JPS6310711B2 - - Google Patents
Info
- Publication number
- JPS6310711B2 JPS6310711B2 JP6519977A JP6519977A JPS6310711B2 JP S6310711 B2 JPS6310711 B2 JP S6310711B2 JP 6519977 A JP6519977 A JP 6519977A JP 6519977 A JP6519977 A JP 6519977A JP S6310711 B2 JPS6310711 B2 JP S6310711B2
- Authority
- JP
- Japan
- Prior art keywords
- deoxyglucopyranosylhexopyranoside
- stirring
- reaction
- present
- glucopyranosyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000001951 carbamoylamino group Chemical group C(N)(=O)N* 0.000 claims description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 8
- 238000003756 stirring Methods 0.000 description 7
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 238000000862 absorption spectrum Methods 0.000 description 2
- 238000000921 elemental analysis Methods 0.000 description 2
- 239000012948 isocyanate Substances 0.000 description 2
- FEMOMIGRRWSMCU-UHFFFAOYSA-N ninhydrin Chemical compound C1=CC=C2C(=O)C(O)(O)C(=O)C2=C1 FEMOMIGRRWSMCU-UHFFFAOYSA-N 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- YSVQUZOHQULZQP-OCEKCAHXSA-N trehalosamine Chemical compound N[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 YSVQUZOHQULZQP-OCEKCAHXSA-N 0.000 description 2
- BCMYXYHEMGPZJN-UHFFFAOYSA-N 1-chloro-2-isocyanatoethane Chemical compound ClCCN=C=O BCMYXYHEMGPZJN-UHFFFAOYSA-N 0.000 description 1
- 125000001340 2-chloroethyl group Chemical group [H]C([H])(Cl)C([H])([H])* 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- -1 alkyl isocyanate Chemical class 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 150000002402 hexoses Chemical group 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- HAMGRBXTJNITHG-UHFFFAOYSA-N methyl isocyanate Chemical compound CN=C=O HAMGRBXTJNITHG-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6519977A JPS53149931A (en) | 1977-06-01 | 1977-06-01 | 2-(3-alkylureido)-hexapyranoside derivatives |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6519977A JPS53149931A (en) | 1977-06-01 | 1977-06-01 | 2-(3-alkylureido)-hexapyranoside derivatives |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS53149931A JPS53149931A (en) | 1978-12-27 |
JPS6310711B2 true JPS6310711B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-03-08 |
Family
ID=13279997
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP6519977A Granted JPS53149931A (en) | 1977-06-01 | 1977-06-01 | 2-(3-alkylureido)-hexapyranoside derivatives |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS53149931A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
-
1977
- 1977-06-01 JP JP6519977A patent/JPS53149931A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS53149931A (en) | 1978-12-27 |
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