic dermatitis in the art, regardless of the direct or indirect causes of atopic dermatitis. Atopic dermatitis is generally classified into infantile atopic dermatitis, pediatric atopic dermatitis, adult atopic dermatitis, and maternal dermatitis, depending on the time of onset or the subject of the onset.

Hereinafter, with reference to the accompanying drawings will be described in detail a preferred embodiment according to the present invention. However, it should be understood that the following embodiments are provided so that those skilled in the art can understand the present invention without departing from the scope and spirit of the present invention. It is not. Wherein like reference numerals refer to like elements throughout.

(Example)

The cosmetic composition for pore contraction using Jeju clusters according to the present invention was prepared in powder form. In this case, the mesh used was sieved using 1300 mesh, and the particle size obtained through the sieved was obtained at 1 μm or less. Purified water was mixed and stirred with respect to the finely ground Jeju clusters.

Jeju propylene glycol is mixed with propylene glycol, butylene glycol, sodium hyaluronate, glycerin, betaine, methyl gluse-20, and biosaccharide gum, which serve as a moisturizing agent, for the mixture of purified water and Jeju cluster. A cosmetic composition for pore contraction was prepared.

The gel-type composition prepared was spread evenly on the right face avoiding the eye area using a pack brush. After 20 minutes, when the test product was hardened, the test product was washed with lukewarm water and washed.

Ten subjects were tested, and the subjects entered the room after washing the face, rested under constant temperature and humidity conditions (22 ± 2 ℃, 50 ± 5%) for 20 minutes, and participated in the test. Immediately after use, pore shrinkage, angular mass improvement, and questionnaire evaluation and safety evaluation by the subject were performed.

The equipment used to analyze the area and number of skin pores was a facial stage DM-3 device made by Moritex (Jp). Subjects were examined on the forearm and forehead of the front face.

1 is a photograph showing an analysis image of the pores according to the present invention.

Referring to FIG. 1, an enlarged view of the right 빰 portion can be seen. It is possible to measure the distribution and size of the pores by using a magnification of the image obtained as described above.

At this time, the program used for statistical analysis is SPSS (statistical packages for the social sciences). SPSS statistical analysis is a statistical specialty program for easily and conveniently analyzing various data obtained from the social science field using a computer.

SPSS statistical methods perform tasks such as data entry and management, aggregation, and statistical analysis. The results of the analysis are clearly displayed in tables and graphs. Complex multivariate analysis is possible, including cross analysis, correlation analysis, regression analysis, analysis of variance, discriminant analysis, and factor analysis. Two of the most popular statistical packages are SPSS and Statistical Analysis System (SAS). SPSS, which adopts a general program interface, is generally more convenient to use than SAS, which is a direct command input method.

In particular, the paired t-test method of the SPSS program package 11.5 was used for analyzing the results of applying the cosmetic composition for pore contraction using the Jeju cluster according to the present invention to the face.

The paired t-test method is used to analyze the difference in means between two groups that are not independent of each other. The paired t-test method is used to analyze the example in the question addition.

The t-test is a statistical test that normalizes the mean difference between two groups to the variance of the two groups. There are two cases when the variances of the two groups are the same and the variances of the two groups are not the same. The unpaired t-test with respect to the paired t-test is an analysis method that is required when analyzing the difference between the means of two independent groups. For simplicity, paired t-test is used when there are two dependent variables. This method is used to analyze the difference caused by two variables for two paired variables.

The equation used for the t-test is Equation 1.

Using Equation 1, it is possible to calculate the rate of increase or decrease of the measured value immediately after use in comparison with before using the product.

Comparing the pore shrinkage analysis is as follows. As a result of analyzing the area and number of pores, the area just after use decreased 6.65%. The number of pores is reduced by 6.62%, it is possible to determine that the cosmetic composition for pores shrinkage using the Jeju cluster according to the present invention to shrink and reduce the pores.

Table 1 is a table showing the area and the number of pores shrinkage according to the present invention.

Item time Subject Average Standard Deviation SEM p-value Decrease (%) The area of pores Before procedure 10 40.60 24.92 7.88 - - After procedure 10 37.90 22.79 7.21 0.05 6.65 ▼ Number of pores Before procedure 10 335.50 171.85 54.34 - - After procedure 10 313.30 155.80 49.27 0.025 * 6.62 ▼

* Indicates that the p-value is less than 0.05, and the data is out of the significance level, and it is effective in reducing the number of pores as well as shrinking pores when the cosmetic composition for pores shrinkage using Jeju pine is applied to the user's face. It can be said.

2A and 2B are graphs showing the area of the pores and the number of pores of the subject applying the cosmetic composition for shrinking pores according to the present invention on the face.

2A and 2B, it is possible to determine that the cosmetic composition for pores shrinkage is effective in shrinking pores and reducing the number of pores.

