JPS61256914A - 高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法 - Google Patents
高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法Info
- Publication number
- JPS61256914A JPS61256914A JP9419985A JP9419985A JPS61256914A JP S61256914 A JPS61256914 A JP S61256914A JP 9419985 A JP9419985 A JP 9419985A JP 9419985 A JP9419985 A JP 9419985A JP S61256914 A JPS61256914 A JP S61256914A
- Authority
- JP
- Japan
- Prior art keywords
- reaction mixture
- silica sol
- ratio
- silica
- type zeolite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title claims abstract description 68
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 67
- 239000010457 zeolite Substances 0.000 title claims abstract description 65
- 229910021536 Zeolite Inorganic materials 0.000 title claims abstract description 63
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 30
- 229910000323 aluminium silicate Inorganic materials 0.000 title claims abstract description 5
- 239000011541 reaction mixture Substances 0.000 claims abstract description 61
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000000203 mixture Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 10
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 10
- 239000002245 particle Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000008119 colloidal silica Substances 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 abstract description 10
- 229910052681 coesite Inorganic materials 0.000 abstract 7
- 229910052906 cristobalite Inorganic materials 0.000 abstract 7
- 229910052682 stishovite Inorganic materials 0.000 abstract 7
- 229910052905 tridymite Inorganic materials 0.000 abstract 7
- 229910052593 corundum Inorganic materials 0.000 abstract 4
- 229910001845 yogo sapphire Inorganic materials 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 19
- 239000000047 product Substances 0.000 description 16
- 238000003756 stirring Methods 0.000 description 10
- 239000000126 substance Substances 0.000 description 8
- 238000004458 analytical method Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 230000032683 aging Effects 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 4
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 4
- 229910001388 sodium aluminate Inorganic materials 0.000 description 4
- 150000001768 cations Chemical class 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 239000007790 solid phase Substances 0.000 description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000002050 diffraction method Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- 238000010420 art technique Methods 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 description 1
- 229910001683 gmelinite Inorganic materials 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9419985A JPS61256914A (ja) | 1985-05-01 | 1985-05-01 | 高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9419985A JPS61256914A (ja) | 1985-05-01 | 1985-05-01 | 高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61256914A true JPS61256914A (ja) | 1986-11-14 |
| JPH0568410B2 JPH0568410B2 (enrdf_load_stackoverflow) | 1993-09-28 |
Family
ID=14103625
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9419985A Granted JPS61256914A (ja) | 1985-05-01 | 1985-05-01 | 高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61256914A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001525781A (ja) * | 1996-07-31 | 2001-12-11 | シェブロン ユー．エス．エー．インコーポレイテッド | 有機テンプレートを用いたｙ型ホージャサイトの製造 |
-
1985
- 1985-05-01 JP JP9419985A patent/JPS61256914A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001525781A (ja) * | 1996-07-31 | 2001-12-11 | シェブロン ユー．エス．エー．インコーポレイテッド | 有機テンプレートを用いたｙ型ホージャサイトの製造 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0568410B2 (enrdf_load_stackoverflow) | 1993-09-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4304686A (en) | Method of preparing improved catalysts | |
| CN105967205A (zh) | 沸石的制造方法 | |
| JPH0574527B2 (enrdf_load_stackoverflow) | ||
| JP2018162206A (ja) | テンプレートである１，６−ビス（メチルピペリジニウム）ヘキサンジブロミドの存在下でのｉｚｍ−２ゼオライトの合成方法 | |
| US5338525A (en) | MFI-type zeolite and its preparation process | |
| US7449168B2 (en) | Process for making a germanium-zeolite | |
| AU696871B2 (en) | Large crystal ZSM-5, its synthesis and use | |
| JPS5939717A (ja) | ゼオライトの製造法 | |
| JP2001058816A (ja) | ＮａＹ型ゼオライト | |
| US11472711B2 (en) | Process for preparing an IZM-2 zeolite in the presence of a mixture of nitrogenous organic structuring agents in hydroxide form and of bromide and of an alkali metal chloride | |
| JPH0154285B2 (enrdf_load_stackoverflow) | ||
| JPH0228523B2 (enrdf_load_stackoverflow) | ||
| EP1587756A1 (en) | Method of preparing zsm-5 using variable temperature without organic template | |
| JPS61256914A (ja) | 高ケイ酸質ｙ型結晶性アルミノシリケ−トゼオライトの製造方法 | |
| US5215736A (en) | Mordenite type zeolite and its preparation process | |
| JPS6243927B2 (enrdf_load_stackoverflow) | ||
| JP3299932B2 (ja) | ゼオライトｌの調製方法 | |
| US5756064A (en) | Siliceous offretite | |
| JP2553609B2 (ja) | ゼオライトｚｓｍ−５の合成法 | |
| JPH08188414A (ja) | 高耐熱性フェリエライト型ゼオライトおよびその製造方法 | |
| JPS6228086B2 (enrdf_load_stackoverflow) | ||
| JPH0339972B2 (enrdf_load_stackoverflow) | ||
| JPS59190928A (ja) | トルエンの不均化法 | |
| JPH11130424A (ja) | 結晶性アルミノ珪酸塩の製造方法 | |
| JPS6323126B2 (enrdf_load_stackoverflow) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |