KR100872783B1 - Manufacturing method for rice cream skin soap - Google Patents

Manufacturing method for rice cream skin soap Download PDF

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KR100872783B1
KR100872783B1 KR1020070021972A KR20070021972A KR100872783B1 KR 100872783 B1 KR100872783 B1 KR 100872783B1 KR 1020070021972 A KR1020070021972 A KR 1020070021972A KR 20070021972 A KR20070021972 A KR 20070021972A KR 100872783 B1 KR100872783 B1 KR 100872783B1
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oil
rice bran
soap
caustic soda
dissolving
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KR20080081658A (en
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김원숙
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주식회사 우성지에스텍
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/02—Boiling soap; Refining
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14—Shaping
    • C11D13/16—Shaping in moulds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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Abstract

본 발명은 미강유를 이용한 천연비누 제조방법에 대한 것으로, 발명의 주된 목적은 미강(쌀겨)으로부터 미강유를 추출하되, 탄산가스를 이용한 초임계 추출방법을 이용하여 추출하고, 그 추출된 미강유를 일정량 포함하여 저온법으로 미용에 우수한 천연비누를 제조할 수 있도록 하는데 있다. The present invention relates to a method for producing natural soap using rice bran oil, the main object of the present invention is to extract rice bran oil from rice bran (rice bran), using a supercritical extraction method using carbon dioxide gas, the extracted rice bran oil contains a certain amount It is to be able to manufacture a natural soap excellent in beauty by low temperature method.

상기 목적하는 바를 이루기 위한 본 발명의 특징적인 방법은 가성소다 약 100g, 물 260g, 올리브유 200g, 코코넛오일 300g, 팜 오일 200g, 라벤더 오일 10g을 준비하는 기본재료 준비단계, 통상의 초임계추출장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 미강유를 추출하여 준비하는 미강유 준비단계, 그리고 준비된 기본재료의 물에 가성소다를 넣고 잘 저어 완전히 녹여 준비하고, 상기 올리브유를 스테인레스 용기에 넣고 가열하면서 고체인 팜오일 및 코코넛오일이 완전히 녹여 준비하는 재료 용해단계, 그리고 상기 용해단계에서 준비된 가성소다액 및 오일용액의 온도가 모두 약 45℃~55℃가 되도록 식힌 후, 서로 섞어서 트레이스 상태가 되도록 하는 트레이스 성형단계, 그리고 트레이스에 준비한 초임계추출 미강유와, 라벤더 오일 등 준비한 첨가물을 넣고, 잘 퍼지도록 저어주는 비누용액 제조단계, 그리고 상기 비누용액을 틀에 붓고 공기가 통하지 않도록 포장하여 30~35일 보관하는 비누 굳힘단계를 차례로 거쳐 제조하는 것이다. Characteristic method of the present invention for achieving the above object is caustic soda about 100g, water 260g, olive oil 200g, coconut oil 300g, palm oil 200g, lavender oil 10g to prepare a basic material preparation step, conventional supercritical extraction equipment and Preparation of rice bran oil by extracting rice bran oil from rice bran (rice bran) using supercritical fluid carbon dioxide (CO 2 ), and adding caustic soda to water of the prepared basic material to stir thoroughly, and preparing the olive oil in a stainless container After dissolving solid palm oil and coconut oil in a solid state and heating them, the caustic soda and oil solutions prepared in the dissolving step are cooled to about 45 ° C. to 55 ° C., and then mixed together and traced. Trace forming step to make the state, supercritical extraction rice bran oil, lavender oil, etc. prepared in the trace Put ruthless additives, manufacturing soap solution to stir so as to better purge step, and is to prepare through the soap solution is poured into a mold and then packaged to the air passing through the soap guthim step to store 30 to 35 days.

비누, 저온법, 미강유, 초임계, 추출, 탄산가스 Soap, low temperature method, rice bran oil, supercritical, extraction, carbon dioxide

Description

미강유를 이용한 천연비누 제조방법{MANUFACTURING METHOD FOR RICE CREAM SKIN SOAP}MANUFACTURING METHOD FOR RICE CREAM SKIN SOAP}

도 1은 본 발명의 제조방법에 따른 진행도이다. 1 is a flow chart according to the manufacturing method of the present invention.

본 발명은 미강유를 이용한 천연비누 제조방법에 대한 것으로, 더 상세하게는 미강유를 초임계추출의 방법으로 추출하여 다른 재료와 함께 준비하고, 준비된 재료를 CP(저온법) 제조방법에 따라 제조하는데 특징이 있는 것이다. The present invention relates to a method for producing natural soap using rice bran oil, and more particularly, extracting rice bran oil by a method of supercritical extraction, preparing it with other materials, and preparing the prepared material according to the CP (low temperature method) manufacturing method. Is there.

일반적인 비누(soap)는 고급지방산의 수용성 알칼리 금속염으로 된 피부 세정용 생활용품으로서, 피부를 세척하여 기름용 때(노폐물)를 제거하고 이에 의해 세균으로부터 피부를 보호하게 하는 목적성을 지닌 용품이다. General soap (soap) is a household article for skin cleansing with a water-soluble alkali metal salt of higher fatty acids, the article having the purpose of washing the skin to remove grease (waste) and thereby protect the skin from bacteria.

하지만, 이러한 일반적인 비누는 통상적으로 피부의 세정을 통해 노폐물 제거에는 효과적이라 할 수 있으나 피부자극 등에 의한 여드름이나 기미 또는 얼굴단 장을 위한 화장물질을 제거하지는 못하는 단점이 있었다. However, such a general soap can be said to be effective to remove the waste through the cleaning of the skin in general, but there was a disadvantage that it does not remove the cosmetic material for acne or blemishes or facial rehabilitation due to skin irritation.

이러한 이유로 미용효과 및 생활개선을 위한 기능성 비누제품이 연구되고 계속적인 출시를 이루고 있으나, 새로운 피부 자극을 유발하거나 피부병을 유발시키는 등의 부작용에 따른 폐해가 지적되어 오고 있는 실정이다. For this reason, functional soap products for cosmetic effects and life improvement have been researched and released continuously, but the adverse effects of side effects such as causing new skin irritation or skin diseases have been pointed out.

한편, 근래에는 미강으로부터 얻은 미강유를 사용하여 비누를 제조하기 시작하였다. In recent years, soap has been started using rice bran oil obtained from rice bran.

미강은 지방, 단백질, 식이섬유가 영양소의 많은 부분을 차지하고 있고, 비타민 A와 티아민, 피리독신, 니아신 등의 비타민 B군 및 칼슘, 아연, 철분 등의 미네랄이 주성분을 이루고 있다. Rice bran is composed of fat, protein, and dietary fiber, a large part of the nutrients, vitamin A, thiamin, pyridoxine, niacin, such as vitamin B group, and calcium, zinc, iron and other minerals.

또, 미강 중에는 곡류에 부족한 필수 아미노산인 리신이 다량 함유되어 있고, 구성 지방산의 70% 이상이 올레인산, 리놀레산, 리놀렌산 등의 불포화지방산으로 영양적인 가치가 뛰어나다. In addition, rice bran contains a large amount of lysine, an essential amino acid lacking in grains, and more than 70% of constituent fatty acids are excellent in nutritional value as unsaturated fatty acids such as oleic acid, linoleic acid, and linolenic acid.

특히, 리놀레산과 리놀렌산은 각각 오메가-6 및 오메가-3계의 다가불포화지방산(PUFA)으로 체내에서 합성이 안되는 필수지방산에 속하여 영양학적으로 매우 중요하게 생각된다. In particular, linoleic acid and linolenic acid are omega-6 and omega-3 polyunsaturated fatty acids (PUFA), respectively, belong to essential fatty acids that are not synthesized in the body and are considered nutritionally very important.

그러나 종래의 미강유는 일반적인 식물성 기름 추출방법에 의해서 추출하는 것이기 때문에 추출된 농도가 약하고 질이 떨어진다. However, because the conventional rice bran oil is extracted by a general vegetable oil extraction method, the extracted concentration is weak and the quality is poor.

따라서 본 발명은 상기와 같은 종래의 문제점을 감안하여 제안하는 것으로, 발명의 주된 목적은 미강(쌀겨)으로부터 미강유를 추출하되, 탄산가스를 이용한 초임계 추출방법을 이용하여 추출하고, 그 추출된 미강유를 일정량 포함하여 저온법으로 미용에 우수한 천연비누를 제조할 수 있도록 하는데 있다. Therefore, the present invention is proposed in view of the conventional problems as described above, the main object of the invention is to extract the rice bran oil from rice bran (rice bran), using a supercritical extraction method using carbon dioxide, the extracted rice bran oil Including a certain amount to be able to manufacture a natural soap excellent in beauty by low temperature method.

