JPS62228289A - 油脂の加水分解方法 - Google Patents
油脂の加水分解方法Info
- Publication number
- JPS62228289A JPS62228289A JP61072324A JP7232486A JPS62228289A JP S62228289 A JPS62228289 A JP S62228289A JP 61072324 A JP61072324 A JP 61072324A JP 7232486 A JP7232486 A JP 7232486A JP S62228289 A JPS62228289 A JP S62228289A
- Authority
- JP
- Japan
- Prior art keywords
- oil
- fat
- lipase
- substrate
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006460 hydrolysis reaction Methods 0.000 title claims description 32
- 230000007062 hydrolysis Effects 0.000 title claims description 15
- 102000004882 Lipase Human genes 0.000 claims abstract description 27
- 108090001060 Lipase Proteins 0.000 claims abstract description 27
- 239000004367 Lipase Substances 0.000 claims abstract description 27
- 235000019421 lipase Nutrition 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000000758 substrate Substances 0.000 claims abstract description 16
- 239000007853 buffer solution Substances 0.000 claims abstract description 11
- 230000003301 hydrolyzing effect Effects 0.000 claims abstract description 8
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 7
- 102000004190 Enzymes Human genes 0.000 claims abstract description 3
- 108090000790 Enzymes Proteins 0.000 claims abstract description 3
- 239000003960 organic solvent Substances 0.000 claims abstract description 3
- 239000003925 fat Substances 0.000 claims description 23
- 239000003921 oil Substances 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 21
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 15
- 150000004665 fatty acids Chemical group 0.000 claims description 8
- 239000000872 buffer Substances 0.000 claims description 4
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 claims description 3
- 150000004671 saturated fatty acids Chemical class 0.000 claims description 2
- 235000003441 saturated fatty acids Nutrition 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 abstract description 6
- 239000003995 emulsifying agent Substances 0.000 abstract 1
- 230000000415 inactivating effect Effects 0.000 abstract 1
- 229940040461 lipase Drugs 0.000 description 23
- 235000019197 fats Nutrition 0.000 description 19
- 235000019198 oils Nutrition 0.000 description 17
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 15
- 238000002844 melting Methods 0.000 description 10
- 230000008018 melting Effects 0.000 description 10
- 235000019482 Palm oil Nutrition 0.000 description 7
- 239000002540 palm oil Substances 0.000 description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- 235000014593 oils and fats Nutrition 0.000 description 5
- 239000004006 olive oil Substances 0.000 description 4
- 235000008390 olive oil Nutrition 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 3
- 241001135917 Vitellaria paradoxa Species 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 229940057910 shea butter Drugs 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000003084 food emulsifier Nutrition 0.000 description 2
- 238000005227 gel permeation chromatography Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- FDCOHGHEADZEGF-QPLCGJKRSA-N 1,3-dipalmitoyl-2-oleoylglycerol Chemical group CCCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCC\C=C/CCCCCCCC FDCOHGHEADZEGF-QPLCGJKRSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 241000235395 Mucor Species 0.000 description 1
- 241000498617 Mucor javanicus Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 102000019280 Pancreatic lipases Human genes 0.000 description 1
- 108050006759 Pancreatic lipases Proteins 0.000 description 1
- 241000235527 Rhizopus Species 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- BAECOWNUKCLBPZ-HIUWNOOHSA-N Triolein Natural products O([C@H](OCC(=O)CCCCCCC/C=C\CCCCCCCC)COC(=O)CCCCCCC/C=C\CCCCCCCC)C(=O)CCCCCCC/C=C\CCCCCCCC BAECOWNUKCLBPZ-HIUWNOOHSA-N 0.000 description 1
- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 description 1
- 239000007983 Tris buffer Substances 0.000 description 1
- 241000179532 [Candida] cylindracea Species 0.000 description 1
- 239000008351 acetate buffer Substances 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 229940088598 enzyme Drugs 0.000 description 1
- 235000021323 fish oil Nutrition 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 230000003100 immobilizing effect Effects 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- -1 olive oil Chemical class 0.000 description 1
- 229940116369 pancreatic lipase Drugs 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000008363 phosphate buffer Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- 229940117972 triolein Drugs 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61072324A JPS62228289A (ja) | 1986-03-28 | 1986-03-28 | 油脂の加水分解方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61072324A JPS62228289A (ja) | 1986-03-28 | 1986-03-28 | 油脂の加水分解方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62228289A true JPS62228289A (ja) | 1987-10-07 |
| JPH0582196B2 JPH0582196B2 (enrdf_load_stackoverflow) | 1993-11-17 |
Family
ID=13485984
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61072324A Granted JPS62228289A (ja) | 1986-03-28 | 1986-03-28 | 油脂の加水分解方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62228289A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2648147A1 (fr) * | 1989-06-13 | 1990-12-14 | Gattefosse Ets Sa | Procede pour la preparation de beta-monoglycerides et produits obtenus |
| US5677160A (en) * | 1989-10-30 | 1997-10-14 | Henkel Corporation | Fat splitting process |
| US5830719A (en) * | 1995-05-31 | 1998-11-03 | Henkel Corporation | Process for continuously splitting a glyceride into carboxylic acids and glycerin |
-
1986
- 1986-03-28 JP JP61072324A patent/JPS62228289A/ja active Granted
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2648147A1 (fr) * | 1989-06-13 | 1990-12-14 | Gattefosse Ets Sa | Procede pour la preparation de beta-monoglycerides et produits obtenus |
| US5677160A (en) * | 1989-10-30 | 1997-10-14 | Henkel Corporation | Fat splitting process |
| US5830719A (en) * | 1995-05-31 | 1998-11-03 | Henkel Corporation | Process for continuously splitting a glyceride into carboxylic acids and glycerin |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0582196B2 (enrdf_load_stackoverflow) | 1993-11-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |