JPS6254777B2 - - Google Patents
Info
- Publication number
- JPS6254777B2 JPS6254777B2 JP58189279A JP18927983A JPS6254777B2 JP S6254777 B2 JPS6254777 B2 JP S6254777B2 JP 58189279 A JP58189279 A JP 58189279A JP 18927983 A JP18927983 A JP 18927983A JP S6254777 B2 JPS6254777 B2 JP S6254777B2
- Authority
- JP
- Japan
- Prior art keywords
- gas
- reaction
- reactor
- fluorine
- purity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910001512 metal fluoride Inorganic materials 0.000 claims description 17
- KWVVTSALYXIJSS-UHFFFAOYSA-L silver(ii) fluoride Chemical compound [F-].[F-].[Ag+2] KWVVTSALYXIJSS-UHFFFAOYSA-L 0.000 claims description 6
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 229910021571 Manganese(III) fluoride Inorganic materials 0.000 claims description 4
- SRVINXWCFNHIQZ-UHFFFAOYSA-K manganese(iii) fluoride Chemical compound [F-].[F-].[F-].[Mn+3] SRVINXWCFNHIQZ-UHFFFAOYSA-K 0.000 claims description 4
- QYSGYZVSCZSLHT-UHFFFAOYSA-N octafluoropropane Chemical compound FC(F)(F)C(F)(F)C(F)(F)F QYSGYZVSCZSLHT-UHFFFAOYSA-N 0.000 claims description 4
- 229960004065 perflutren Drugs 0.000 claims description 4
- 229910021583 Cobalt(III) fluoride Inorganic materials 0.000 claims description 2
- WZJQNLGQTOCWDS-UHFFFAOYSA-K cobalt(iii) fluoride Chemical compound F[Co](F)F WZJQNLGQTOCWDS-UHFFFAOYSA-K 0.000 claims description 2
- 239000007789 gas Substances 0.000 description 25
- 238000006243 chemical reaction Methods 0.000 description 19
- 238000000034 method Methods 0.000 description 16
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 14
- 239000011737 fluorine Substances 0.000 description 14
- 229910052731 fluorine Inorganic materials 0.000 description 14
- 238000003682 fluorination reaction Methods 0.000 description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000006227 byproduct Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 3
- 229910001634 calcium fluoride Inorganic materials 0.000 description 3
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000012025 fluorinating agent Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- CTNMMTCXUUFYAP-UHFFFAOYSA-L difluoromanganese Chemical compound F[Mn]F CTNMMTCXUUFYAP-UHFFFAOYSA-L 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- GKXWTRSVUPXQMM-UHFFFAOYSA-N 1,1,1,2,2-pentachloro-3,3,3-trifluoropropane Chemical compound FC(F)(F)C(Cl)(Cl)C(Cl)(Cl)Cl GKXWTRSVUPXQMM-UHFFFAOYSA-N 0.000 description 1
- OPLWDQVQIWKMSG-UHFFFAOYSA-N 1-chloro-1-fluoropropane Chemical class CCC(F)Cl OPLWDQVQIWKMSG-UHFFFAOYSA-N 0.000 description 1
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminium flouride Chemical compound F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 description 1
- 229910021582 Cobalt(II) fluoride Inorganic materials 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 229910001515 alkali metal fluoride Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000003842 bromide salts Chemical class 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 description 1
- YCYBZKSMUPTWEE-UHFFFAOYSA-L cobalt(ii) fluoride Chemical compound F[Co]F YCYBZKSMUPTWEE-UHFFFAOYSA-L 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- -1 fluorosilicates Chemical class 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- UKACHOXRXFQJFN-UHFFFAOYSA-N heptafluoropropane Chemical compound FC(F)C(F)(F)C(F)(F)F UKACHOXRXFQJFN-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000004694 iodide salts Chemical class 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 238000011403 purification operation Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000003826 tablet Substances 0.000 description 1
- JOHWNGGYGAVMGU-UHFFFAOYSA-N trifluorochlorine Chemical compound FCl(F)F JOHWNGGYGAVMGU-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18927983A JPS6081134A (ja) | 1983-10-12 | 1983-10-12 | オクタフルオロプロパンの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18927983A JPS6081134A (ja) | 1983-10-12 | 1983-10-12 | オクタフルオロプロパンの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6081134A JPS6081134A (ja) | 1985-05-09 |
| JPS6254777B2 true JPS6254777B2 (zh) | 1987-11-17 |
Family
ID=16238653
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18927983A Granted JPS6081134A (ja) | 1983-10-12 | 1983-10-12 | オクタフルオロプロパンの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6081134A (zh) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4335179A1 (de) * | 1993-10-15 | 1995-04-20 | Solvay Fluor & Derivate | Verfahren zur Herstellung von Pentafluorethan und zur Reinigung von 1,1,1,2-Tetrafluorethan |
| JP4539793B2 (ja) * | 2000-08-30 | 2010-09-08 | 昭和電工株式会社 | オクタフルオロプロパンの製造方法及びその用途 |
| TWI288025B (en) | 2000-09-14 | 2007-10-11 | Showa Denko Kk | Adsorbent for purifying perfluorocarbon, process for producing same, high purity octafluoropropane and octafluorocyclobutane, and use thereof |
| US7041264B2 (en) | 2001-01-15 | 2006-05-09 | Showa Denko K.K. | Process for purifying octafluoropropane |
| KR100447804B1 (ko) * | 2001-07-09 | 2004-09-08 | 울산화학주식회사 | 고순도 퍼플루오로프로판의 제조방법 |
| JP4822255B2 (ja) * | 2005-10-17 | 2011-11-24 | 独立行政法人産業技術総合研究所 | １，１，２，２，３−ペンタフルオロシクロブタンの製造方法 |
| JP2007176842A (ja) * | 2005-12-27 | 2007-07-12 | Showa Denko Kk | オクタフルオロプロパンの製造方法 |
| CN103497086A (zh) * | 2013-09-22 | 2014-01-08 | 佛山市华特气体有限公司 | 八氟丙烷的制备方法 |
-
1983
- 1983-10-12 JP JP18927983A patent/JPS6081134A/ja active Granted
Non-Patent Citations (1)
| Title |
|---|
| THE JOURNAL OF ORGANIC CHEMISTRY 28=1963 * |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6081134A (ja) | 1985-05-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US10464869B2 (en) | Processes for selective dehydrohalogenation of halogenated alkanes | |
| US7135601B2 (en) | Catalytic method for the production of fluoroalkylenes from chlorofluorohydrocarbons | |
| US7799959B2 (en) | Process for producing 1,2,3,4-tetrachlorohexafluorobutane | |
| US7812202B2 (en) | Process for producing hexafluoro-1,3-butadiene | |
| KR20100040897A (ko) | 할로겐화 하이드로카본의 촉매 디하이드로할로겐화에 의한 플루오르화 올레핀의 제조 | |
| JP3213929B2 (ja) | １，１，１，２，３，３，３−ヘプタフルオロプロパンの製造方法 | |
| JP3248184B2 (ja) | １，１，１，３，３‐ペンタフルオロプロパンの製造方法，及び１，１，１，３，３‐ペンタフルオロ‐２，３‐ジクロロプロパンの製造方法 | |
| KR20170053624A (ko) | 클로로트리플루오로에틸렌 제조방법 | |
| US3591646A (en) | Process for obtaining halogenated,fluorine containing organic compounds | |
| JPS6254777B2 (zh) | ||
| EP0462514B1 (en) | Process for preparing 1-chloro-2,2,2-trifluoroethane | |
| EP0712826A1 (en) | 1,1,1-Trifluoroethane synthesis using a supported lewis acid | |
| EP0515402A1 (en) | METHOD FOR FLUORINATION BY HALOGEN EXCHANGE. | |
| CN1054970A (zh) | 卤素交换氟化反应 | |
| JP4727830B2 (ja) | １，１，１−トリフルオロ−２，２−ジクロロエタンの製造方法 | |
| US5574193A (en) | Initiators for telomerization of polyfluoroalkyl iodides with fluoroolefins | |
| EP0366404B1 (en) | Improved process for the preparation of 1,1,1,2-tetrafluoroethane | |
| KR930002956B1 (ko) | 액상 플루오르화 반응용 촉매 | |
| JPH0665117A (ja) | １，１，１，２−テトラフルオロエタンの製造法 | |
| KR950008281B1 (ko) | 퍼할로히드로카본 하이포클로라이트의 제조방법 | |
| US20100121117A1 (en) | Process for preparing decafluorocyclohexene | |
| US5008476A (en) | Process for the preparation of 1,1,1,2-tetrafluoroethane | |
| US5545776A (en) | Synthesis of n-perfluorooctyl bromide | |
| JPS60109533A (ja) | ヘキサフルオロエタンの製造方法 | |
| EP0728126A1 (en) | Preparation of 1,1,2,3,3-pentafluoropropane |