JPS6169754A - ペルフルオルヘキシルベンジルスルホン酸およびその塩 - Google Patents
ペルフルオルヘキシルベンジルスルホン酸およびその塩Info
- Publication number
- JPS6169754A JPS6169754A JP59193422A JP19342284A JPS6169754A JP S6169754 A JPS6169754 A JP S6169754A JP 59193422 A JP59193422 A JP 59193422A JP 19342284 A JP19342284 A JP 19342284A JP S6169754 A JPS6169754 A JP S6169754A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- water
- acid
- sulfuric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000003839 salts Chemical class 0.000 title claims abstract description 8
- VNYUOSLPHKNISN-UHFFFAOYSA-N FC(C1=C(C(=C(C(=C1F)F)F)F)F)(S(=O)(=O)O)C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F Chemical compound FC(C1=C(C(=C(C(=C1F)F)F)F)F)(S(=O)(=O)O)C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F VNYUOSLPHKNISN-UHFFFAOYSA-N 0.000 title 1
- 229910052751 metal Inorganic materials 0.000 claims abstract description 6
- 239000002184 metal Substances 0.000 claims abstract description 6
- 150000001412 amines Chemical class 0.000 claims abstract description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 abstract description 13
- 150000001875 compounds Chemical class 0.000 abstract description 10
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical compound FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract description 4
- -1 benzyl halide Chemical class 0.000 abstract description 3
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 2
- 230000002940 repellent Effects 0.000 abstract description 2
- 239000005871 repellent Substances 0.000 abstract description 2
- 238000006277 sulfonation reaction Methods 0.000 abstract description 2
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 abstract 1
- 238000010539 anionic addition polymerization reaction Methods 0.000 abstract 1
- 239000000539 dimer Substances 0.000 abstract 1
- 229910052731 fluorine Inorganic materials 0.000 abstract 1
- 239000011737 fluorine Substances 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000006082 mold release agent Substances 0.000 abstract 1
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Inorganic materials O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 abstract 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 9
- 239000002253 acid Substances 0.000 description 6
- 125000005010 perfluoroalkyl group Chemical group 0.000 description 5
- 125000003118 aryl group Chemical group 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical class FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 2
- 238000010189 synthetic method Methods 0.000 description 2
- NZEXBCLLEJJKOM-UHFFFAOYSA-N 1,1,1,5,5,5-hexafluoropentane Chemical compound FC(F)(F)CCCC(F)(F)F NZEXBCLLEJJKOM-UHFFFAOYSA-N 0.000 description 1
- NAOLWIGVYRIGTP-UHFFFAOYSA-N 1,3,5-trihydroxyanthracene-9,10-dione Chemical compound C1=CC(O)=C2C(=O)C3=CC(O)=CC(O)=C3C(=O)C2=C1 NAOLWIGVYRIGTP-UHFFFAOYSA-N 0.000 description 1
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- USSIQXCVUWKGNF-UHFFFAOYSA-N 6-(dimethylamino)-4,4-diphenylheptan-3-one Chemical class C=1C=CC=CC=1C(CC(C)N(C)C)(C(=O)CC)C1=CC=CC=C1 USSIQXCVUWKGNF-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- WBLIXGSTEMXDSM-UHFFFAOYSA-N chloromethane Chemical compound Cl[CH2] WBLIXGSTEMXDSM-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical compound COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000009902 electrolytic hydrogenation reaction Methods 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000006384 oligomerization reaction Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 125000005005 perfluorohexyl group Chemical group FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)* 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59193422A JPS6169754A (ja) | 1984-09-14 | 1984-09-14 | ペルフルオルヘキシルベンジルスルホン酸およびその塩 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59193422A JPS6169754A (ja) | 1984-09-14 | 1984-09-14 | ペルフルオルヘキシルベンジルスルホン酸およびその塩 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6169754A true JPS6169754A (ja) | 1986-04-10 |
| JPH0430942B2 JPH0430942B2 (enrdf_load_stackoverflow) | 1992-05-25 |
Family
ID=16307702
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59193422A Granted JPS6169754A (ja) | 1984-09-14 | 1984-09-14 | ペルフルオルヘキシルベンジルスルホン酸およびその塩 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6169754A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108690680A (zh) * | 2018-06-29 | 2018-10-23 | 佛山市高明区爪和新材料科技有限公司 | 一种脱模剂的制备方法 |
-
1984
- 1984-09-14 JP JP59193422A patent/JPS6169754A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108690680A (zh) * | 2018-06-29 | 2018-10-23 | 佛山市高明区爪和新材料科技有限公司 | 一种脱模剂的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0430942B2 (enrdf_load_stackoverflow) | 1992-05-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4383929A (en) | Fluorinated sulphobetaines and compositions containing the same | |
| US6268532B1 (en) | Sulfonated perfluorovinyl functional monomers | |
| US3419595A (en) | Fluorocarbon fluoroalkanesulfonates | |
| JPH04505916A (ja) | 脂肪アルキルスルフェートおよび脂肪アルキルポリアルキレングリコールエーテルスルフェート、それらの製法並びにそれらの用途 | |
| JPS6226264A (ja) | Ｎ−フルオロ−ｎ−ペルフルオロメチルスルホンアミド類 | |
| Vieira et al. | Fluorinated Ionic Liquids as Task-Specific Materials: An | |
| JPS6169754A (ja) | ペルフルオルヘキシルベンジルスルホン酸およびその塩 | |
| JPH0321015B2 (enrdf_load_stackoverflow) | ||
| DE2362648A1 (de) | Verfahren zur herstellung von halogenphenolen | |
| JPS6228169B2 (enrdf_load_stackoverflow) | ||
| US2098114A (en) | Process for sulphonating alcohols | |
| Rosen et al. | The relationship of structure to properties in surfactants: V. Synthesis and properties of α, ω-bis (sodium p-sulfophenoxy) alkanes | |
| JPH0449534B2 (enrdf_load_stackoverflow) | ||
| KR920012101A (ko) | 수용성 디포스핀의 제조방법 | |
| US3763207A (en) | Perfluorocyclic carbinol sulfate salts | |
| CN104906996B (zh) | 一种磺酸盐型含氟表面活性剂、其合成方法及应用 | |
| DE1668252C3 (de) | Fluorierte Sulfonsäure und deren Salze sowie Verfahren zu deren Herstellung | |
| US2293265A (en) | Surface active agent | |
| US2213588A (en) | Detergent aid | |
| KR960010671A (ko) | 5h- 페닐-3,13- 디설포네이토디벤조포스폴 및 이의 제조방법 | |
| US3328454A (en) | Polyhalobenzyloxyalkanol sulfates | |
| US3201461A (en) | Alkylhalonaphthalene sulfonates | |
| DE852998C (de) | Verfahren zur Herstellung von Sulfonsaeureestern | |
| Wayne | The nitration of carbamates using boron tifluoride as a dehydrating agent | |
| DE913771C (de) | Verfahren zur Herstellung von 2-Chloranthrachinon-3,5,7- und 2-Chloranthrachinon-3,6,8-trisulfonsaeure |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |