KR101144773B1 - A processing method of liquid for anti-bacterial and anti-aging and whitening care - Google Patents

Abstract

The present invention relates to a method for producing a complex functional sap for cosmetics by mixing and stirring selenium and marine deep water and natural herbal extract extracted from deep sea water and squid intestine. Pretreatment step of sorting the remaining internal organs after separation and removal, washing with alkaline electrolyzed water and disinfecting with acidic electrolyzed water; Incineration process in which pre-treated squid intestines are first dried at a moisture content of 10-20% and incinerated second in an incineration furnace to extract minerals; A selenium separation and purification step of removing foreign substances from the extracted inorganic substance and separating and purifying selenium having a purity of 10-20% using gas chromatography (Gas Chromatography); It is characterized in that it comprises a stirred manufacturing process for preparing a sap by mixing and stirring the separated and purified selenium 0.1% to 92.9 to 94.9% by weight deep sea water and 5.0 to 7.0% by weight natural herbal extract.

Description

A process for producing antibacterial anti-aging whitening complex functional sap for cosmetics {A PROCESSING METHOD OF LIQUID FOR ANTI-BACTERIAL AND ANTI-AGING AND WHITENING CARE}

The present invention relates to a method for producing a complex functional sap by mixing and stirring selenium and natural herbal extracts extracted from deep sea water and squid gut. More specifically, the squid gut which is a by-product of squid (Mok bag, gill, heart) , Visceral sac) extracted from selenium and deep sea water and natural herbal extracts in an appropriate ratio and stirred, and relates to a method for producing antibacterial anti-aging whitening complex functional sap and sap prepared accordingly.

Skin is the largest organ in the human body, its size is about 1.6㎡, and it is a large organ that weighs 16% of its weight by weight. The skin serves as the most basic skin covering the body to protect internal organs. In addition, it is a very important institution that performs many functions.

The skin is constantly in contact with changes in the external environment such as ultraviolet rays, temperature changes, moisture, dust, and air pollution, and it is important to protect the individual by quickly reading the information essential for survival and allowing the body to react appropriately. On its mission, it has additional functions to protect the skin itself to some extent from external harm.

However, as we get older, our skin cannot deny the inherent loss of its own function, and in order to supplement it, we have to borrow the power of cosmetics following the consumption of food.

The close association between aging and oxidation is well known in many studies.

In particular, it is known that wrinkling caused by aging of the skin and blackening phenomena such as local spots and blemishes are correlated with this oxidation phenomenon. And genetic factors due to the shape of the muscles and the constant relaxation of the muscles. Furthermore, it can be divided into external factors due to environmental pollution and stress.

Skin aging caused by various factors such as keratin production, decreased fibroblast division, decreased collagen synthesis, decreased hyaluronic acid production, increased signal transduction of melanin production, wrinkles, blemishes and freckles And blemishes gradually increase.

In order to improve such skin aging, AHA, retinoic acid, retinol, ascorbic acid and the like have been mainly used to apply the herbal extracts containing the antioxidant polyphenols.

According to research from the National Fisheries Research and Development Agency, squid contains protein, ash, calcium, phosphorus, etc. It is richer in protein than meat meat, has good digestibility, and contains a large amount of minerals such as vitamins and selenium.

Selenium, which is widely distributed in the squid gut, is an essential mineral for our body and is an important component of antioxidant enzymes that protect cells from free radicals generated during normal oxygen metabolism.

This can be said to be an essential ingredient for the normal functioning of the immune system. Therefore, if it is extracted, purified and emulsified in the internal organs, a squid by-product, to be absorbed into the body through the skin, The research could be more active.

In addition, researches and product launches of natural cosmetics, which are made by mixing natural herbal extracts and antibacterial functional additives to help wrinkle improvement, skin elasticity and whitening, are actively underway.

Currently, functional cosmetics in Korea are categorized into three categories: Wrinkle improvement products, whitening products, and UV protection products recognized by the Korea Food and Drug Administration through the review of functional cosmetics. As a product for improving functional anti-wrinkle with the addition of an antioxidant functional composition, it is being developed and marketed and relatively expensive products are the mainstream.

Therefore, the present invention relates to a method for producing a sap that can give a complex functionality by using natural herbal extracts selenium extracted from deep sea water and squid by-products internal organs, skin aging and lack of elasticity and whitening with age A sap that satisfies the preferences of the elderly and the general consumers who need antibacterial and moisturizing skin as well as extracts of deep seawater and squid by-products that can be mass-produced and distributed for sale. Antibacterial anti-aging using selenium and natural herbal medicines It is an object of the present invention to provide a method for preparing a whitening complex functional sap.

In order to solve the object of the functional improvement of the skin as described above, the method for producing the antibacterial anti-aging whitening complex sap of the present invention is to squid and collect the squid body internal organs and to remove the anal part, the remaining internal organs ( Pretreatment step of selectively collecting the ink sacs, gills, heart, visceral sac), washing them with alkaline electrolyzed water and disinfecting them with acidic electrolyzed water; Incineration process in which pre-treated squid intestines are first dried at a moisture content of 10-20% and incinerated second in an incineration furnace to extract minerals; A selenium separation and purification step of removing foreign substances from the extracted inorganic matter and separating and purifying selenium having a purity of 10-20% using gas chromatography (GasChromatography); It comprises a stirred manufacturing process for mixing and stirring the separated and purified selenium 0.1% to 92.9% to 94.9% by weight of deep sea water and 5.0 to 7.0% by weight of the natural herbal extracts.

In addition, the washing process in the alkaline electrolyzed water of the pretreatment step in the method for producing a multi-functional sap of the present invention is characterized in that it is immersed for 5-15 minutes in a pH 10.5-11.5 strong alkaline electrolytic water of 2-5 times the weight of the squid gut. do.

 In addition, the process of sterilizing and disinfecting the acidic electrolyzed water of the pretreatment step in the method of producing a multi-functional sap of the present invention is 5 to 5 to 2.5 to 3.5 strong acidic electrolytic water of pH 2.5-3.5 with respect to the weight of the squid internal organs It is characterized by immersion in -15 minutes.

In addition, the natural herbal extract of the stirring step in the manufacturing method of the multifunctional sap of the present invention is rosehip extract, rosemary extract, ginkgo biloba extract, green tea extract, grapefruit seed extract, eochocho extract, pomegranate extract, licorice extract, Astragalus extract, caviar It is characterized by consisting of extract, golden extract, red ginseng extract.

 In addition, the rosehip extract in the method of producing a multi-functional sap of the present invention is a mixture of rose hips and alcohol content of 95% alcohol in a ratio of 1: 5 to 1:20 by weight in a sealed hermetically sealed glass container of 4-10 degrees Let the primary leaching extract for 3-8 weeks in a cool and dark place to avoid temperature and sunlight, pour out the extract, and the ratio of 1: 5 ~ 1: 20 to the rosehip and alcohol distilled alcohol 25% Sealed in a sealed glass container with a secondary leaching extract for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of 4-10 degrees Celsius, followed by the extract, leaching the rosehip and pH2. 5-3.5 strongly acidic electrolyzed water is mixed at a ratio of 1:60 to 1:90, and the rose hips and water are bathed at a temperature of 100 to 120 ° C. for 1 to 30 hours for 4 to 6 hours. The extract was extracted three times, followed by extracting the extract, and extracted three times with a strong acid water bath. Rosehip and pH10.5-11.5 strongly alkaline electrolytic water is mixed at a ratio of 1:60 to 1:90 by weight, and then the rose hips and water are 1:20 to 1:30 at a temperature of 100 to 120 ° C. Extract the extract from the 4th time by extracting it in 4th order by boiling water for 6 hours, and mix the extract extracted from each of the 4th time from above, and use the vacuum rotary evaporator to mix the concentrate and the extract at a temperature of 10-40 ° C. It is characterized in that it is prepared by concentrating for 10-40 minutes to the ratio of 10 ~ 1:40,

The rosemary extract is sealed in a closed glass container mixed with rosemary and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and then the leached rosemary and alcohol, 25% alcohol, is sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching rosemary and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the rosemary and water are heated at 100 to 120 ° C for 4 to 6 hours in a ratio of 1:20 to 1:30, followed by extraction in 3rd order, followed by the extract, and strongly acidic water. Rosemary and pH10.5-11.5 strongly alkaline electrolyzed water After mixing at a ratio of 1:60 to 1:90 to the weight of the rosemary and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 so that the fourth extraction Drain the extract, mix the extract extracted from each of the above 4 times, and use the vacuum rotary evaporator to make the concentrate and the extract at a ratio of 1:10 to 1:40 by weight at a temperature of 10-40 degrees Celsius. Characterized in that to prepare for 10-40 minutes,

The ginkgo biloba extract is sealed in a closed glass container mixed with ginkgo biloba and alcohol content of 95% alcohol in a ratio of 1: 5 to 1:20, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leach extraction, the extract is drained, and the leached and extracted primary leaves of ginkgo biloba and alcohol 25% alcohol in a ratio of 1: 5 to 1:20 by weight are sealed in a sealed glass container, and 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the seed, pour out the extract, leaching the secondary extract ginkgo leaf and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the ginkgo biloba and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. Ginkgo biloba extracted 3 times with water bath and pH10.5-11.5 strongly alkaline electrolyzed water After mixing at a ratio of 1:60 to 1:90, the extract and the extract were extracted in a 4th to 6 hour so that the ginkgo leaf and water were at a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that it is prepared by concentration, the green tea extract is sealed in a sealed glass container mixed with green tea and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight and the temperature of 4-10 degrees Celsius Let the primary leaching extract for 3-8 weeks in a cool dark place to avoid sunlight, pour out the extract, leaching the first extraction green tea and alcohol 25% alcohol at a ratio of 1: 5 to 1:20 by weight Cold place to avoid 4-10 ° C temperature and sunlight after sealing in mixed sealed glass container Second leaching extraction for 3-8 weeks to pour the extract, leaching second extraction green tea and pH2.5-3.5 strongly acidic electrolyzed water at a ratio of 1:60 to 1:90 to the weight of 100 ~ 120 The green tea and water at a temperature of ℃ ℃ 1:20 ~ 1:30 in a ratio of 4 to 6 hours in a water bath to extract the third extract, the green tea extracted with a strong acid water bath 3 times and pH10.5-11.5 After mixing strongly alkaline electrolyzed water at a ratio of 1:60 to 1:90, the green tea and water are heated at a temperature of 100 to 120 ° C. for 4 to 6 hours so that the ratio is 1:20 to 1:30. The extract was extracted, followed by extracting the extract, and the extracted extracts were mixed in each of the 4th stages above, and the concentrated solution and the extracts were prepared at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator. Characterized in that to prepare a concentration for 10-40 minutes,

The grapefruit seed extract is sealed in a sealed glass container mixed with a grapefruit seed and alcohol content of 95% alcohol in a ratio of 1: 5 to 1:20 by weight in a cold dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius After the first leaching extraction for 3-8 weeks, pour out the extract, and then sealed the grapefruit seed and alcoholic beverage 25% alcohol extracted by leaching at a ratio of 1: 5 to 1:20 by weight in a sealed glass container. Compared to the weight of the grapefruit seed and pH2.5-3.5 strongly acidic electrolyzed water extracted by distilling the extract, allowing the second leaching to be extracted for 3-8 weeks in a cool dark place where temperature and 4-10 degrees Celsius can be avoided. After mixing at a ratio of 1:60 to 1:90, the grapefruit seeds and water are heated at a temperature of 100 to 120 ° C. in a ratio of 1:20 to 1:30 for 4 to 6 hours to be extracted in a third manner. Pour the extract and compare the grapefruit seed extracted with the strong acid water bath with strong alkaline electrolytic water at pH10.5-11.5 After mixing at a ratio of 1:60 to 1:90, the grapefruit seeds and water are heated at 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30, and extracted in a fourth order. After the extraction, the extracts were extracted from each of the four rounds above, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that for 40 minutes to produce,

The Eoseongcho extract is sealed in a sealed glass container mixed with Eoseongcho and alcoholic alcohol 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and the leached and extracted primary fish and 25% alcoholic alcohol are sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Leak extraction for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the second extraction extracted fish and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the fish paste and water are heated at 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30, followed by extraction in 3rd order, followed by the extract, and strongly acidic water. Comparison of Eocho-chocho Extracted with Boiled Bath and pH10.5-11.5 Strongly Alkaline Electrolyzed Water After mixing at a ratio of 1:60 to 1:90, the fish paste and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours, and extracted in a fourth order. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that the concentration is prepared for a minute,

The pomegranate extract is sealed in a sealed glass container mixed with pomegranate and alcoholic alcohol 95% alcohol in a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and the leached and extracted primary pomegranate and alcoholic alcohol 25% spirits are sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the second extraction pomegranate and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing in a ratio of 1:90, the pomegranate and water are heated at 100-120 ° C. for 4-6 hours in a ratio of 1: 20-1: 30, followed by extraction in 3rd order, followed by the extract, and strongly acidic water. The ratio of pomegranate extracted from the water bath and the pH10.5-11.5 strong alkaline electrolyzed water in the ratio of 1:60 to 1:90 After mixing to 100 ~ 120 ℃ temperature of the pomegranate and water in a ratio of 1:20 ~ 1:30 in 4 to 6 hours to be extracted in 4th to extract the extract, from above each of the fourth The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. ,

The licorice extract is sealed in a sealed glass container mixed with licorice and 95% alcohol content in a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place that can avoid temperatures of 4-10 degrees Celsius and sunlight. After 8 weeks of primary leaching extraction, the extract is drained, and the licorice and alcoholic liquor extracted 25% of alcoholic liquor are sealed in a sealed glass container at a ratio of 1: 5 to 1:20 by weight, then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching licorice and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the licorice and water at a temperature of 100 to 120 ° C. are soaked for 4 to 6 hours in a ratio of 1:20 to 1:30, and extracted in a third manner, followed by extracting the extract, and a strong acidic water. The ratio of licorice extracted from the water bath three times and the pH10.5-11.5 strong alkaline electrolyzed water to the weight ratio of 1:60 to 1:90 After mixing to 100 ~ 120 ℃ the licorice and water at a temperature of 1:20 ~ 1:30 in a ratio of 4 to 6 hours to be extracted in 4th to extract the extract, and from above each 4 times The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. ,

The Astragalus extract is sealed in an airtight glass container mixed with a ratio of 1: 5 to 1:20 of Astragalus and alcoholic alcohol at 95% alcohol by weight, and then cooled in a cool dark place that can avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained and the leaching and primary extraction of sulfur and alcoholic alcohol 25% alcohol is sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the secondary extract and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the sulfuric acid and water are heated at a temperature of 100 to 120 ° C for 4 to 6 hours so that the ratio is 1:20 to 1:30, and extracted three times. A ratio of 1:60 to 1:90 of the weight of the sulfuric acid and pH10.5-11.5 strongly alkaline electrolyzed water extracted with a strong acid water bath After mixing to 100 to 120 ℃ the sulfur and water in a ratio of 1:20 ~ 1:30 in a ratio of 4 to 6 hours in a hot water to extract the fourth step, the extract is poured over each of the fourth The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. ,

The caviar extract is sealed in a closed glass container mixed with caviar and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained and the leached caviar and alcoholic alcohol 25% alcohol is sealed in a sealed glass container mixed at a ratio of 1: 5 to 1:20 by weight, then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the decant, pour out the extract, leaching the second extracted caviar and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the caviar and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 to be extracted in a third to extract the extract, strong acidic water Comparison of Caviar Extracted with the Bath in 3rd Weight and pH10.5-11.5 Strongly Alkaline Electrolyzed Water The mixture is mixed at a ratio of 1:60 to 1:90, and then extracted at a temperature of 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30 so that the extract is extracted in the fourth order. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that the concentration is prepared for a minute,

The golden extract is sealed in a sealed glass container mixed with a ratio of 1: 5 to 1:20 of gold and alcohol content of 95% alcohol, and then stored in a cool dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, pour out the extract, and immerse the primary extract of gold and alcohol 25% alcohol in a ratio of 1: 5 to 1:20 by weight in a sealed hermetically sealed glass container, then 4-10 Let the secondary leaching extract for 3-8 weeks in the cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the secondary extracted gold and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the mixture of gold and water at a temperature of 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30 is extracted in a third manner, followed by extraction of the extract, and a strong acidic water. The ratio of the gold extracted from the water bath and the pH10.5-11.5 strongly alkaline electrolyzed water in the water bath is 1:60 to 1:90 by weight. After mixing to 100 ~ 120 ℃ at a temperature of 100 ~ 120 ℃ in a ratio of 1:20 ~ 1:30 in a 4 to 6 hours so that the extraction is to extract the fourth step to pour the extract, each from the top four The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. ,

The red ginseng extract is sealed in a closed glass container mixed with red ginseng and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract was drained, and the red ginseng extracted with primary leaching and alcoholic beverage 25% alcohol was sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the seed, rinse the extract, leaching second extraction red ginseng and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the red ginseng and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. The ratio of red ginseng extracted with water bath and pH10.5-11.5 strong alkaline electrolyzed water in the ratio of 1:60 to 1:90 After mixing with the red ginseng and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 so that the extraction is carried out 4 times, the extract is poured over each of the fourth The extracted extract is mixed and prepared by concentrating the extract and the extract for 10-40 minutes using a vacuum rotary evaporator at a temperature of 10-40 ° C. in a ratio of 1:10 to 1:40 by weight. .

 In the pretreatment step of the present invention, the squid used is not limited to the type and size of the squid, such as domestic coastal acid, overseas North American Mexico, South America Peru.

In the incineration step of the incineration of the present invention, the incineration furnace for incineration is characterized in that it operates for 1 hour 25-45 hours with heat of 400-600 degrees Celsius.

In the separation and purification step of the present invention, the selenium extracted through the incineration process is characterized by qualitative and quantitative determination using gas chromatography (Gas Chromatography) to confirm the purity and separation.

In the sealing and packaging step of the present invention, weighing the sap prepared by stirring and weighing the contents and sealed with a PP molding container and a film of PE material characterized in that the packaged product passed through a metal detector after screening and distribution. do.

According to the manufacturing method of the antimicrobial anti-aging whitening complex functional sap using selenium and natural herbal extract of marine deep water and squid by-product extract of the present invention according to the above configuration, there is no big obstacle in supplying raw materials of internal organs, which are squid by-products, in the pretreatment step Deep sea water that can be understood and immediately checked for easy skin recovery and maintenance, and adaptation to skin antibacterial anti aging, and easy adaptation to everyone by raising awareness of antioxidant skin care that people have neglected. Provided is a method for producing antibacterial anti-aging whitening complex sap using squid by-product extraction selenium and natural herbal ingredients.

The technical problem achieved by the present invention and the practice of the present invention will be more clearly understood by preferred embodiments of the present invention described below.

The following examples are merely illustrative of the present invention and are not intended to limit the scope of the present invention.

Hereinafter, embodiments of the present invention will be described in detail with reference to the accompanying drawings and experimental examples.

1 is a flow chart illustrating a method for producing antibacterial anti-aging whitening complex functional sap using deep seawater and squid by-product extraction selenium and natural herbal ingredients according to an embodiment of the present invention.

Referring to the drawings, the squid is circulated to collect the internal organs of the squid body, and the remaining internal organs (black ink bag, gills, heart, visceral sac) are collected after separating and removing the anal part, washed with alkaline electrolyzed water, and acidic electrolyzed water. Sterilization pre-treatment step (S11); Firstly drying the pretreated squid gut with a moisture content of 10-20% and incineration in a second incineration furnace to extract minerals incineration step (S12); Selenium separation and purification step (S13) of removing foreign substances of the extracted inorganic substance and separating and purifying selenium having a purity of 10-20% using gas chromatography (GasChromatography); Stirring manufacturing step of preparing a sap by mixing and stirring the separated purified selenium 0.1% to 92.9 to 94.9% by weight deep sea water and 5.0 to 7.0% by weight natural herbal extract (S14); Sealing packaging step (S15) to put the prepared sap in a container to seal the packaging; consists of.

In particular, the method for preparing antimicrobial anti-aging whitening complex functional sap using deep seawater and squid by-product extraction selenium and natural herbal ingredients according to an embodiment of the present invention is immersed in alkaline electrolytic water immersion solution for 5-15 minutes in the pre-treatment step. It is necessary to prepare electrolytic water for the preparation of immersion liquid because it is sterilized by immersing in acid electrolytic water immersion solution for 5-15 minutes in order to prepare the immersion liquid.The same amount of strong acid electrolytic water and strong alkaline electrolytic water produced by electrolysis of drinking water etc. All of the generated strong electrolytic water can be effectively utilized by preparing an immersion liquid for each purpose.

Looking at this in more detail, the above-mentioned pretreatment step (S11) is a process of collecting tap water drinking water, which is a raw material, and electrolyzing it in an electrolytic cell to produce and use the produced alkaline electrolytic water and acid electrolytic water as an immersion aqueous solution, and also disable squid. It is a process of removing and washing the intestinal filth and foreign substances, which are the food parts, and collecting them.

When the water temperature of the electrolyte is increased during the generation of electrolytic water, the ionic change is activated in the diaphragm in the electrolytic cell, so that the strong acid electrolytic water generated at the anode not only increases the concentration of hypochlorite (HOCL), which is an effective chlorine having a disinfectant disinfection effect, but also the steel produced at the cathode. Alkaline electrolyzed water has a high concentration of sodium hydroxide (NaOH) having an interfacial effect, so that an underwater heater, which is a heating facility, is installed in a distilled water reservoir to operate at a temperature of 35-40 degrees Celsius.

In addition, in the above-described electrolysis process, 0.1-10.0% sodium chloride (NACL) is added to distilled water, mixed and diluted to make an electrolyte, and then electrolyzed in a electrolyte membrane electrolyte tank in an electrolytic cell. Exhaust pipes are installed to allow the discharge of chlorine gas from the anode.

In general, electro-analysised water refers to water obtained by applying electric force to general water such as tap water or ground water.

If the anode and cathode platinum-plated titanium is put into the water and the electricity is supplied by direct current, the anion dissolved in the water is collected on the (+) pole to become acidic ionized water, and cations gather on the (-) pole to the alkaline ionized water. Occurs.

The electrolyzed water thus produced has its ionic effect for 7-8 days when exposed to air and about 3-4 weeks when stored with the lid closed.

In the process of collecting the strongly alkaline electrolyzed water and the strongly acidic electrolyzed water generated in the above-mentioned electrolytic water collection process for use as the strongly alkaline pretreatment aqueous solution and the strongly acidic pretreatment aqueous solution, the strongly acidic electrolytic water at the anode side and the strong side at the cathode side were produced. Collect alkaline electrolytic water separately and put it in the sump and circulate so that the water temperature is maintained at 5-10 degrees Celsius using chiller, a cooling facility in each sump.

Underwater UV sterilizer is installed and operated in each reservoir to sterilize so that pH property does not change.

In addition, care should be taken to prevent re-contamination of each collected ionized water.

In case of acidic ionized water, it has a converging effect and constricts the skin.

Therefore, since it protects the skin slightly acidic, it is of course excellent in skin care and disinfection.

Hypochlorite Water Additive Standard by Korea Food and Drug Administration and Hypochlorite Water Food Additive Approval Standard by Japan Ministry of Health and Welfare applies the same standards and standards, according to which the component standard of Hypochlorous Acid Water is strong acidic hot water. (Also called strongly acidic hypochlorous acid) is less than pH2.7 and contains 20-60ppm of hypochlorous acid (HOCL), an effective chlorine, and non-acidic water (also called non-acidic hypochlorous acid) is pH5.0-6.5 It contains 10-30 ppm of hypochlorous acid (HOCL), and 10 ppm of effective chlorine has bactericidal effect against bacteria with low disinfectant resistance, and 20-30 ppm of effective chlorine has bactericidal effect against bacteria that do not have apopoies. Furthermore, if the effective chlorine is 60ppm, it has a bactericidal effect against infant germs within minutes.

Sodium hypochlorite water is not effective in killing follicles, but strong acid hypochlorite is a very effective fungicide for follicles, and Bacillus and clostridium have a killing effect within 3 minutes.

Hypochlorite water is characterized by a strong bactericidal and deodorizing effect but very low biotoxicity. The bactericidal power is fungus, Staphylococcus aureus, Pseudomonas aeruginosa, Escherichia coli, and other nutrients, Cereus, Acidophilus, Fungi, Viruses, Heterogeneous bacteria, Salmonella It has strong bactericidal power against food poisoning such as bacteria and Vibrio bacteria, as well as all pathogenic microorganisms caused by raw water. (Source: less than 5 seconds of Staphylococcus aureus, Pseudomonas aeruginosa, Escherichia coli, and other trophic bacteria of less than 5 minutes , 1 min-2 min 30 sec, fungus 5 sec-1 min, virus less than 5 sec, antimicrobial effect of strong acidic electrolyzed water, clinical test, 37: 919-919, 1993) Salmonella and Vibrio bacteria were not detected after 120,000-200,000 bacteria at 30 seconds after treatment, Test report on sterilization ability, Korea Testing and Research Institute, 2002) Hypochlorite is a fundamental measure of sterilization The odor is weak and experimentally 80 times stronger than sodium hypochlorite (NAOCL) and practically 5-10 times stronger, so the effect is that the bactericidal power of hypochlorite water with 30 ppm chlorine concentration is hypochlorous acid with 150 ppm chlorine concentration The US FDA (Food and Drug Administration) recognizes 1/50 of sodium hypochlorite in terms of the biotoxicity of hypochlorite water as well as being superior to sodium water (a disinfectant diluted in water). It is already widely used as a substitute for chemicals such as food disinfectants and pesticides.

Hypochlorite water is already used as an optimal disinfectant for airborne poisoning due to water, food raw materials, and spray because it is free of odors and does not contain salts.

Sterilization is increased by increasing the temperature of hypochlorous acid.

Strong alkaline ionized water is generated on the opposite (-) side as much as the amount of strong acidic water is made on the hypochlorite water production device (+) side, and serves as a surfactant, so strong alkaline ionized water is used as a cleaning agent, chemicals such as wax, chemical fertilizer, etc. It is also used as a substitute.

In addition, alkaline ionized water has more beneficial minerals (inorganic salts) than normal water, and makes water molecules smaller, so the absorption of minerals is increased, which helps improve diarrhea and constipation, and works on the stomach.

Strong alkaline ionized water is a natural emulsifier with excellent dissolving and detergency, as well as a surfactant with excellent natural surfactant effect, containing 40-120 ppm of sodium hydroxide (NaOH) at pH11.0 or higher. Because of its physical properties, it has a function to improve cleaning power, so it is mainly used for cleaning raw materials such as root vegetables (potatoes, potatoes, carrots, etc.), fruit vegetables (cucumbers, pumpkins, tomatoes, etc.), and grains (beans, brown rice, etc.). .

In foreign countries, strong alkaline water with a pH greater than 11.0 is recognized as a dilution solution of sodium hydroxide solution. It contains sodium hydroxide and natural emulsifiers and functions as a non-toxic natural detergent. It is due to the effect of washing off grease well.

The cleaning power is increased by increasing the temperature of the strong alkaline water.

In the case of countries where electrolyzed water is legalized by strong acid and strong alkaline ionized water, Kangsan Electrolyzed Water was announced in Korea in December 2005 by the Korea Food & Drug Administration (Packaging Container Team) No. 2005-75. It was first used as a standard and standard for hypochlorite, which is a disinfectant for facilities, and was announced as No. 2007-74 of the Korea Food and Drug Administration (Food Additives Team) in November 2007. And specifications.

Foreign cases preceded us. In June 2002, the Ministry of Health, Labor and Welfare Ordinance No. 75 and Notice No. 212 recognized strong acidic water as hypochlorous acid and approved as a food additive (sterilizer). In 1999, the sanitary water generator was approved by the Ministry of Sanitation as a disinfection device, and in 1998, the EPA (Environmental Protection Agency) approved the strong electric water generation device as a disinfectant manufacturing device in 1999, and in 1999, the FDA approved the strong acid electrolytic water. Recognized as the same as hypochlorous acid water, it was applied as a disinfectant for food materials and utensil containers, and the same year USDA (Agricultural) approved the use of electrolytic hypochlorous acid for the purpose of disinfecting intestinal pathogens of growth.

In foreign countries, since 1996, in Japan, hand sterilization, endoscopy disinfection, antibacterial measures, prevention of in-hospital infection, treatment of burns, and oral disinfection in the medical sector, and pesticide control for crop disease control in the agricultural sector since 1996. Since 2002, it has been used for cultivating pesticides and maintaining freshness of harvests. By 2002, it has been used in the environmental sector to remove organic odors, to decompose pollutants, and to manufacture drinking water. Its use has been expanded to improve the quality and preservation of containers and strong alkaline electrolyzed water.

Therefore, strong acidic electrolyzed water is a product that is approved for use in food hygiene not only in Korea but also in the world. It is harmless to humans, has no residue, and has excellent sterilizing power as can be seen from the above examples. .

As described above, the characteristics of each strong electric seawater are summarized first, and then the strong alkaline electrolyzed water should be cleaned and then sterilized and disinfected with strong acidic hypochlorite water as a rule. If the object is first immersed in strong alkaline electrolyzed water to remove organic contaminants and washed and disinfected with strong acidic electrolyzed water, the sterilization effect can be expected to be greatly increased.

Therefore, in the present invention, by setting the squid gut immersed in strong alkaline electrolytic water and then sterilized by immersion in strong acid electrolytic water, sterilization and disinfection in order to maximize the effect.

In more detail, the above-described pretreatment step (S11) is a process of squid squid to sterilize by immersing the by-product squid internal organs in the root and alkaline electrolytic water to wash and immerse in acid electrolytic water.

In general, raw materials can use all kinds of squid, such as domestic coastal, Peruvian, Mexican, North Pacific.

In addition, squid is a dried or specially processed biological squid can be used both frozen and alive squid, thawed if frozen.

In the case of thawing frozen squid, thaw without immersion in the refrigerated thawing room with an outdoor temperature of minus 5 ° C or above, and use a fan for quick thawing.

The cuttlefish consists of the head, torso and leg parts and the eyes, bones, teeth, and guts, which are invisible parts. Sac, gills, heart, visceral sac), collected and weighed and washed with foreign substances and dirts in the intestines in running water, and pH10.5-11.5 alkaline electrolyzed water and pH2 with 2-5 times dipping solution .5-3.5 Acid electrolyzed water shall be prepared and collected in an electrolytic water bath, firstly immersed in an alkaline electrolytic water immersion bath for 5-15 minutes and secondly immersed in an acid electrolytic water immersion bath for 5-15 minutes.

In this case, for hygiene, work table, knife, cutting board, etc. should be disinfected frequently using 100 ~ 200ppm solution of chlorine or 20 ~ 25ppm solution of iodine.

The above-described incineration step (S12) is a process of firstly drying the pretreated squid gut with a moisture content of 10-20% and incineration it in a second furnace to extract inorganic matters.

The above-described separation and purification step (S13) is a process of removing and removing foreign substances from the extracted inorganic matters, identifying and purifying purity by performing qualitative and quantitative selenium having a purity of 10-20% using gas chromatography (Gas Chromatography).

The above-described stirring preparation step (S14) is a high-purity selenium, deep sea water and natural herbal extracts, which are separated and purified and filtered using gas chromatography in a weight ratio of 0.1: 92.9-94.9; Mix at a rate of 5.0-7.0 and finally stir with a homogenizer for 30-45 minutes at a temperature condition of 50-70 degrees Celsius.

In the above-described configuration, the sealing packaging step (S15) is weighed and prepared by weighing the prepared sap and sealed in a glass container to pass the packaged product through a metal detector immediately after distribution.

Each of the sap prepared above is taken to measure pH.

In this case, the container should be sterilized by air drying after immersion in the disinfectant solution using alcohol, strong acidic electrolyzed water and iodine.

In the above series of processes, in order to prevent the growth of microorganisms at room temperature, the elapsed time of the process should be made within 4 hours during the stirring packaging process and the sealing packaging and the rapid freezing process.

Hereinafter, a method for preparing antimicrobial anti-aging whitening complex functional sap using selenium and natural herbal extract extracted from deep sea water and squid by-products prepared according to an embodiment of the present invention, and sap prepared according to the sap prepared in accordance with another comparative example Compare and review the results of experiments with various characteristics.

Hereinafter, a method for preparing antimicrobial anti-aging whitening complex functional sap using selenium and natural herbal extract extracted from deep sea water and squid by-products according to an embodiment of the present invention, and the sap manufacturing process prepared according to this process is carried out as follows.

[Pretreatment Process]

1) Collect the cuttlefish internal organs, the by-products of the cuttlefish removed by halving the squid on the workbench, and then remove the foreign matters, wash them in running water, weigh 1,000g, immerse in alkaline electrolyzed water for 10 minutes to wash, wash and acidic electrolyzed water. Sterilize by soaking for a minute.

2) In the electrolysis process, weigh 20.0 g of tap water and 30.0 g of sodium chloride relative to the weight of distilled water in an electrolytic solution, stir it in an electrolytic cell, and then electrolyze it in a diaphragm electrolytic cell in the electrolytic cell.

An underwater heater, which is a heating facility, is installed in the alkaline electrolytic water collector generated by the cathode to operate the water temperature at 35 degrees Celsius.

10,015g strongly alkaline electrolyzed water and 10,015g strongly acidic electrolyzed water generated in the above-mentioned electrolytic water collection process are collected for use as a strong alkaline pretreatment aqueous solution and a strong acid pretreatment aqueous solution, respectively. The strong alkaline electrolytic water on the cathode side is collected separately and placed in water collecting tanks, and the water temperature is maintained at 5-10 degrees Celsius by using a chiller as a cooling facility in each water collecting tank.

Underwater UV sterilizers are installed and operated in each reservoir to sterilize them so that the pH properties do not change.

In addition, care should be taken to prevent re-contamination of each collected ionized water.

[Incineration furnace incineration process]

3) The pre-treated squid intestines are dried first with a water content of 10-20% and incinerated second in an incineration furnace to extract minerals.

Even in this case, the food contact surfaces around the cold and warm air drying chambers or work benches are frequently disinfected using 70% alcohol solution.

[Separation Purification Step]

4) Remove the foreign substance of the extracted inorganic substance and check and purify selenium with purity 10-20% by using gas chromatography (Gas Chromatography) to confirm the purity and quantification.

[Stirring step]

5) Prepare the sap for wrinkle improvement by adding highly purified selenium, natural herb extract, thickener, moisturizer and functional additives, separated and purified using molecular distillation apparatus and chromatography.

0.1 g selenium, 93.9 g desalted deep sea water, 0.5 g rosehip extract, 0.5 g rosemary extract, 0.5 g ginkgo leaf extract, 0.5 g green tea extract, 0.5 g grapefruit seed extract, 0.5 g fish paste extract , 0.5g pomegranate extract, 0.5g licorice extract, 0.5g astragalus extract, 0.5g caviar extract, 0.5g golden extract, 0.5g red ginseng extract at a temperature of 70 ° C. Stir.

[Sealing packing step]

7) Each of the sap prepared above is sorted into a PP container, sealed with a PE film, sealed packaging, and passed through a metal detector.

8) Store the product at room temperature and distribute it at room temperature.

Hereinafter, a method for preparing antibacterial anti-aging whitening complex functional sap using deep seawater and squid by-product extracting selenium and natural herbal ingredients prepared according to an embodiment of the present invention, and sap prepared according to the comparative example and other comparative examples Compare and review the results of experiments with various characteristics.

Antimicrobial anti-aging whitening complex functional sap using selenium and natural herbal extract extracted from deep sea water and squid by-products prepared by the above process [Experimental Example 1] Sensory test for antibacterial calm and anti-aging wrinkle improvement and whitening improvement Was carried out.

Experimental Example 1

0.1% by weight of selenium and 99.9% by weight of purified water (Comparative Example 1), 0.1% by weight of selenium and 99.9% by weight of deep sea water (Comparative Example 2) When 90.9% by weight of deep sea water and 9.0% by weight of natural herbal extract (the same composition as the embodiment of the present invention) are mixed (Comparative Example 3), 0.1% by weight of selenium and 97.9% by weight of deep sea water and 2.0% by weight When the natural herbal extract (% of the same composition as the embodiment of the present invention) is mixed (Comparative Example 4) and each sap prepared according to the embodiment of the present invention (application) applied to the skin and applied Two weeks later, a comprehensive sensory evaluayion of antimicrobial sedation, anti-aging wrinkles and skin whitening was performed.

The sensory inspectors were 20 males and females who were trained in their 20s and 40s.The 5-point scoring method (5: very strong, 4: strong, 3: normal, 2: weak, 1: very weak) was used. The samples were repeated and averaged, and the sample was applied twice a day by lightly spreading on the skin under the condition of application after washing the face twice a day in the morning and evening. The skin whitening effect was evaluated and arithmetic average (Table 1).

As a result of the experiment, the antibacterial soothing effect and skin elasticity wrinkle improvement and skin whitening improvement effect were found to be higher when the water base was used as the deep sea water than when the water base was used as the normal purified water (Comparative Example 1) (Comparative Example 2) When the herbal extracts were added (Comparative Examples 3 and 4), they were higher, and were highest in the Examples.

Skin side effects according to the application of the sap appeared large in Comparative Example 3, where the ratio of natural herbal extracts was added, and the rest were insignificant. Therefore, it is preferable that the addition ratio of the natural herbal extract is 7.0 wt% or less.

(Table 1)

division Comparative Example 1 Comparative Example 2 Comparative Example 3 Comparative Example 4 Example Antibacterial soothing improvement 1.05 1.26 3.98 3.38 4.85 Elasticity wrinkle improvement 1.94 2.55 3.34 3.88 4.67 Skin whitening improvement 1.55 2.45 3.24 3.32 4.56 Skin side effects 1.06 1.09 3.13 1.08 1.10

In the embodiment of the present invention, the highest synergistic effect is considered to have augmented the complementary effect by interacting with the active ingredient that can give each function and effect.

Accordingly, when mass-producing cosmetic sap by the method for producing a multifunctional sap of the present invention, a complex effect of anti-aging anti-aging wrinkle improvement skin whitening suitable for the skin can be expected, and the present invention can provide a suitable multifunctional sap. It is a useful invention.

1 is a flow chart showing the manufacturing process of the antibacterial anti-aging whitening complex functional sap according to an embodiment of the present invention.

