JPS6119707A - 高反応性亜鉛粉末の製造方法 - Google Patents
高反応性亜鉛粉末の製造方法Info
- Publication number
- JPS6119707A JPS6119707A JP59139410A JP13941084A JPS6119707A JP S6119707 A JPS6119707 A JP S6119707A JP 59139410 A JP59139410 A JP 59139410A JP 13941084 A JP13941084 A JP 13941084A JP S6119707 A JPS6119707 A JP S6119707A
- Authority
- JP
- Japan
- Prior art keywords
- metal
- dioxane
- highly reactive
- metal powder
- reactive metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 31
- 239000002184 metal Substances 0.000 title claims abstract description 31
- 239000000843 powder Substances 0.000 title claims abstract description 22
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims abstract description 16
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 229910001507 metal halide Inorganic materials 0.000 claims abstract description 9
- 150000005309 metal halides Chemical class 0.000 claims abstract description 9
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 125000005843 halogen group Chemical group 0.000 claims abstract description 4
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 3
- 239000011701 zinc Substances 0.000 claims abstract description 3
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 14
- 238000010438 heat treatment Methods 0.000 abstract description 12
- 238000003756 stirring Methods 0.000 abstract description 12
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract description 11
- 239000002904 solvent Substances 0.000 abstract description 7
- 239000011592 zinc chloride Substances 0.000 abstract description 6
- 235000005074 zinc chloride Nutrition 0.000 abstract description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 4
- 229910052717 sulfur Inorganic materials 0.000 abstract description 4
- 239000011593 sulfur Substances 0.000 abstract description 4
- 230000035484 reaction time Effects 0.000 abstract description 3
- 238000005695 dehalogenation reaction Methods 0.000 abstract description 2
- 230000018044 dehydration Effects 0.000 abstract description 2
- 238000006297 dehydration reaction Methods 0.000 abstract description 2
- 238000010992 reflux Methods 0.000 abstract description 2
- OIXUJRCCNNHWFI-UHFFFAOYSA-N 1,2-dioxane Chemical compound C1CCOOC1 OIXUJRCCNNHWFI-UHFFFAOYSA-N 0.000 abstract 1
- VDFVNEFVBPFDSB-UHFFFAOYSA-N 1,3-dioxane Chemical compound C1COCOC1 VDFVNEFVBPFDSB-UHFFFAOYSA-N 0.000 abstract 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 150000001491 aromatic compounds Chemical class 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- UEXCJVNBTNXOEH-UHFFFAOYSA-N Ethynylbenzene Chemical group C#CC1=CC=CC=C1 UEXCJVNBTNXOEH-UHFFFAOYSA-N 0.000 description 4
- 238000007792 addition Methods 0.000 description 4
- 125000004429 atom Chemical group 0.000 description 4
- 230000003197 catalytic effect Effects 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 238000004817 gas chromatography Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- ODRZAZBEQWAOGU-UHFFFAOYSA-N 1,4-dioxin-2-one Chemical compound O=C1COC=CO1 ODRZAZBEQWAOGU-UHFFFAOYSA-N 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 229910001111 Fine metal Inorganic materials 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- DHXVGJBLRPWPCS-UHFFFAOYSA-N Tetrahydropyran Chemical compound C1CCOCC1 DHXVGJBLRPWPCS-UHFFFAOYSA-N 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000005909 ethyl alcohol group Chemical group 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- NGKSKVYWPINGLI-UHFFFAOYSA-N prop-2-ynylbenzene Chemical group C#CCC1=CC=CC=C1 NGKSKVYWPINGLI-UHFFFAOYSA-N 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59139410A JPS6119707A (ja) | 1984-07-05 | 1984-07-05 | 高反応性亜鉛粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59139410A JPS6119707A (ja) | 1984-07-05 | 1984-07-05 | 高反応性亜鉛粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6119707A true JPS6119707A (ja) | 1986-01-28 |
| JPS622001B2 JPS622001B2 (enrdf_load_stackoverflow) | 1987-01-17 |
Family
ID=15244592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59139410A Granted JPS6119707A (ja) | 1984-07-05 | 1984-07-05 | 高反応性亜鉛粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6119707A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5358546A (en) * | 1992-02-04 | 1994-10-25 | Board Of Regents Of The University Of Nebraska | Highly reactive forms of zinc and reagents thereof |
| US5507973A (en) * | 1991-04-26 | 1996-04-16 | Board Of Regents Of The University Of Nebraska | Highly reactive zerovalent metals from metal cyanides |
| US5756653A (en) * | 1992-02-04 | 1998-05-26 | Board Of Regents Of The University Of Nebraska | Substituted polythiophenes from highly reactive zinc reagents |
| KR100607027B1 (ko) * | 2002-10-14 | 2006-07-31 | 주식회사 엘지생명과학 | 아연 금속의 새로운 활성화 방법 |
-
1984
- 1984-07-05 JP JP59139410A patent/JPS6119707A/ja active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5507973A (en) * | 1991-04-26 | 1996-04-16 | Board Of Regents Of The University Of Nebraska | Highly reactive zerovalent metals from metal cyanides |
| US5358546A (en) * | 1992-02-04 | 1994-10-25 | Board Of Regents Of The University Of Nebraska | Highly reactive forms of zinc and reagents thereof |
| US5756653A (en) * | 1992-02-04 | 1998-05-26 | Board Of Regents Of The University Of Nebraska | Substituted polythiophenes from highly reactive zinc reagents |
| US5964919A (en) * | 1992-02-04 | 1999-10-12 | Board Of Regents Of The University Of Nebraska | Method of storing active zero valent zinc metal |
| KR100607027B1 (ko) * | 2002-10-14 | 2006-07-31 | 주식회사 엘지생명과학 | 아연 금속의 새로운 활성화 방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS622001B2 (enrdf_load_stackoverflow) | 1987-01-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |