KR100856867B1 - Composites and preparation method of toothpaste containing sulfur salts produced the Himalayas - Google Patents

Abstract

The present invention relates to a toothpaste composition using the Himalayan rock salt extract, the final product of the Himalayan rock salt extract-containing toothpaste composition relates to a method for producing a toothpaste composition using natural materials considered safety and high quality.

In other words, the Himalayan sulfur salt has a functional aspect viewed from the biochemical and anthropological aspects of sulfur, but its use is extremely limited in its primitive methods such as natural hot spring baths and acne skin removal. It was insufficient. Accordingly, the present invention is to provide a method for producing a natural toothpaste composition that satisfies hygiene and consumer needs by adding to the modern toothpaste composition in consideration of the functional and hygienic aspects of the Himalayan rock salt extract.

Himalayan rock salt, salt water salt, bad breath removal, oral composition

Description

Composition and preparation method of toothpaste containing sulfur salts produced the Himalayas

1 is a manufacturing process showing an embodiment of the present invention

The present invention relates to a method for pretreatment (low temperature dissolution, decolorization, salt crystallization, etc.) of the Himalayan rock salt, which is used for manufacturing toothpaste, and more specifically, by preparing a toothpaste using rock salt which is a raw material of the present invention. The purpose is to provide functional toothpaste suitable for added value and consumer preference.

Looking at the related prior art, registration number 10-0085705-0000 is 'toothpaste composition containing bamboo salt' whose main purpose is to prevent periodontal disease prevention, treatment and tooth decay by mixing bamboo salt alone or with sodium chloride, registration number 10 -0067484-0000 relates to a method for the preparation of transparent toothpaste compositions containing granular salts, which are complex and raw materials for the mass production and industrialization due to the pretreatment of raw materials and the limitation of raw materials. The technical situation regarding the safety of the present situation. In addition, as a related patent using rock salt, registration number 20-0332693-0000 is 'crystal lamp using a natural rock salt (fragment)' registration number 20-0323077-0000 'light fixture using rock salt', Application No. 10-2006 -0001214, 'Shoe insole containing rock salt and a method of manufacturing the same' Application No. 20-2005-0015187 is the structure of the lamp holder base of rock salt lamp, Application No. 20-2005-0014841 'Light fixture using rock salt or natural minerals 'Internal structure' and the like has been filed. Therefore, no toothpaste products that have been grafted with pretreated rock salt have been reported so far.

Therefore, in the present invention, using the Himalayan sulfur salts, which are well known for their functionality and safety, in preparing various kinds of functional toothpastes excellent for oral diseases, whitening, dermatitis, blood improvement, etc., the ground powder is not directly treated and grafted. The present invention has been made in view of the technical problem of the present invention, by providing a highly functional toothpaste manufacturing in consideration of safety and economy by applying the raw material processed through (pre) treatment (low temperature dissolution, decolorization, salt crystallization, etc.) to toothpaste manufacturing. Finished

The present invention is characterized by producing a useful toothpaste by grafting to functional toothpaste using Himalayan rock salt (sulfur salt). Therefore, Figure 1 is described in detail the configuration and operation of the present invention as a process diagram of the preferred embodiment of the present invention.

Himalayan rock salt is a salt containing high-quality sulfur, and minerals in the composition obtained by heat treatment of natural rock salt in the Himalayan salt mountain range and the natural raw material from the Himalayan desert tree roots for a long time above 1200 ° C 590mg) Magnesium (300mg) Calcium (290mg), Iron (6.6mg), Manganese (210mg), Iodine (5.3mg), Sodium Chloride (92.26g), It is known that there are no heavy metals than ordinary salt and many useful minerals. . In addition, in terms of efficacy, it is known that there are effects such as oral disease, whitening, dandruff and hair loss, and blood improvement. On the other hand, sulfur in rock salt is a mineral that is absorbed only in the form of organic matter, and is a mineral necessary for tissues of nails, toenails, joints and skin. Its function is to remove harmful toxins through oxidation and reduction in the body, to maintain the equilibrium of acid-alkali, to release heavy metals and toxic substances such as mercury and lead, and to purify cells with resistance to bacteria. Etc. In addition, it is known to maintain the elasticity of the skin and closely act on skin immunity to control acne, rough skin, psoriasis, wrinkles, hair loss and scalp, eczema, skin eczema and the like. Moreover, the large amount of negative ions and far infrared rays generated from rock salt together with minerals help to balance the human body and facilitate metabolism, which is beneficial for internal and external benefits, such as clearing blood and relieving joint pain. Contamination makes the skin rough and smooth, and removes mold, fungi, or toxins from the cells. In addition, the major application of calcium present in large amounts in rock salt forms the skeleton and teeth, as well as regulating metabolic functions in the body by ionic calcium in the blood.

The main component of teeth is a crystalline compound called hydroxy apatite, which is composed of calcium and phosphorus. There are many factors that can damage teeth, but it is a process of balancing the balance of chemical reactions such as natural wear and tear, improper brushing habits, and corrosion caused by acid, a bacterial metabolite. Therefore, the composition of the rock salt is beneficial to oral disease of the teeth, bad breath removal, blood circulation of the gums.

Looking in detail the step-by-step manufacturing method of the present invention using the raw materials grafts,

① rock salt as a raw material is sterilized by heat treatment at 1200 ℃ ~ 1300 ℃ for over 24 hours,

② The step of pulverizing the solidified rock salt with a grinder (Halled SB-4, Sweden) after heating

③ filtering the material of ② (80 mesh) and then mixing the water and crushed rock salt (4: 1 w / w),

④ After dissolving the mixture of ③, the solution is passed through the filter paper (110 mm) under reduced pressure and then the filtrate is ozone treated to remove residual discoloration and odor,

Concentrate the solution of ⑤ ④ to crystallize and then grind to powder,

The final powder and toothpaste composition of ⑥ ⑤, abrasive (precipitated calcium carbonate), wetting agent (glycerine, sorbitol solution), foaming agent (sodium lauryl sulfate), sweetener (xylitol), PH regulator (sodium pyrophosphate), active ingredient (day Mixing with sodium phosphate), fragrance (menthol), solvent (purified water), binder (carboxymethyl cellulose sodium), brightener (titanium dioxide), etc.

⑦ the mixture and powder and flavoring, dilution (glycerol or sorbitol liquid) step,

⑧ is the packaging and product phase of the mixture of ⑦

Hereinafter, the invention will be described in detail with reference to the following examples.

〈 Example 〉

1. Materials and Methods

(1) Toothpaste compositions include abrasives (precipitated calcium carbonate), wetting agents (glycerine, sorbitol liquid), foaming agents (sodium lauryl sulfate), sweeteners (xylitol), PH regulators (sodium pyrophosphate), active ingredients (sodium fluorophosphate) The basic ingredients of toothpaste, such as fragrance (menthol), solvent (purified water), binder (sodium carboxymethyl cellulose) and brightener (titanium dioxide), were purchased commercially.

(2) Rock salt was purchased from Pakistan Himalayan rock salt.

(3) Rock salt extraction and powder production- The raw rock salt was ground in a grinder (Hallde SB-4, Sweden) for 20 minutes and distilled water (20 ℃) to 1: 4 (rock salt: distilled water, w / w) After dissolving, the solution was passed through filter paper (110 mm) under reduced pressure, and the filtrate was then ozonated to remove residual discoloration and odor. At this time, ozone was used, and ozone treatment was performed for 10 minutes with an ozone concentration of 0.01 PPM. The ozone generator used a generator (Woosung Hitech, SP-100, Korea) that can adjust the amount of generation by voltage, and the ozone concentration was measured by an ozone monitor (Ibara, PL-320, Japan). In the next step, a general vacuum concentrator was concentrated to 95 ~ 98% of the initial weight, and then pulverized and powdered.

(4) Elimination of bad breath-After 20 men and women who are aware of bad breath have been subjected to clinical trials, the same type of meal was used, and the degree of bad breath using a halimeter (Model SB-17, USA) After the exclusion from the experiment, very strong people (over 350) were divided into 5 groups in the Comparative Examples and Examples, and the average value was adjusted to be similar between the groups. After 20 minutes, the first meal after 30 minutes and 60 minutes after the same meal was measured and the toothbrush and toothpaste after each composition (Example) was measured in 30 minutes and 60 minutes after the last 3 minutes after the same method was measured

(5) Gingivitis Inhibition Test- This experiment was conducted on 20 subjects in a relatively same environment. The test method was a single blind method, in which all subjects were given the same detergent and toothbrush during the residual effect removal period of 4 weeks before the experiment.

Experimental method was calculated as the average value of the index by dividing the gingiva per tooth into the buccal and lingual. Each gingivitis was evaluated from 0 to 3 points according to the scores of Loe and Silnis. The gingivitis index of each tooth was calculated, and the average gingivitis index of the individual was calculated. .

(6) Bacterial Membrane Index Comparison-20 subjects in the same environment were compared. All the subjects underwent a first-order oral examination before the test to obtain a baseline. The experiment was applied with a single blind method and all subjects were given the same dentifrice and toothbrush of the same standard during the residual effect removal period for 4 weeks prior to the experiment. In this method, 20 ml of water was mixed with 10 drops of plaque, mixed for 1 minute in the mouth, spited out, lightly brushed with water, and the coloration was applied to Quigley & Hein's Turesky modification criteria. .

(7) Rock Salt Toothpaste Composition Preparation

Table 1. Preparation of Rock Salt Toothpaste Composition

(weight%)

number Ingredient Name Comparative Example 1 Example 1 Example 2 Example 3  One  Precipitated Calcium Carbonate  37  25  25  20  2  Glycerol  -  50  -  -  3  Sorbitol  40  -  40  44  4  Lauryl sulfate  2.0  0.01  2.0  2.0  5  Xylitol  1.5  1.0  2.0  2.0  6  Narium Pyrophosphate  2.5  0.48  2.0  3.0  7  Sodium monofluorophosphate  0.5  1.0  0.5  1.0  8  Titanium dioxide  1.0  0.5  0.5  0.5  9 Carboxymethyl Cellulose Sodium  1.5  1.0  1.5  1.0  10  Tranexamic acid  0.5  0.5  0.5  0.5  11  Spices  1.0  1.5  1.0  1.0  12  Treated Rock Salt  -  0.01  2.0  5.0  13  Purified water  Remaining amount  Remaining amount  Remaining amount  Remaining amount  14  system  100  100  100  100

2. Results and Summary

Table 2. Bad Breath Removal Effects

Treatment sphere base line 30 minutes after eating 60 minutes after eating Comparative Example 1 200 150 170 Example 1 200 140 160 Example 2 210 130 150 Example 3 220 150 165

1) The given value is the average of two experiments

<Result>

 ① In Comparative Example 1, the bad breath removal rate was 30 minutes after eating and 60 minutes after eating.

    15 ~ 25% decrease compared to

 ② Examples 1, 2 and 3 showed a decrease of about 20 to 38% compared to the baseline, and in particular, the case of Example 2 showed the largest decrease of 29 to 38%.

Table 3. Comparison of gingivitis inhibition

Treatment sphere base line 2 months later 4 months later Comparative Example 1 0.63 0.59 0.60 Example 1 0.62 0.50 0.47 Example 2 0.61 0.52 0.38 Example 3 0.62 0.53 0.49

1) The given value is the average of two experiments

<Result>

 ① In Comparative Example 1, there is no significant change even after 2 to 4 months.

 ② In the case of Examples 1, 2 and 3, the reduction was 15-19% after 2 months and 21-38% after 4 months.

 ③ The case of Example 2 showed the greatest reduction.

Table 4. Comparison of Dental Bacterial Membrane Index

Treatment sphere base line 2 months later 4 months later Comparative Example 1 0.77 0.77 0.76 Example 1 0.76 0.70 0.63 Example 2 0.76 0.65 0.44 Example 3 0.75 0.65 0.56

1) The given value is averaged twice in the experiment.

<Result>

 ① Comparative Example 1 shows no significant change after 2 months and 4 months.

 ② Examples 1, 2 and 3 show a decrease of 8 to 14% compared to the baseline after 2 months and a decrease of 18 to 42% after 4 months.

 ③ Example 2 shows the largest reduction.

Functional toothpaste using the Himalayan natural rock salt extract provided by the present invention as described in detail above is excellent in preventing or preventing bad breath diseases and gum disease such as gingivitis. Therefore, by applying to various types of functional toothpaste through the present invention, it is an invention that can greatly benefit the national economy with high added value considering safety and economic feasibility.

Claims (2)

delete In the manufacture of toothpaste, Heat-treat the Himalayan rock salt at 1200 ° C. to 1300 ° C. for at least 24 hours, then grind the solidified rock salt with a grinder, filter the material (80 mesh), and mix the water with the filtered rock salt 4: 1 by weight, After the ozone treatment (dissolved ozone 0.01 PPM, treatment time 10 minutes), the total weight of the other toothpaste composition through the compounding process of the composition consisting of powdering the material consisting of the concentrated concentration under reduced pressure to 95 ~ 98% after ozone treatment Toothpaste manufacturing method containing Himalayan rock salt comprising the composition comprising 0.01 to 5% by weight.

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