상기 목적하는 바를 이루기 위한 본 발명의 특징적인 방법은 가성소다 약 100g, 물 260g, 올리브유 200g, 코코넛오일 300g, 팜 오일 200g, 라벤더 오일 10g을 준비하는 기본재료 준비단계, 통상의 초임계추출장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 미강유를 추출하여 준비하는 미강유 준비단계, 그리고 준비된 기본재료의 물에 가성소다를 넣고 잘 저어 완전히 녹여 준비하고, 상기 올리브유를 스테인레스 용기에 넣고 가열하면서 고체인 팜오일 및 코코넛오일이 완전히 녹여 준비하는 재료 용해단계, 그리고 상기 용해단계에서 준비된 가성소다액 및 오일용액의 온도가 모두 약 45℃~55℃가 되도록 식힌 후, 서로 섞어서 트레이스 상태가 되도록 하는 트레이스 성형단계, 그리고 트레이스에 준비한 초임계추출 미강유와, 라벤더 오일 등 준비한 첨가물을 넣고, 잘 퍼지도록 저어주는 비누용액 제조단계, 그리고 상기 비누용액을 틀에 붓고 공기가 통하지 않도록 포장하여 30~35일 보관하는 비누 굳힘단계를 차례로 거쳐 제조하는 것이다. Characteristic method of the present invention for achieving the above object is caustic soda about 100g, water 260g, olive oil 200g, coconut oil 300g, palm oil 200g, lavender oil 10g to prepare a basic material preparation step, conventional supercritical extraction equipment and Preparation of rice bran oil by extracting rice bran oil from rice bran (rice bran) using supercritical fluid carbon dioxide (CO 2 ), and adding caustic soda to water of the prepared basic material to stir thoroughly, and preparing the olive oil in a stainless container After dissolving solid palm oil and coconut oil in a solid state and heating them, the caustic soda and oil solutions prepared in the dissolving step are cooled to about 45 ° C. to 55 ° C., and then mixed together and traced. Trace forming step to make the state, supercritical extraction rice bran oil, lavender oil, etc. prepared in the trace Put ruthless additives, manufacturing soap solution to stir so as to better purge step, and is to prepare through the soap solution is poured into a mold and then packaged to the air passing through the soap guthim step to store 30 to 35 days.

이하 본 발명의 제조방법에 따른 실시 예를 자세히 설명한다. Hereinafter, the embodiment according to the manufacturing method of the present invention will be described in detail.

본 발명은 기본재료 준비단계로부터 초임계추출 미강유 준비단계, 재료 용해단계, 트레이시 성형단계, 비누용액 제조단계, 비누 굳힘단계를 거친다. The present invention undergoes supercritical extraction rice bran oil preparation step, material dissolution step, tracing molding step, soap solution production step, soap solidification step from the basic material preparation step.

먼저, 재료 준비단계에서는 비누 제조에 따른 안전장비를 착용하고, 필요한 재료들을 계량한 후 용기에 담아둔다. First, in the material preparation step, wear safety equipment according to soap manufacturing, weigh the necessary materials and put them in a container.

즉, 가성소다를 사용할 때는 꼭 장갑을 착용하여 가성소다가 비누에 묻지 않도록 해야 하며, 오일과 가성소다의 양은 저울을 사용하여 정확히 측정하여 한다.That is, when using caustic soda, be sure to wear gloves to prevent caustic soda from getting on the soap, and the amount of oil and caustic soda should be accurately measured using a scale.

다음의 미강유 준비단계에서는 초임계추출의 방법으로 쌀겨에서 미강유를 얻어 둔다. In the next stage of preparation of rice bran oil, rice bran oil is obtained from rice bran by supercritical extraction.

초임계 추출방법은 널리 알려진 원액 추출방법이며, 탄산가스(CO2) 성분의 초임계유체는 혼합물에서 특정 성분을 추출·분리하는 능력이 뛰어나서 식품 분야에서 응용이 활발하다. 예컨대, 맥주용 홉 엑스 추출, 커피의 탈 카페인 프로세스 등에 이용되며, 식품의 비가열살균 시스템 등에서도 적용중이다. Supercritical extraction is a well-known method for extracting undiluted liquor, and the supercritical fluid of carbon dioxide (CO 2 ) is excellent in the ability to extract and separate specific components from the mixture, which makes it suitable for food applications. For example, it is used for hop extracting for beer, decaffeine process of coffee, and the like, and is also applied to food non-heat sterilization system.

따라서 초임계 추출장비와 초임계 추출 유체를 이용하여 쌀겨로부터 미강유를 추출하면 농도가 일반 미강유의 수배에 달한다. Therefore, the extraction of rice bran oil from rice bran using supercritical extraction equipment and supercritical extracting fluid reaches several times the concentration of ordinary rice bran oil.

다음의 재료 용해단계에서는 측정된 올리브유, 코코넛 오일 등 베이스 오일을 스테인레스 용기에 담고, 오일을 45~55도 사이의 약한 불로 가열하여 고체인 팜유나 코코넛 오일이완전히 녹을 때까지 저어준다. In the next material dissolving step, base oil, such as measured olive oil and coconut oil, is placed in a stainless steel container, and the oil is heated to a low heat between 45 and 55 degrees and stirred until solid palm oil or coconut oil is completely dissolved.

온도계는 바닥이나 용기의 벽에 붙지 않도록 손으로 잡고 오일 한가운데 넣고 온도를 측정해야 오일의 온도를 정확하게 잴 수 있다. Hold the thermometer with your hand so that it does not stick to the floor or the wall of the container and place it in the middle of the oil to measure the temperature.

이와 또 다른 한편으로 환기가 잘 되는 곳에서 가성소다를 증류수에 넣으며 잘 녹을 때까지 저어준다. On the other hand, in a well-ventilated place caustic soda in distilled water and stir until dissolved.

이와같이 가성소다 용액을 만들 때는 반드시 고무장갑을 끽, 마스크를 쓰며 눈에 들어가거나 피부에 튀지 않도록 조심한다. When making caustic soda solution, be sure to squeeze rubber gloves and wear a mask to avoid getting into your eyes or splashing on your skin.

가성소다가 피부에 닿으면 반드시 흐르는 물에 빨리 씻어내고 식초로 닿은 부위를 중화시켜 준다. 그리고 가성 소다 용액에서 발생하는 수증기를 호흡하지 않도록 주의한다. If caustic soda comes into contact with your skin, wash it off with running water quickly and neutralize any contact with vinegar. And be careful not to breathe the water vapor from caustic soda solution.

가성소다를 증류수에 넣을 때 스테인레스 용기를 사용하는 것이 바람직하다. It is preferable to use a stainless container when adding caustic soda to distilled water.

다음으로 트레이스 성형단계에서는 위의 공정에서 만들어진 가성소다 용액이 45~55도 정도로 식을 때까지 기다린다. (빨리 식히기 위해서는 찬물에 스테인레스 용기를 담구어 줄 수 있다.)Next, in the trace forming step, wait until the caustic soda solution made in the above process cools to 45-55 degrees. (To cool down quickly, you can dip a stainless container into cold water.)

오일과 가성소다의 온도가 45~55도 사이가 되면 가성소다액을 오일에 천천히 부으며 주걱으로 천천히 저어준다. When the temperature of oil and caustic soda is between 45 and 55 degrees, pour caustic soda into the oil slowly and stir slowly with a spatula.

저을 때 핸드 블렌더를 사용하면 약 5분 안에 트레이스 상태가 된다. If you use a hand blender while stirring, you will be in a trace in about 5 minutes.

비누에서 트레이스 상태란 반죽을 들어 떨어뜨렸을 때 반죽이 떨어진 자국이 없어지지 않고 남아 있는 즉, 크림 스프 정도의 상태를 말한다. 주걱으로 저을 경 우 약 1시간 이상 저어주어야 트레이스 상태가 된다. The trace state in soap is the state of the cream soup, which remains when the dough is not removed when the dough is dropped. If you stir with a spatula, you need to stir for at least 1 hour to get a trace.

다음으로 비누 용액 제조단계에서는 상기와 같이 엷은 트레이스가 되면 첨가물을 넣는다. 첨가물을 넣은 후에는 첨가물들이 골고루 잘 퍼지게 젖는다.Next, in the soap solution manufacturing step, the additive is added when the light trace as described above. After adding the additives, the additives are well spread evenly.

이어서, 비누 굳힘단계에서는 트레이스 표면에 확실하게 자국이 선명하게 생기면 틀에 붓는 것이다. Subsequently, during the soap hardening step, if the traces are clearly formed on the trace surface, it is poured into the mold.

이때 기포가 생기지 않도록 주의한다. 그리고 틀에 유산지나 비닐을 깔고 천천히 부은 후 공기가 통하지 않도록 랩으로 싸고, 30~35일 정도 보온 보관한다. Be careful not to create bubbles at this time. Lay the paper or vinyl on the mold and pour it slowly. Wrap it in air to keep it out of the air and keep it warm for 30 to 35 days.

마지막으로 완성된 비누는 최소 4주~6주 정도 후부터 사용 가능하다. pH측정으로 비누 사용 여부를 가늠할 수 있다. pH가 7 - 9.5정도 이면 사용 가능하다.Finally, the finished soap can be used after at least 4-6 weeks. pH measurement can determine whether soap is used. It can be used if the pH is between 7 and 9.5.

위에서 상세히 설명한 바와 같은 본 발명은 미강(쌀겨)으로부터 추출한 미강유로써 비누를 제조하되, 종래와 달리 탄산가스를 이용한 초임계 추출방법을 이용하여 미강유를 추출하여 제조한 것이기 때문에 고농도의 미강유를 사용할 수 있게 된 것이고, 이는 종래의 일반 미강유를 넣어 제조한 비누에 비하여 월등히 우수한 천연비누를 제조할 수 있는 것이다. The present invention as described in detail above is to prepare a soap with rice bran oil extracted from rice bran (rice bran), unlike conventional, because it is manufactured by extracting rice bran oil using a supercritical extraction method using carbon dioxide gas so that a high concentration of rice bran oil can be used. That is, it is possible to produce a natural soap that is much superior to the soap prepared by the conventional ordinary rice bran oil.

Claims (1)

가성소다 100g , 물 260g , 올리브유 200g , 코코넛오일 300g, 팜오일 200g , 라벤더 오일 10g 을 준비하는 기본재료 준비단계 ; A basic material preparation step of preparing 100 g of caustic soda, 260 g of water, 200 g of olive oil, 300 g of coconut oil, 200 g of palm oil, and 10 g of lavender oil; 초임계추출장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 미강유를 추출하여 준비하는 미강유 준비단계 ; Rice bran oil preparation step of extracting and preparing rice bran oil from rice bran (rice bran) using a supercritical extraction equipment and supercritical fluid carbon dioxide (CO 2 ); 준비된 기본재료의 물에 가성소다를 넣고 잘 저어 완전히 녹여 준비하고, 상기 올리브유를 스테인레스 용기에 넣고 가열하면서 고체인 팜오일 및 코코넛 오일이 완전히 녹여 준비하는 재료 용해단계 ; Dissolving caustic soda in water of the prepared basic material, stir well to dissolve completely, and dissolving the solid palm oil and coconut oil while dissolving the olive oil in a stainless steel container; 상기 용해단계에서 준비된 가성소다액 및 오일용액의 온도가 모두 45도~55도가 되도록 식힌 후,서로 섞어서 트레이스 상태가 되도록 하는 트레이스 성형단계 ; 트레이스에 준비한 초임계추출 미강유와 라벤더 오일이 포함된 준비한 첨가물을 넣고 , 잘 퍼지도록 저어주는 비누용액 제조단계 ; A trace forming step of cooling the caustic soda solution and the oil solution prepared in the dissolving step to 45 degrees to 55 degrees, and then mixing them to form a trace state; Preparing a supercritical extract rice bran oil and lavender oil prepared in the trace, and preparing a soap solution to stir well; 상기 비누용액을 틀에 붓고 공기가 통하지 않도록 포장하여 30~35일 보관하는 비누 굳힘단계 를 차례로 거쳐 제조하는 것을 특징으로 하는 미강유를 이용한 천연비누 제조방법.Pour the soap solution into the mold and packaging to prevent air from passing through the soap solidification step to prepare for 30 to 35 days stored in order to produce natural soap using rice bran oil.
KR1020070021972A 2007-03-06 2007-03-06 Manufacturing method for rice cream skin soap KR100872783B1 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100959695B1 (en) 2008-10-09 2010-05-26 전정례 Manufacturing method of eco-friendly detergent composition

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR960023005A (en) * 1994-12-09 1996-07-18 김정순 Liquid human cleanser composition with improved antibacterial and deodorant effect
JP2005264128A (en) 2004-03-18 2005-09-29 Amyuure:Kk Whitening soap
KR20060091730A (en) * 2005-02-16 2006-08-21 (주)참미래 Soap containing rice germ and rice bran

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR960023005A (en) * 1994-12-09 1996-07-18 김정순 Liquid human cleanser composition with improved antibacterial and deodorant effect
JP2005264128A (en) 2004-03-18 2005-09-29 Amyuure:Kk Whitening soap
KR20060091730A (en) * 2005-02-16 2006-08-21 (주)참미래 Soap containing rice germ and rice bran

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100959695B1 (en) 2008-10-09 2010-05-26 전정례 Manufacturing method of eco-friendly detergent composition

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