3A and 3B are graphs showing that the cosmetic composition for pore contraction using Jeju clusters according to the present invention is applied to the face of a subject.

Referring to Figure 3a and 3b, it can be seen that the number of pores was reduced compared to before applying the cosmetic composition for shrinking pores using Jeju clusters.

In addition, using the Black D-quame® analysis system made by CuDerm (USA) at the time before and immediately after using the product, the body mass index (Body Mass Image) was taken after taking a 700-time digital photograph of the keratin microscope on the left frontal area. BMI) analysis software was used to determine the area of keratin (pixel).

As a result of the angular mass spectrometry, the reduction rate was significantly reduced to 29.50% immediately after use. Table 2 is a table showing the degree of skin scaling according to the administration of the cosmetic composition for pore contraction using the Jeju cluster according to the invention.

Item Time Test embroidery Average (1/1000) Standard Deviation SEM p-value Reduction rate Skin Scaling I'm 10 20.95 5.70 1.80 - - after 10 14.77 2.81 0.89 0.006 * 29.50 ▼

4 is a graph showing the degree of skin scaling.

Referring to FIG. 4, in the case of the cosmetic composition for pore contraction using Jeju clusters according to the present invention, the number of pixels may be significantly reduced.

When the statistical analysis was performed in the same way as the effect of the pores shrinkage, the p-value was found to be 0.05 or less, which is a significant level. Therefore, it can be said that the cosmetic composition for pores contraction using Jeju matsutake according to the present invention is effective for keratin improvement. .

5A and 5B are scanning electron microscope (SEM) micrographs showing pore contraction before and after using the cosmetic composition for pore contraction using Jeju clusters according to the present invention.

Referring to FIGS. 5A and 5B, since the pores contracted or the number of pores was reduced, black portions were reduced, and it is possible to determine the effect of shrinking pores and reducing the number of pores from the photograph.

Figure 6 is a graph showing the results of testing the subject's subjective evaluation of the subject for the cosmetic composition for pores contraction using Jeju clusters according to the present invention.

Referring to Figure 6, the subject's satisfaction is divided into 1 to 5 levels 1. Very much. 2 No. 3. It is normal. 4. Yes. 5. The evaluation was made very differently, and the test result of the subject showed that the positive evaluation of the angular mass improvement and smoothness items was obtained.

In the above described the present invention based on the preferred embodiment, the present invention is not limited to the above embodiment, various modifications by those skilled in the art within the scope of the technical idea of the present invention This is possible.

Claims (5)

In the cosmetic composition for pore shrinkage,
Natural ceramic minerals, including 0.1-80% by weight of Jeju pine, kaolinite, montmorillonite, illite, zeolite and ocher, are heated at a temperature of 120-180 ° C, sieved with a mesh of 300-600 mesh, 10 to 80% by weight of purified water removed by preparing an aqueous saturated aqueous solution of an ionic metal salt in an inorganic acid, or a mixed acid solution of an organic acid and an inorganic acid of two or more, and exchanging anions of the water-soluble ionic metal salts using an anion exchange resin. , Propylene glycol 0.1-3 wt%, Butylene glycol 0.1-3 wt%, Sodium hyaluronate 0.1-3 wt%, Glycerin 0.1-3 wt%, Betaine 0.1-3 wt%, Methyl glutes-20 Cosmetic composition for pore contraction using Jeju clusters, characterized in that it comprises 0.1 to 3% by weight and biosaccharide gum 0.1 to 3% by weight. The method of claim 1, wherein the Jeju clusters,
45 to 48% by weight of silicon dioxide (SiO ₂ ), 16 to 18% by weight of aluminum oxide (Al ₂ O ₃ ), 11 to 13% by weight of iron oxide (Fe ₂ O ₃ ), Na 1 to 5% by weight, K 1 to 5 Cosmetic composition for pore contraction using Jeju clusters, comprising a weight%, Ca 1-5% by weight, Mg 1-5% by weight and Ti 1-5% by weight. The method according to claim 1 or 2,
The cosmetic composition for pore contraction using the Jeju clusters, Dandelion root 0,1-2 wt%, March extract 0.1-2 wt%, brown seaweed extract 0.1-2 wt%, Centella extract 0.1-2 wt%, Panthenol 0.1- 2% by weight, methyl paraffin 0.1 ~ 2% by weight, allantoin 0.1 ~ 2% by weight, tocopheryl acetate 0.1 ~ 2% by weight, disodium idiate 0.1 ~ 2% by weight, citric acid 0.1 ~ 2% by weight, sodium citrate Cosmetic composition for pore contraction using Jeju clusters, characterized in that it further comprises any one or more components selected from 0.1 to 2% by weight. delete The method of claim 1,
The Jeju cluster is a far-infrared emissivity of 0.9 or more, the radiation energy is 350 ~ 400W / ㎡ a cosmetic composition for pore contractions using Jeju clusters, characterized in that.

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