Claims (5)

Pretreatment step of collecting squid and collecting the internal organs of the squid body, separating and removing the anal part, and collecting the remaining internal organs, washing them with alkaline electrolytic water, and disinfecting them with acid electrolytic water; Incineration process in which pre-treated squid intestines are first dried at a moisture content of 10-20% and incinerated second in an incineration furnace to extract minerals; A selenium separation and purification step of removing foreign matters from the extracted inorganic substance and separating and purifying selenium having a purity of 10-20% using gas chromatography (Gas Chromatography); A stirred manufacturing process of mixing and stirring the separated purified selenium, 92.9 to 94.9% by weight of deep seawater, and 5.0 to 7.0% by weight of the natural herbal extract; Method for producing a composite functional sap for cosmetics, characterized in that comprising a. The method of claim 1, The process of washing in alkaline electrolytic water in the pretreatment step is a method for producing a composite functional sap for cosmetics, characterized in that it is immersed in pH 10.5-11.5 strong alkaline electrolytic water of 2-5 times the weight of the squid gut. The method according to claim 1 or 2, Sterilizing and disinfecting the acidic electrolytic water in the pretreatment step is a cosmetic complex characterized in that the squid intestine washed in alkaline electrolyzed water immersed in a strong acidic electrolytic water of pH 2.5-3.5 2-5 times the weight of the squid gut 5-15 minutes Method for producing functional sap. The method according to claim 1 or 2, In the stirring manufacturing step, the natural herbal extract is composed of rose hip extract, rosemary extract, ginkgo biloba extract, green tea extract, grapefruit seed extract, eochocho extract, pomegranate extract, licorice extract, Astragalus extract, caviar extract, golden extract, red ginseng extract Method for producing a composite functional sap for cosmetics. 5. The method of claim 4, The rose hip extract is sealed in a sealed glass container mixed with a rose hip and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and the leached rosehip and alcoholic liquor 25% spirits are sealed in a mixed airtight glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Leave and extract the secondary leaching for 3-8 weeks in a cool dark place where temperature and sunlight can be avoided. Drain and extract the rosehip and pH2.5-3.5 strongly acidic electrolyzed water, which are leached by secondary extraction. After mixing at a ratio of 1:90, the rose hips and water were heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. Compare the weight of the rose hips extracted with the water bath and the pH10.5-11.5 strong alkaline electrolyzed water After mixing at a ratio of 1:60 to 1:90, the rose hips and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C for 4 to 6 hours, and extracted in a fourth order. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that the concentration is prepared for a minute, The rosemary extract is sealed in a closed glass container mixed with rosemary and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and then the leached rosemary and alcohol, 25% alcohol, is sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching rosemary and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the rosemary and water were heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C for 4 to 6 hours, followed by extraction in 3rd order, followed by extracting the extract, and a strong acidic water. Rosemary and pH10.5-11.5 strongly alkaline electrolytically extracted from the water bath After mixing at a ratio of 1:60 to 1:90 to the weight of the rosemary and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 so that the fourth extraction Drain the extract, mix the extract extracted from each of the above 4 times, and use the vacuum rotary evaporator to make the concentrate and the extract at a ratio of 1:10 to 1:40 by weight at a temperature of 10-40 degrees Celsius. Characterized in that to prepare for 10-40 minutes, The ginkgo biloba extract is sealed in a closed glass container mixed with ginkgo biloba and alcohol content of 95% alcohol in a ratio of 1: 5 to 1:20, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leach extraction, the extract is drained, and the leached and extracted primary leaves of ginkgo biloba and alcohol 25% alcohol in a ratio of 1: 5 to 1:20 by weight are sealed in a sealed glass container, and 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the seed, pour out the extract, leaching the secondary extract ginkgo leaf and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the ginkgo biloba and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. Ginkgo biloba extracted 3 times with water bath and pH10.5-11.5 strongly alkaline electrolyzed water After mixing at a ratio of 1:60 to 1:90, the extract and the extract were extracted in a 4th to 6 hour so that the ginkgo leaf and water were at a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that it is prepared by concentration, the green tea extract is sealed in a sealed glass container mixed with green tea and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight and the temperature of 4-10 degrees Celsius Let the primary leaching extract for 3-8 weeks in a cool dark place to avoid sunlight, pour out the extract, and mix the leached primary tea with 25% alcohol content in a ratio of 1: 5 to 1:20 by weight. Cold place to avoid 4-10 degrees Celsius temperature and sunlight after sealing in airtight glass container Second leaching extraction for 3-8 weeks to pour the extract, leaching second extraction green tea and pH2.5-3.5 strongly acidic electrolyzed water at a ratio of 1:60 to 1:90 to the weight of 100 ~ 120 The green tea and water at a temperature of ℃ ℃ 1:20 ~ 1:30 in a ratio of 4 to 6 hours in a water bath to extract the third extract, the green tea extracted with a strong acid water bath 3 times and pH10.5-11.5 After mixing strongly alkaline electrolyzed water at a ratio of 1:60 to 1:90, the green tea and water are heated at a temperature of 100 to 120 ° C. for 4 to 6 hours so that the ratio is 1:20 to 1:30. The extract was extracted, followed by extracting the extract, and the extracted extracts were mixed in each of the 4th stages above, and the concentrated solution and the extracts were prepared at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator. Characterized in that to prepare a concentration for 10-40 minutes, The grapefruit seed extract is sealed in a sealed glass container mixed with a grapefruit seed and alcohol content of 95% alcohol in a ratio of 1: 5 to 1:20 by weight in a cold dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius After the first leaching extraction for 3-8 weeks, pour out the extract, and then sealed the grapefruit seed and alcoholic beverage 25% alcohol extracted by leaching at a ratio of 1: 5 to 1:20 by weight in a sealed glass container. Compared to the weight of the grapefruit seed and pH2.5-3.5 strongly acidic electrolyzed water extracted by distilling the extract, allowing the second leaching to be extracted for 3-8 weeks in a cool dark place where temperature and 4-10 degrees Celsius can be avoided. After mixing at a ratio of 1:60 to 1:90, the grapefruit seeds and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours, and extracted in a third manner. The weight of grapefruit seed and pH10.5-11.5 strong alkaline electrolyzed water After mixing at a ratio of 1:60 to 1:90, the grapefruit seeds and water are heated at 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30, and extracted in a fourth order. After the extraction, the extracts were extracted from each of the four rounds above, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that for 40 minutes to produce, The Eoseongcho extract is sealed in a sealed glass container mixed with Eoseongcho and alcoholic alcohol 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and the leached and extracted primary fish and 25% alcoholic alcohol are sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Leak extraction for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the second extraction extracted fish and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the fish paste and water are heated at 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30, followed by extraction in 3rd order, followed by the extract, and strongly acidic water. Comparison of Eocho-chocho Extracted with Water Bath and pH10.5-11.5 Strongly Alkaline Electrolyzed Water After mixing at a ratio of 1:60 to 1:90, the fish paste and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours, and extracted in a fourth order. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that the concentration is prepared for a minute, The pomegranate extract is sealed in a sealed glass container mixed with pomegranate and alcoholic alcohol 95% alcohol in a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained, and the leached and extracted primary pomegranate and alcoholic alcohol 25% spirits are sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the second extraction pomegranate and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing in a ratio of 1:90, the pomegranate and water are heated at 100-120 ° C. for 4-6 hours in a ratio of 1: 20-1: 30, followed by extraction in 3rd order, followed by the extract, and strongly acidic water. The ratio of pomegranate extracted from the water bath and the pH10.5-11.5 strong alkaline electrolyzed water in the ratio of 1:60 to 1:90 After mixing to 100 ~ 120 ℃ temperature of the pomegranate and water in a ratio of 1:20 ~ 1:30 in 4 to 6 hours to be extracted in 4th to extract the extract, from above each of the fourth The extracted extract is mixed and concentrated using a vacuum rotary evaporator at a temperature of 10-40 degrees Celsius for 10-40 minutes to prepare a concentrate and extract at a ratio of 1:10 to 1:40 by weight. , The licorice extract is sealed in a sealed glass container mixed with licorice and 95% alcohol content in a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place that can avoid temperatures of 4-10 degrees Celsius and sunlight. After 8 weeks of primary leaching extraction, the extract is drained, and the licorice extracted by leaching and alcoholic beverage 25% alcohol is sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching licorice and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the licorice and water at a temperature of 100 to 120 ° C. are soaked for 4 to 6 hours in a ratio of 1:20 to 1:30, and extracted in a third manner, followed by extracting the extract, and a strong acidic water. The ratio of licorice extracted from the water bath three times and the pH10.5-11.5 strong alkaline electrolyzed water to the weight ratio of 1:60 to 1:90 After mixing to 100 ~ 120 ℃ the licorice and water at a temperature of 1:20 ~ 1:30 in a ratio of 4 to 6 hours to be extracted in 4th to extract the extract, and from above each 4 times The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. , The Astragalus extract is sealed in an airtight glass container mixed with a ratio of 1: 5 to 1:20 of Astragalus and alcoholic alcohol at 95% alcohol by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained and the leaching and primary extraction of sulfur and alcoholic alcohol 25% alcohol is sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the secondary extract and pH2.5-3.5 strongly acidic electrolyzed water by weight 1: 60 ~ After mixing at a ratio of 1:90, the sulfuric acid and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. Ratio of 1:60 to 1:90 ratio of the weight of sulfuric acid and pH10.5-11.5 strong alkaline electrolyzed water After mixing to 100 to 120 ℃ the sulfur and water in a ratio of 1:20 ~ 1:30 in a ratio of 4 to 6 hours in a hot water to extract the fourth step, the extract is poured over each of the fourth The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. , The caviar extract is sealed in a closed glass container mixed with caviar and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20 by weight, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, the extract is drained and the leached caviar and alcoholic alcohol 25% alcohol is sealed in a sealed glass container mixed at a ratio of 1: 5 to 1:20 by weight, then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the decant, pour out the extract, leaching the second extracted caviar and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the caviar and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 to be extracted in a third to extract the extract, strong acidic water Comparison of Caviar Extracted from the Bath in the Bath and pH10.5-11.5 Strongly Alkaline Electrolyzed Water The mixture is mixed at a ratio of 1:60 to 1:90, and then extracted at a temperature of 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30 so that the extract is extracted in the fourth order. The extracts were extracted from each of the above four rounds, and the concentrates and extracts were mixed at a temperature of 10-40 degrees Celsius using a vacuum rotary evaporator at a ratio of 1:10 to 1:40 by weight. Characterized in that the concentration is prepared for a minute, The golden extract is sealed in a sealed glass container mixed with a ratio of 1: 5 to 1:20 of gold and alcohol content of 95% alcohol, and then stored in a cool dark place that can avoid the temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching extraction, pour out the extract, and immerse the primary extract of gold and alcohol 25% alcohol in a ratio of 1: 5 to 1:20 by weight in a sealed hermetically sealed glass container, then 4-10 Let the secondary leaching extract for 3-8 weeks in the cool and dark place to avoid the temperature and sunlight of the degree, pour out the extract, leaching the secondary extracted gold and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the mixture of gold and water at a temperature of 100 to 120 ° C. for 4 to 6 hours in a ratio of 1:20 to 1:30 is extracted in a third manner, followed by extraction of the extract, and a strong acidic water. The ratio of the gold extracted from the water bath and the pH10.5-11.5 strongly alkaline electrolyzed water in the water bath is 1:60 to 1:90 by weight. After mixing to 100 ~ 120 ℃ at a temperature of 100 ~ 120 ℃ in a ratio of 1:20 ~ 1:30 in a 4 to 6 hours so that the extraction is to extract the fourth step to pour the extract, each from the top four The extracted extract is mixed and concentrated using a vacuum rotary evaporator at a temperature of 10-40 degrees Celsius for 10-40 minutes to prepare a concentrate and extract at a ratio of 1:10 to 1:40 by weight. , The red ginseng extract is sealed in a closed glass container mixed with red ginseng and alcohol content of 95% alcohol at a ratio of 1: 5 to 1:20, and then cooled in a cool dark place to avoid temperature and sunlight of 4-10 degrees Celsius. After 8 weeks of primary leaching and extraction, the extract was drained, and the red ginseng extracted with primary leaching and alcoholic beverage 25% alcohol was sealed in a mixed-sealed glass container at a ratio of 1: 5 to 1:20 by weight, and then 4-10. Let the secondary leaching extract for 3-8 weeks in a cool and dark place to avoid the temperature and sunlight of the seed, rinse the extract, leaching second extraction red ginseng and pH2.5-3.5 strongly acidic electrolyzed water 1: 60 ~ After mixing at a ratio of 1:90, the red ginseng and water are heated in a ratio of 1:20 to 1:30 at a temperature of 100 to 120 ° C. for 4 to 6 hours to be extracted in a third manner, followed by extracting the extract, and a strong acidic water. The ratio of red ginseng extracted with water bath and pH10.5-11.5 strong alkaline electrolyzed water in the ratio of 1:60 to 1:90 After mixing with the red ginseng and water at a temperature of 100 ~ 120 ℃ 4 to 6 hours so that the ratio of 1:20 ~ 1:30 so that the extraction is carried out 4 times, the extract is poured over each of the fourth The extracted extract is mixed and prepared by concentrating the extract and the extract at a temperature of 10-40 ° C. using a vacuum rotary evaporator for 10-40 minutes in a ratio of 1:10 to 1:40 by weight. Extraction of deep water and squid by-products Preparation of antibacterial anti-aging whitening complex sap using selenium and natural herbal ingredients.

Images