JPS6348448A - 測定試料の熱容量の測定法並びに熱量計 - Google Patents
測定試料の熱容量の測定法並びに熱量計Info
- Publication number
- JPS6348448A JPS6348448A JP61191955A JP19195586A JPS6348448A JP S6348448 A JPS6348448 A JP S6348448A JP 61191955 A JP61191955 A JP 61191955A JP 19195586 A JP19195586 A JP 19195586A JP S6348448 A JPS6348448 A JP S6348448A
- Authority
- JP
- Japan
- Prior art keywords
- temperature
- support means
- measurement
- sample support
- thermal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000005259 measurement Methods 0.000 title claims description 48
- 238000000034 method Methods 0.000 title claims description 16
- 239000000523 sample Substances 0.000 claims description 37
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000013074 reference sample Substances 0.000 claims description 11
- 230000007613 environmental effect Effects 0.000 claims description 6
- 230000001419 dependent effect Effects 0.000 claims description 4
- 229910052732 germanium Inorganic materials 0.000 claims description 4
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims description 4
- 230000008878 coupling Effects 0.000 claims description 3
- 238000010168 coupling process Methods 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 3
- 229910052594 sapphire Inorganic materials 0.000 claims description 3
- 239000010980 sapphire Substances 0.000 claims description 3
- 239000007769 metal material Substances 0.000 claims description 2
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims 1
- 238000001816 cooling Methods 0.000 description 9
- 238000007707 calorimetry Methods 0.000 description 6
- 238000010586 diagram Methods 0.000 description 6
- 229910052734 helium Inorganic materials 0.000 description 5
- 239000001307 helium Substances 0.000 description 5
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 230000007274 generation of a signal involved in cell-cell signaling Effects 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000004020 conductor Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical group [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 238000002076 thermal analysis method Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 208000031636 Body Temperature Changes Diseases 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 229910018487 Ni—Cr Inorganic materials 0.000 description 1
- 241000233805 Phoenix Species 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 229920002522 Wood fibre Polymers 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 description 1
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000012886 linear function Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000007738 vacuum evaporation Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000002025 wood fiber Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4846—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample
- G01N25/4866—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample by using a differential method
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3529489.2 | 1985-08-16 | ||
| DE19853529489 DE3529489A1 (de) | 1985-08-16 | 1985-08-16 | Verfahren und einrichtung zum bestimmen der waermekapazitaet einer probe |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6348448A true JPS6348448A (ja) | 1988-03-01 |
Family
ID=6278736
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61191955A Pending JPS6348448A (ja) | 1985-08-16 | 1986-08-15 | 測定試料の熱容量の測定法並びに熱量計 |
Country Status (4)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019049502A (ja) * | 2017-09-12 | 2019-03-28 | エスペック株式会社 | 熱容量測定装置及び熱容量測定方法 |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2626371B1 (fr) * | 1988-01-25 | 1991-09-20 | Agronomique Inst Nat Rech | Methode d'etude et de controle des changements d'etat d'un milieu liquide ou gelifie par mesure differentielle des caracteristiques thermiques dudit milieu et dispositif capteur pour la mise en oeuvre de cette method |
| US5217690A (en) * | 1989-05-05 | 1993-06-08 | The United States Of America As Represented By The Department Of Health And Human Services | All tantallum stopped flow microcalorimeter |
| US5186540A (en) * | 1991-12-30 | 1993-02-16 | Raytheon Company | Power measurement calorimeter |
| US5335993A (en) * | 1992-03-02 | 1994-08-09 | Ta Instruments, Inc. | Method and apparatus for thermal conductivity measurements |
| US5248199A (en) * | 1992-03-02 | 1993-09-28 | Ta Instruments, Inc. | Method and apparatus for spatially resolved modulated differential analysis |
| US5439291C1 (en) * | 1992-03-02 | 2002-04-16 | Ta Instr Inc | Method and apparatus for ac differential thermal analysis |
| US5224775C2 (en) * | 1992-03-02 | 2002-04-23 | Ta Instr Inc | Method and apparatus for modulated differential analysis |
| US5624187A (en) * | 1992-03-02 | 1997-04-29 | Ta Instruments, Inc. | Method and apparatus for gas flow modulated differential scanning calorimetry |
| US5474385A (en) * | 1992-03-02 | 1995-12-12 | Ta Instruments, Inc. | Method and apparatus for parsed dynamic differential analysis |
| US5549387A (en) * | 1994-06-01 | 1996-08-27 | The Perkin-Elmer Corporation | Apparatus and method for differential analysis using real and imaginary signal components |
| JP3556227B2 (ja) * | 1994-06-01 | 2004-08-18 | ザ パーキン−エルマー コーポレイション | 実部信号成分と虚部信号成分を用いた示差分析のための装置および方法 |
| TW473518B (en) | 1995-07-28 | 2002-01-21 | Ciba Sc Holding Ag | Soluble chromophores containing solubilising groups which can be easily removed |
| US5965606A (en) * | 1995-12-29 | 1999-10-12 | Allergan Sales, Inc. | Methods of treatment with compounds having RAR.sub.α receptor specific or selective activity |
| DE69730699T2 (de) * | 1996-11-01 | 2005-08-18 | TA Instruments, Inc., New Castle | Differentialabtastkalorimeter |
| US5973299A (en) * | 1996-11-01 | 1999-10-26 | Ta Instruments, Inc. | System and method for heater control for evaporation of cryogenic fluids for cooling scientific instruments |
| US5806979A (en) * | 1996-11-19 | 1998-09-15 | Iowa State University Research Foundation, Inc. | Calorimetric system and method |
| USD412991S (en) | 1997-01-16 | 1999-08-17 | The Perkin-Elmer Corp. | Enclosure for analytical instrumentation |
| US6113261A (en) * | 1997-06-27 | 2000-09-05 | Ta Instruments, Inc. | Method and apparatus of modulated-temperature thermogravimetry |
| JP3434694B2 (ja) * | 1997-12-01 | 2003-08-11 | セイコーインスツルメンツ株式会社 | 示差走査熱量計 |
| US6238085B1 (en) * | 1998-12-31 | 2001-05-29 | Honeywell International Inc. | Differential thermal analysis sensor |
| DE19910924A1 (de) * | 1999-03-12 | 2000-09-14 | Mettler Toledo Gmbh | Kryostat-Kalorimeter |
| US6193413B1 (en) * | 1999-06-17 | 2001-02-27 | David S. Lieberman | System and method for an improved calorimeter for determining thermodynamic properties of chemical and biological reactions |
| US6488406B2 (en) | 2000-03-23 | 2002-12-03 | Ta Instruments-Waters, Llc | Differential scanning calorimeter |
| US6561692B2 (en) | 2000-03-23 | 2003-05-13 | Ta Instruments-Waters Llc | Differential scanning calorimeter |
| US6431747B1 (en) | 2000-03-23 | 2002-08-13 | Ta Instruments, Inc. | Heat flux differential scanning calorimeter sensor |
| US6428203B1 (en) | 2000-03-23 | 2002-08-06 | Ta Instruments, Inc. | Power compensation differential scanning calorimeter |
| ES2162766B1 (es) * | 2000-06-15 | 2003-04-01 | Consejo Superior Investigacion | Microcalorimetro de combustion. |
| US6843595B2 (en) * | 2001-01-26 | 2005-01-18 | Waters Investment Limited | Differential scanning calorimeter accounting for heat leakage |
| US6641300B1 (en) | 2001-01-29 | 2003-11-04 | Waters Investment, Ltd. | Differential scanning calorimeter |
| US6648504B2 (en) | 2002-03-01 | 2003-11-18 | Waters Investment Limited | System and method for calibrating contact thermal resistances in differential scanning calorimeters |
| JP4116526B2 (ja) * | 2003-11-18 | 2008-07-09 | エスアイアイ・ナノテクノロジー株式会社 | 第二のヒーターを備えた示差走査熱量計 |
| US7371006B2 (en) * | 2004-02-10 | 2008-05-13 | Perkinelmer Las, Inc. | Differential scanning calorimeter (DSC) with temperature controlled furnace |
| EP2133690B1 (en) * | 2008-06-13 | 2011-03-09 | Mettler-Toledo AG | Thermoanalytical instrument with dynamic power compensation |
| US8418480B2 (en) * | 2008-12-18 | 2013-04-16 | Waters Technologies Corporation | Cooling system using positive displacement cryogenic liquid pump |
| FI126419B (en) * | 2014-12-30 | 2016-11-30 | Valmet Technologies Oy | Method of measuring heat or rate of heat generated from a slow reaction of a substance or substances |
| WO2019045901A1 (en) | 2017-08-31 | 2019-03-07 | Waters Technologies Corporation | HYBRID CALORIMETER CELL |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3643491A (en) * | 1968-10-11 | 1972-02-22 | Du Pont | Derivative differential scanning microcalorimeter |
| JPS53496A (en) * | 1976-06-23 | 1978-01-06 | Toshiba Corp | Laser working control method |
| US4255961A (en) * | 1978-10-17 | 1981-03-17 | University Of Va. Alumni Patents Foundation | Differential calorimeter based on the heat leak principle |
| JPS60209158A (ja) * | 1984-03-31 | 1985-10-21 | Shimadzu Corp | 熱流束示差走査熱量計用試料セル |
-
1985
- 1985-08-16 DE DE19853529489 patent/DE3529489A1/de active Granted
-
1986
- 1986-08-13 FR FR868611687A patent/FR2586297B1/fr not_active Expired - Lifetime
- 1986-08-15 JP JP61191955A patent/JPS6348448A/ja active Pending
- 1986-08-18 US US06/897,530 patent/US4783174A/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019049502A (ja) * | 2017-09-12 | 2019-03-28 | エスペック株式会社 | 熱容量測定装置及び熱容量測定方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3529489A1 (de) | 1987-02-26 |
| DE3529489C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-06-23 |
| FR2586297A1 (fr) | 1987-02-20 |
| FR2586297B1 (fr) | 1990-04-27 |
| US4783174A (en) | 1988-11-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPS6348448A (ja) | 測定試料の熱容量の測定法並びに熱量計 | |
| US4944035A (en) | Measurement of thermal conductivity and specific heat | |
| US4956793A (en) | Method and apparatus for measuring the density of fluids | |
| US5288147A (en) | Thermopile differential thermal analysis sensor | |
| Gravelle | Heat-flow microcalorimetry and its application to heterogeneous catalysis | |
| US5177696A (en) | Method of determination of gas properties at reference conditions | |
| US5038304A (en) | Calibration of thermal conductivity and specific heat devices | |
| US7626144B2 (en) | Method and apparatus for rapid temperature changes | |
| US20130121369A1 (en) | Adiabatic scanning calorimeter | |
| US3971246A (en) | Method and apparatus for measuring the coefficient of thermal conductivity of a sample | |
| Gmelin et al. | Automatic low temperature calorimetry for the range 0.3-320K | |
| EP0711431B1 (en) | Thermostatic method and device | |
| US3298220A (en) | Thermocouple for dta | |
| Inaba | Nano-watt stabilized DSC and ITS applications | |
| US4073182A (en) | Temperature compensated optical measuring instruments | |
| JPS6140062B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| US4623263A (en) | Apparatus for the thermal measurement of the texture of a porous body | |
| Stokka et al. | A simple system for automatic specific heat measurements | |
| Ostrovskii | Differential microcalorimeter for isothermal measurements of heat effects in two-phase systems and examples of its application | |
| US4140396A (en) | Measuring instrument | |
| Compans | Dynamic method for in situ measurement of the thermoelectric power of vapor quenched thin films | |
| Finotello et al. | AC calorimetric studies of phase transitions in porous substrates. Superfluid helium and liquid crystals | |
| Zrudsky et al. | A high resolution dynamic technique of thermoelectric power measurements | |
| Guy et al. | Temperature measurement in high pressure cells using a rhodium+ 0.5% iron-chromel thermocouple pair | |
| US3498113A (en) | Method and apparatus for determining solute concentrations |