JPS6257067B2 - - Google Patents
Info
- Publication number
- JPS6257067B2 JPS6257067B2 JP55029509A JP2950980A JPS6257067B2 JP S6257067 B2 JPS6257067 B2 JP S6257067B2 JP 55029509 A JP55029509 A JP 55029509A JP 2950980 A JP2950980 A JP 2950980A JP S6257067 B2 JPS6257067 B2 JP S6257067B2
- Authority
- JP
- Japan
- Prior art keywords
- sample
- nozzle
- jet
- working gas
- gasified
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000523 sample Substances 0.000 claims description 76
- 239000007788 liquid Substances 0.000 claims description 45
- 238000000034 method Methods 0.000 claims description 24
- 238000004458 analytical method Methods 0.000 claims description 22
- 238000004811 liquid chromatography Methods 0.000 claims description 16
- 230000007246 mechanism Effects 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 12
- 238000000889 atomisation Methods 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000012141 concentrate Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 239000012468 concentrated sample Substances 0.000 claims description 3
- 239000007789 gas Substances 0.000 description 30
- 150000001875 compounds Chemical class 0.000 description 10
- 238000004128 high performance liquid chromatography Methods 0.000 description 8
- 238000004895 liquid chromatography mass spectrometry Methods 0.000 description 8
- 230000003321 amplification Effects 0.000 description 5
- 238000000752 ionisation method Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000003199 nucleic acid amplification method Methods 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 238000004949 mass spectrometry Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000008878 coupling Effects 0.000 description 3
- 238000010168 coupling process Methods 0.000 description 3
- 238000005859 coupling reaction Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000001819 mass spectrum Methods 0.000 description 3
- 230000008016 vaporization Effects 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 238000000451 chemical ionisation Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229910001369 Brass Inorganic materials 0.000 description 1
- 102000015636 Oligopeptides Human genes 0.000 description 1
- 108010038807 Oligopeptides Proteins 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000001282 iso-butane Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 150000003431 steroids Chemical class 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0468—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample
- H01J49/049—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample with means for applying heat to desorb the sample; Evaporation
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0431—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples
- H01J49/0445—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples with means for introducing as a spray, a jet or an aerosol
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0431—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples
- H01J49/0454—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples with means for vaporising using mechanical energy, e.g. by ultrasonic vibrations
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Electron Tubes For Measurement (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2950980A JPS56126241A (en) | 1980-03-07 | 1980-03-07 | Method and apparatus for introducing a sample into an analyzer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2950980A JPS56126241A (en) | 1980-03-07 | 1980-03-07 | Method and apparatus for introducing a sample into an analyzer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS56126241A JPS56126241A (en) | 1981-10-03 |
| JPS6257067B2 true JPS6257067B2 (enrdf_load_stackoverflow) | 1987-11-28 |
Family
ID=12278058
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2950980A Granted JPS56126241A (en) | 1980-03-07 | 1980-03-07 | Method and apparatus for introducing a sample into an analyzer |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS56126241A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0399171A (ja) * | 1989-09-11 | 1991-04-24 | Matsushita Electric Ind Co Ltd | ヒートポンプ式空気調和機 |
| CN1331400C (zh) * | 2005-11-10 | 2007-08-15 | 上海交通大学 | 复合光触媒抗菌剂的制备方法 |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4814612A (en) * | 1983-08-30 | 1989-03-21 | Research Corporation | Method and means for vaporizing liquids for detection or analysis |
| US4730111A (en) * | 1983-08-30 | 1988-03-08 | Research Corporation | Ion vapor source for mass spectrometry of liquids |
| US4861989A (en) * | 1983-08-30 | 1989-08-29 | Research Corporation Technologies, Inc. | Ion vapor source for mass spectrometry of liquids |
| JPS61193062A (ja) * | 1985-02-21 | 1986-08-27 | Okazaki Kokuritsu Kyodo Kenkyu Kikouchiyou | 液体クロマトグラフ・質量分析器直結用インタ−フエ−ス装置 |
| JPH0722727B2 (ja) * | 1986-05-08 | 1995-03-15 | スペクトラム コントロール インコーポレーテツド | モノマー液体の霧化及び気化蒸着装置 |
| JP2528837B2 (ja) * | 1986-10-11 | 1996-08-28 | 孝雄 津田 | 液体クロマトグラフから質量分析計への試料導入方法およびその導入器 |
| DE10014962A1 (de) | 2000-03-25 | 2001-10-04 | Gsf Forschungszentrum Umwelt | Pulsbares Kapillarventil |
| FR2817088B1 (fr) * | 2000-11-17 | 2003-02-21 | Mecanique Magnetique Sa | Machine tournante a butee axiale magnetique integrant une generatrice de courant |
| JP4521255B2 (ja) * | 2004-11-29 | 2010-08-11 | 株式会社日立ハイテクノロジーズ | キャピラリーカラム接続部材及びエレクトロスプレーイオン源 |
| JP5663725B2 (ja) * | 2010-09-03 | 2015-02-04 | 学校法人日本大学 | 質量分析装置用試料導入装置 |
-
1980
- 1980-03-07 JP JP2950980A patent/JPS56126241A/ja active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0399171A (ja) * | 1989-09-11 | 1991-04-24 | Matsushita Electric Ind Co Ltd | ヒートポンプ式空気調和機 |
| CN1331400C (zh) * | 2005-11-10 | 2007-08-15 | 上海交通大学 | 复合光触媒抗菌剂的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS56126241A (en) | 1981-10-03 |
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