JPS6151012A - プレポリマ−の製造方法 - Google Patents
プレポリマ−の製造方法Info
- Publication number
- JPS6151012A JPS6151012A JP17235584A JP17235584A JPS6151012A JP S6151012 A JPS6151012 A JP S6151012A JP 17235584 A JP17235584 A JP 17235584A JP 17235584 A JP17235584 A JP 17235584A JP S6151012 A JPS6151012 A JP S6151012A
- Authority
- JP
- Japan
- Prior art keywords
- tertiary
- polymerization
- temperature
- initial polymerization
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 238000006116 polymerization reaction Methods 0.000 claims abstract description 57
- 239000003505 polymerization initiator Substances 0.000 claims abstract description 17
- 150000002978 peroxides Chemical class 0.000 claims abstract description 16
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 7
- SYFOAKAXGNMQAX-UHFFFAOYSA-N bis(prop-2-enyl) carbonate;2-(2-hydroxyethoxy)ethanol Chemical compound OCCOCCO.C=CCOC(=O)OCC=C SYFOAKAXGNMQAX-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims description 22
- -1 butyl peroxy Chemical group 0.000 claims description 16
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- IOYVRBJBKRRYGY-UHFFFAOYSA-N hexyl 3,3-dimethylbutaneperoxoate Chemical group CCCCCCOOC(=O)CC(C)(C)C IOYVRBJBKRRYGY-UHFFFAOYSA-N 0.000 claims description 2
- ZLAJWQIJAVXCAT-UHFFFAOYSA-N pentyl 7,7-dimethyloctaneperoxoate Chemical group CCCCCOOC(=O)CCCCCC(C)(C)C ZLAJWQIJAVXCAT-UHFFFAOYSA-N 0.000 claims description 2
- OEPDDHXBGNWCHS-UHFFFAOYSA-N 2,2-dimethyloctaneperoxoic acid Chemical group CCCCCCC(C)(C)C(=O)OO OEPDDHXBGNWCHS-UHFFFAOYSA-N 0.000 claims 1
- HEEKCUUSDRHGAC-UHFFFAOYSA-N 7,7-dimethyl-2-(2,4,4-trimethylpentyl)octaneperoxoic acid Chemical compound CC(C)(C)CC(C)CC(C(=O)OO)CCCCC(C)(C)C HEEKCUUSDRHGAC-UHFFFAOYSA-N 0.000 claims 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 238000003860 storage Methods 0.000 abstract description 7
- 239000000203 mixture Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- 230000000379 polymerizing effect Effects 0.000 abstract 1
- OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000001879 gelation Methods 0.000 description 11
- 229920000642 polymer Polymers 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 10
- NUHSROFQTUXZQQ-UHFFFAOYSA-N isopentenyl diphosphate Chemical compound CC(=C)CCO[P@](O)(=O)OP(O)(O)=O NUHSROFQTUXZQQ-UHFFFAOYSA-N 0.000 description 9
- 238000007796 conventional method Methods 0.000 description 5
- 239000013256 coordination polymer Substances 0.000 description 4
- MBOQKJVESPQPMS-UHFFFAOYSA-N hexyl 7,7-dimethyloctaneperoxoate Chemical group CCCCCCOOC(=O)CCCCCC(C)(C)C MBOQKJVESPQPMS-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229950010765 pivalate Drugs 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- BWJUFXUULUEGMA-UHFFFAOYSA-N propan-2-yl propan-2-yloxycarbonyloxy carbonate Chemical compound CC(C)OC(=O)OOC(=O)OC(C)C BWJUFXUULUEGMA-UHFFFAOYSA-N 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- BEQKKZICTDFVMG-UHFFFAOYSA-N 1,2,3,4,6-pentaoxepane-5,7-dione Chemical compound O=C1OOOOC(=O)O1 BEQKKZICTDFVMG-UHFFFAOYSA-N 0.000 description 1
- VDHJESBEVUVUHB-UHFFFAOYSA-N 2,2-dimethylnonaneperoxoic acid Chemical compound CCCCCCCC(C)(C)C(=O)OO VDHJESBEVUVUHB-UHFFFAOYSA-N 0.000 description 1
- SXAMGRAIZSSWIH-UHFFFAOYSA-N 2-[3-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,2,4-oxadiazol-5-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NOC(=N1)CC(=O)N1CC2=C(CC1)NN=N2 SXAMGRAIZSSWIH-UHFFFAOYSA-N 0.000 description 1
- YJLUBHOZZTYQIP-UHFFFAOYSA-N 2-[5-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,3,4-oxadiazol-2-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NN=C(O1)CC(=O)N1CC2=C(CC1)NN=N2 YJLUBHOZZTYQIP-UHFFFAOYSA-N 0.000 description 1
- OSIXWYRQOMVKMH-UHFFFAOYSA-N CCCCCC(C)(C(=O)OO)C(C)(C)C Chemical compound CCCCCC(C)(C(=O)OO)C(C)(C)C OSIXWYRQOMVKMH-UHFFFAOYSA-N 0.000 description 1
- DDMBAIHCDCYZAG-UHFFFAOYSA-N butyl 7,7-dimethyloctaneperoxoate Chemical group CCCCOOC(=O)CCCCCC(C)(C)C DDMBAIHCDCYZAG-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17235584A JPS6151012A (ja) | 1984-08-21 | 1984-08-21 | プレポリマ−の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17235584A JPS6151012A (ja) | 1984-08-21 | 1984-08-21 | プレポリマ−の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6151012A true JPS6151012A (ja) | 1986-03-13 |
| JPH0529644B2 JPH0529644B2 (enrdf_load_html_response) | 1993-05-06 |
Family
ID=15940361
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP17235584A Granted JPS6151012A (ja) | 1984-08-21 | 1984-08-21 | プレポリマ−の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6151012A (enrdf_load_html_response) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03219013A (ja) * | 1989-08-22 | 1991-09-26 | Acos Especiais Itabira Acesita:Co | フェライト・ステンレス鋼の製造方法および製造装置 |
| US5952441A (en) * | 1997-12-30 | 1999-09-14 | Ppg Industries Ohio, Inc. | Partially polymerized mixture of diethylene glycol (allyl carbonate) compounds |
| US6057411A (en) * | 1997-12-30 | 2000-05-02 | Ppg Industries Ohio, Inc. | Process for forming poly(allyl carbonate)-functional prepolymer composition |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58167124A (ja) * | 1982-03-29 | 1983-10-03 | Nippon Oil & Fats Co Ltd | プラスチツクレンズの製造法 |
| JPS60124604A (ja) * | 1983-11-09 | 1985-07-03 | ピ−ピ−ジ− インダストリ−ズ インコ−ポレ−テツド | 部分重合したジエチレングリコールビス（アリルカルボナート）単量体の重合性液状組成物の製造法 |
-
1984
- 1984-08-21 JP JP17235584A patent/JPS6151012A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58167124A (ja) * | 1982-03-29 | 1983-10-03 | Nippon Oil & Fats Co Ltd | プラスチツクレンズの製造法 |
| JPS60124604A (ja) * | 1983-11-09 | 1985-07-03 | ピ−ピ−ジ− インダストリ−ズ インコ−ポレ−テツド | 部分重合したジエチレングリコールビス（アリルカルボナート）単量体の重合性液状組成物の製造法 |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03219013A (ja) * | 1989-08-22 | 1991-09-26 | Acos Especiais Itabira Acesita:Co | フェライト・ステンレス鋼の製造方法および製造装置 |
| US5952441A (en) * | 1997-12-30 | 1999-09-14 | Ppg Industries Ohio, Inc. | Partially polymerized mixture of diethylene glycol (allyl carbonate) compounds |
| US6057411A (en) * | 1997-12-30 | 2000-05-02 | Ppg Industries Ohio, Inc. | Process for forming poly(allyl carbonate)-functional prepolymer composition |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0529644B2 (enrdf_load_html_response) | 1993-05-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |