KR100872784B1 - Manufacturing method for rice cream skin soap - Google Patents

Manufacturing method for rice cream skin soap Download PDF

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KR100872784B1
KR100872784B1 KR1020070021973A KR20070021973A KR100872784B1 KR 100872784 B1 KR100872784 B1 KR 100872784B1 KR 1020070021973 A KR1020070021973 A KR 1020070021973A KR 20070021973 A KR20070021973 A KR 20070021973A KR 100872784 B1 KR100872784 B1 KR 100872784B1
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rice bran
bran oil
soap
oil
soap base
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KR20080081659A (en
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김원숙
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주식회사 우성지에스텍
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/02—Boiling soap; Refining
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14—Shaping
    • C11D13/16—Shaping in moulds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Chemical & Material Sciences (AREA)
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Abstract

본 발명은 미강유를 이용한 천연비누 제조방법에 대한 것으로, 발명의 주된 목적은 비누 베이스를 녹인 후, 각종 추가물과 함께 미강유를 첨가하되, 이 미강유를 탄산가스를 이용한 초임계추출의 방법으로 추출된 고 농도의 미강유를 일정량 포함하여 녹여붓기의 방법으로 미용에 우수한 천연비누를 제조할 수 있도록 하는데 있다. The present invention relates to a method for producing natural soap using rice bran oil, and the main object of the present invention is to melt the soap base and add rice bran oil together with various additives, and the rice bran oil is extracted by supercritical extraction using carbon dioxide gas. Including a certain amount of high concentration of rice bran oil to be able to manufacture a natural soap excellent in beauty by the method of melting and pouring.

상기 목적하는 바를 이루기 위한 본 발명의 특징적인 방법은 비누 베이스(TEA FREE)와, 에센스 오일 등 기타 추가물을 준비하는 기본재료 준비단계; 그리고 통상의 초임계 추출장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 고농도의 미강유를 추출하여 준비하는 미강유 준비단계; 그리고 준비된 비누 베이스를 약 2~7cm로 깎뚝썰기한 후, 스테인레스 통에 넣어 가열로 용해시키는 용해단계; 그리고 녹인 비누 베이스를 잘 저어 가면서 에센스 오일 등을 포함한 추가물을 첨가하는 추가물 첨가단계; 그리고 다시 가열하여 고체화되기 이전에 초임계추출의 방법으로 추출한 고농도의 미강유를 비누 베이스의 중량비 약 2∼5%를 투입하는 미강유 첨가단계; 그리고 상기와 같이 미강유 첨가단계를 마친 비누 베이스를 미리 준비한 성형틀에 붓고 공기가 잔류하지 않도록 마무리하여 약 24시간 보관하는 비누 굳힘단계를 차례로 거쳐 제조하는 것이다. Characteristic method of the present invention for achieving the above object is a base material preparation step of preparing a soap base (TEA FREE) and other additives such as essence oil; And rice bran oil preparation step of extracting and preparing a high concentration of rice bran oil from rice bran (rice bran) using a conventional supercritical extraction equipment and supercritical fluid carbon dioxide (CO 2 ); And after dipping the prepared soap base to about 2 ~ 7cm, dissolution step to dissolve by heating into a stainless steel barrel; And the addition step of adding the addition including the essence oil while stirring the melted soap base well; And the step of adding the rice bran oil to the high concentration of rice bran oil extracted by the method of supercritical extraction before the solidification by heating again, about 2 to 5% by weight of the soap base; Then, the soap base, which has been added with rice bran oil, is poured into a mold prepared in advance and finished so that air does not remain.

비누, 녹여붓기법, 미강유, 초임계, 추출 Soap, Melting, Rice Bran Oil, Supercritical, Extraction

Description

미강유를 이용한 천연비누 제조방법{MANUFACTURING METHOD FOR RICE CREAM SKIN SOAP}MANUFACTURING METHOD FOR RICE CREAM SKIN SOAP}

도 1은 본 발명의 제조방법에 따른 진행도이다. 1 is a flow chart according to the manufacturing method of the present invention.

본 발명은 미강유를 이용한 천연비누 제조방법에 대한 것으로, 더 상세하게는 미강유를 초임계추출의 방법으로 추출하여 다른 재료와 함께 준비하고, 준비된 재료를 MP(녹여붓기) 제조방법에 따라 제조하는데 특징이 있는 것이다. The present invention relates to a method for producing natural soap using rice bran oil, and more particularly, extracting rice bran oil by a method of supercritical extraction, preparing it with other materials, and preparing the prepared material according to the MP (melt pouring) manufacturing method. Is there.

일반적인 비누(soap)는 고급지방산의 수용성 알칼리 금속염으로 된 피부 세정용 생활용품으로서, 피부를 세척하여 기름용 때(노폐물)를 제거하고 이에 의해 세균으로부터 피부를 보호하게 하는 목적성을 지닌 용품이다. General soap (soap) is a household article for skin cleansing with a water-soluble alkali metal salt of higher fatty acids, the article having the purpose of washing the skin to remove grease (waste) and thereby protect the skin from bacteria.

하지만, 이러한 일반적인 비누는 통상적으로 피부의 세정을 통해 노폐물 제거에는 효과적이라 할 수 있으나 피부자극 등에 의한 여드름이나 기미 또는 얼굴단 장을 위한 화장물질을 제거하지는 못하는 단점이 있었다. However, such a general soap can be said to be effective to remove the waste through the cleaning of the skin in general, but there was a disadvantage that it does not remove the cosmetic material for acne or blemishes or facial rehabilitation due to skin irritation.

이러한 이유로 미용효과 및 생활개선을 위한 기능성 비누제품이 연구되고 계속적인 출시를 이루고 있으나, 새로운 피부 자극을 유발하거나 피부병을 유발시키는 등의 부작용에 따른 폐해가 지적되어 오고 있는 실정이다. For this reason, functional soap products for cosmetic effects and life improvement have been researched and released continuously, but the adverse effects of side effects such as causing new skin irritation or skin diseases have been pointed out.

한편, 근래에는 미강으로부터 얻은 미강유를 사용하여 비누를 제조하기 시작하였다. In recent years, soap has been started using rice bran oil obtained from rice bran.

미강은 지방, 단백질, 식이섬유가 영양소의 많은 부분을 차지하고 있고, 비타민 A와 티아민, 피리독신, 니아신 등의 비타민 B군 및 칼슘, 아연, 철분 등의 미네랄이 주성분을 이루고 있다. Rice bran is composed of fat, protein, and dietary fiber, a large part of the nutrients, vitamin A, thiamin, pyridoxine, niacin, such as vitamin B group, and calcium, zinc, iron and other minerals.

또, 미강 중에는 곡류에 부족한 필수 아미노산인 리신이 다량 함유되어 있고, 구성 지방산의 70% 이상이 올레인산, 리놀레산, 리놀렌산 등의 불포화지방산으로 영양적인 가치가 뛰어나다. In addition, rice bran contains a large amount of lysine, an essential amino acid lacking in grains, and more than 70% of constituent fatty acids are excellent in nutritional value as unsaturated fatty acids such as oleic acid, linoleic acid, and linolenic acid.

특히, 리놀레산과 리놀렌산은 각각 오메가-6 및 오메가-3계의 다가불포화지방산(PUFA)으로 체내에서 합성이 안되는 필수지방산에 속하여 영양학적으로 매우 중요하게 생각된다. In particular, linoleic acid and linolenic acid are omega-6 and omega-3 polyunsaturated fatty acids (PUFA), respectively, belong to essential fatty acids that are not synthesized in the body and are considered nutritionally very important.

그러나 종래의 미강유는 일반적인 식물성 기름 추출방법에 의해서 추출하는 것이기 때문에 추출된 농도가 약하고 질이 떨어진다. However, because the conventional rice bran oil is extracted by a general vegetable oil extraction method, the extracted concentration is weak and the quality is poor.

따라서 본 발명은 상기와 같은 종래의 문제점을 감안하여 제안하는 것으로, 발명의 주된 목적은 비누 베이스를 녹인 후, 각종 추가물과 함께 미강유를 첨가하되, 이 미강유를 탄산가스를 이용한 초임계추출의 방법으로 추출된 고 농도의 미강유를 일정량 포함하여 녹여붓기의 방법으로 미용에 우수한 천연비누를 제조할 수 있도록 하는데 있다. Therefore, the present invention is proposed in view of the conventional problems as described above, the main object of the invention is to dissolve the soap base, add the rice bran oil with various additives, but the method of supercritical extraction using carbon dioxide gas Including a certain amount of the high concentration of rice bran oil extracted by the method of melting and to be able to manufacture a natural soap excellent in beauty.

상기 목적하는 바를 이루기 위한 본 발명의 특징적인 방법은 비누 베이스(TEA FREE)와, 에센스 오일 등 기타 추가물을 준비하는 기본재료 준비단계; 그리고 통상의 초임계 추출장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 고농도의 미강유를 추출하여 준비하는 미강유 준비단계; 그리고 준비된 비누 베이스를 약 2~7cm로 깎뚝썰기한 후, 스테인레스 통에 넣어 가열로 용해시키는 용해단계; 그리고 녹인 비누 베이스를 잘 저어 가면서 에센스 오일 등을 포함한 추가물을 첨가하는 추가물 첨가단계; 그리고 다시 가열하여 고체화되기 이전에 초임계추출의 방법으로 추출한 고농도의 미강유를 비누 베이스의 중량비 약 2∼5%를 투입하는 미강유 첨가단계; 그리고 상기와 같이 미강유 첨가단계를 마친 비누 베이스를 미리 준비한 성형틀에 붓고 공기가 잔류하지 않도록 마무리하여 약 24시간 보관하는 비누 굳힘단계를 차례로 거쳐 제조하는 것이다. Characteristic method of the present invention for achieving the above object is a base material preparation step of preparing a soap base (TEA FREE) and other additives such as essence oil; And rice bran oil preparation step of extracting and preparing a high concentration of rice bran oil from rice bran (rice bran) using a conventional supercritical extraction equipment and supercritical fluid carbon dioxide (CO 2 ); And after dipping the prepared soap base to about 2 ~ 7cm, dissolution step to dissolve by heating into a stainless steel barrel; And the addition step of adding the addition including the essence oil while stirring the melted soap base well; And the step of adding the rice bran oil to the high concentration of rice bran oil extracted by the method of supercritical extraction before the solidification by heating again, about 2 to 5% by weight of the soap base; Then, the soap base, which has been added with rice bran oil, is poured into a mold prepared in advance and finished so that air does not remain.

이하 본 발명의 제조방법에 따른 실시 예를 자세히 설명한다. Hereinafter, the embodiment according to the manufacturing method of the present invention will be described in detail.

본 발명은 기본재료 준비단계로부터 초임계추출 미강유 준비단계, 재료 용해단계, 추가물 첨가단계, 미강유 첨가단계, 비누 굳힘단계를 거친다. The present invention is subjected to the supercritical extraction rice bran oil preparation step, material dissolution step, additive addition step, rice bran oil addition step, soap solidification step from the basic material preparation step.

먼저, 재료 준비단계에서는 비누 제조에 따른 비누 베이스를 준비하고, 에센스 오일 등 필요한 재료들을 계량한 후 용기에 담아둔다. First, in the material preparation step, a soap base according to soap preparation is prepared, and necessary materials such as essence oil are weighed and placed in a container.

다음으로 미강유 준비단계에서는 초임계추출의 방법으로 쌀겨에서 미강유를 얻어 둔다. Next, rice bran oil is obtained from rice bran by the method of supercritical extraction.

탄산가스 초임계 추출방법은 널리 알려진 원액 추출방법이며, 탄산가스(CO2) 성분의 초임계유체는 혼합물에서 특정 성분을 추출·분리하는 능력이 뛰어나서 식품 분야에서 응용이 활발하다. Carbon dioxide supercritical extraction is a well-known method for extracting undiluted liquor, and the supercritical fluid of carbon dioxide (CO 2 ) is excellent in the ability to extract and separate a specific component from the mixture, and thus is widely applied in the food field.

예컨대, 맥주용 홉 엑스 추출, 커피의 탈 카페인 프로세스 등에 이용되며, 식품의 비가열살균 시스템 등에서도 적용중이다. For example, it is used for hop extracting for beer, decaffeine process of coffee, and the like, and is also applied to food non-heat sterilization system.

따라서 초임계 추출장비와 초임계 추출 유체를 이용하여 쌀겨로부터 미강유를 추출하면 농도가 일반 미강유의 수배에 달한다. Therefore, the extraction of rice bran oil from rice bran using supercritical extraction equipment and supercritical extracting fluid reaches several times the concentration of ordinary rice bran oil.

다음의 재료 용해단계에서는 준비된 비누 베이스를 약 2~7cm로 깎뚝썰기 한 후 스테인레스 용기에 넣고 가열하여 용해시킨다. In the next material dissolving step, the prepared soap base is diced into about 2 ~ 7 cm and then put into a stainless steel container to dissolve by heating.

비누 베이스를 깍뚝썰기 하는 이유는 용해시키기가 쉽도록 하기 위한 것이므로 적당한 크기로 자르면 된다. The reason for dicing the soap base is to make it easier to dissolve, so you can cut it to a suitable size.

다음의 추가물 첨가단계에서는 비누 베이스가 다 녹으면 스테인레스 용기를 불 위에서 꺼낸 상태에서 잘 저으면서 에센스 오일 등의 추가물을 넣는 것이다. In the next addition step, when the soap base is completely dissolved, the stainless steel container is removed from the fire and the addition of essence oil is performed while stirring.

이때의 추가물은 프래그런스 오일, 드라이 허브, 색소 등이 있고, 비누를 사용하고자 하는 취향에 따라 기타 다른 추가물을 포함시킬 수 있다. At this time, the additives are fragrance oils, dry herbs, pigments, and the like, and other additives may be included depending on the taste of using soap.

다음의 미강유 첨가단계에서는 비누 베이스의 중량비 약 2∼5%를 투입한다. In the next step of adding the rice bran oil, about 2 to 5% by weight of the soap base is added.

이어서, 비누 굳힘단계에서는 비누 용액을 미리 준비한 성형틀에 붓고 공기가 잔류하지 않도록 마무리하여 약 24시간 보관하는 것이다. Subsequently, in the soap solidification step, the soap solution is poured into a molding mold prepared in advance and finished so that air does not remain and stored for about 24 hours.

마지막으로 약 24시간 후, 성형틀로부터 비누를 꺼낸 후, 프레스, 절단 및 트리밍하여 완제품화 한다. Finally, after about 24 hours, the soap is removed from the mold, and then pressed, cut and trimmed to complete the product.

위에서 상세히 설명한 바와 같은 본 발명은 미강(쌀겨)으로부터 추출한 미강유로써 녹여붓기의 방법으로 비누를 제조하되, 종래와 달리 탄산가스를 이용한 초임계 추출방법을 이용하여 미강유를 추출하여 제조한 것이기 때문에 고농도의 미강유를 사용할 수 있게 된 것이고, 이는 종래의 일반 미강유를 넣어 제조한 비누에 비하여 월등히 우수한 천연비누를 제조할 수 있는 것이다. In the present invention as described in detail above, the soap is prepared by the method of dissolving as rice bran oil extracted from rice bran (rice bran), but unlike the conventional art by extracting rice bran oil using a supercritical extraction method using carbon dioxide gas of high concentration The rice bran oil can be used, which is capable of producing a natural soap that is much superior to the soap prepared by putting conventional rice bran oil.

Claims (1)

비누 베이스와 에센스 오일을 포함하는 추가물을 준비하는 기본 준비단계 ; 초임계 추출 장비와 초임계유체 탄산가스(CO2)를 이용하여 미강(쌀겨)으로부터 고농도의 미강유를 추출하여 준비하는 미강유 준비단계 ; 준비된 비누 베이스를 2~7cm로 깍둑썰기한 후, 스테인레스 통에 넣어 가열로 용해시키는 용해단계 ; 녹인 비누 베이스를 잘 저어 가면서 에센스 오일을 포함한 추가물을 첨가하는 추가물 첨가단계 ; 다시 가열하여 고체화되기 이전에 초임계 추출의 방법으로 추출한 고농도의 미강유를 비누 베이스의 중량비 2 ~ 5 % 를 투입하는 미강유 첨가단계 ; 상기와 같이 미강유 첨가단계를 마친 비누 베이스를 미리 준비한 성형틀에 붓고 공기가 잔류하지 않도록 마무리하여 상기의 비누 베이스가 굳을 때까지 보관하는 비누 굳힘 단계를 차례로 거쳐 제조하는 것을 특징으로 하는 미강유를 이용한 천연비누 제조방법A basic preparation step of preparing an additive comprising a soap base and an essence oil; Rice bran oil preparation step of extracting and preparing a high concentration of rice bran oil from rice bran (rice bran) using a supercritical extraction equipment and supercritical fluid carbon dioxide (CO 2 ); Diced prepared soap base to 2 ~ 7cm, dissolution step to dissolve by heating in a stainless steel barrel; Addition step of adding the addition including the essence oil while stirring the melted soap base well; Rice bran oil addition step of injecting a high concentration of rice bran oil 2 ~ 5% by weight of the soap base before the solidification by heating again; Naturally using the rice bran oil, characterized in that the soap base after the step of adding the rice bran oil is poured into a molding mold prepared in advance and finished so that air does not remain, followed by a soap firming step to store until the soap base is solid. Soap manufacturing method
KR1020070021973A 2007-03-06 2007-03-06 Manufacturing method for rice cream skin soap KR100872784B1 (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970042994A (en) * 1995-12-22 1997-07-26 손경식 Cosmetic soap composition with excellent deodorant effect
JP2005264128A (en) 2004-03-18 2005-09-29 Amyuure:Kk Whitening soap
KR20060091730A (en) * 2005-02-16 2006-08-21 (주)참미래 Soap containing rice germ and rice bran

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970042994A (en) * 1995-12-22 1997-07-26 손경식 Cosmetic soap composition with excellent deodorant effect
JP2005264128A (en) 2004-03-18 2005-09-29 Amyuure:Kk Whitening soap
KR20060091730A (en) * 2005-02-16 2006-08-21 (주)참미래 Soap containing rice germ and rice bran

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