JPS61132519A - 微粒状酸化ビスマスの製造方法 - Google Patents
微粒状酸化ビスマスの製造方法Info
- Publication number
- JPS61132519A JPS61132519A JP25201484A JP25201484A JPS61132519A JP S61132519 A JPS61132519 A JP S61132519A JP 25201484 A JP25201484 A JP 25201484A JP 25201484 A JP25201484 A JP 25201484A JP S61132519 A JPS61132519 A JP S61132519A
- Authority
- JP
- Japan
- Prior art keywords
- bismuth
- precipitate
- aqueous solution
- bismuth oxide
- fine powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910000416 bismuth oxide Inorganic materials 0.000 title claims description 17
- TYIXMATWDRGMPF-UHFFFAOYSA-N dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Bi+3].[Bi+3] TYIXMATWDRGMPF-UHFFFAOYSA-N 0.000 title claims description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 239000000843 powder Substances 0.000 title abstract 3
- 239000002244 precipitate Substances 0.000 claims abstract description 20
- 239000003513 alkali Substances 0.000 claims abstract description 14
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims abstract description 6
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 6
- 238000001354 calcination Methods 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims description 17
- RXPAJWPEYBDXOG-UHFFFAOYSA-N hydron;methyl 4-methoxypyridine-2-carboxylate;chloride Chemical compound Cl.COC(=O)C1=CC(OC)=CC=N1 RXPAJWPEYBDXOG-UHFFFAOYSA-N 0.000 claims description 9
- 238000000967 suction filtration Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 abstract description 17
- 239000007864 aqueous solution Substances 0.000 abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 8
- 239000000243 solution Substances 0.000 abstract description 5
- WMWLMWRWZQELOS-UHFFFAOYSA-N bismuth(iii) oxide Chemical compound O=[Bi]O[Bi]=O WMWLMWRWZQELOS-UHFFFAOYSA-N 0.000 abstract 4
- 238000013019 agitation Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 229910052797 bismuth Inorganic materials 0.000 description 10
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 8
- 229910000014 Bismuth subcarbonate Inorganic materials 0.000 description 4
- MGLUJXPJRXTKJM-UHFFFAOYSA-L bismuth subcarbonate Chemical compound O=[Bi]OC(=O)O[Bi]=O MGLUJXPJRXTKJM-UHFFFAOYSA-L 0.000 description 4
- 229940036358 bismuth subcarbonate Drugs 0.000 description 4
- 238000010304 firing Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 description 4
- 239000010419 fine particle Substances 0.000 description 3
- 229910002651 NO3 Inorganic materials 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000011362 coarse particle Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 241000272814 Anser sp. Species 0.000 description 1
- HWSISDHAHRVNMT-UHFFFAOYSA-N Bismuth subnitrate Chemical compound O[NH+]([O-])O[Bi](O[N+]([O-])=O)O[N+]([O-])=O HWSISDHAHRVNMT-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 241001442654 Percnon planissimum Species 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 229940049676 bismuth hydroxide Drugs 0.000 description 1
- 229960001482 bismuth subnitrate Drugs 0.000 description 1
- XAEZALCLBRUCLR-UHFFFAOYSA-K bismuth;hydrogen carbonate Chemical compound [Bi+3].OC([O-])=O.OC([O-])=O.OC([O-])=O XAEZALCLBRUCLR-UHFFFAOYSA-K 0.000 description 1
- TZSXPYWRDWEXHG-UHFFFAOYSA-K bismuth;trihydroxide Chemical compound [OH-].[OH-].[OH-].[Bi+3] TZSXPYWRDWEXHG-UHFFFAOYSA-K 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25201484A JPS61132519A (ja) | 1984-11-30 | 1984-11-30 | 微粒状酸化ビスマスの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25201484A JPS61132519A (ja) | 1984-11-30 | 1984-11-30 | 微粒状酸化ビスマスの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61132519A true JPS61132519A (ja) | 1986-06-20 |
| JPH0526725B2 JPH0526725B2 (enrdf_load_stackoverflow) | 1993-04-19 |
Family
ID=17231371
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP25201484A Granted JPS61132519A (ja) | 1984-11-30 | 1984-11-30 | 微粒状酸化ビスマスの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61132519A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH111322A (ja) * | 1997-06-10 | 1999-01-06 | Dowa Mining Co Ltd | 酸化ビスマス粉およびその製造方法 |
| WO2013191075A1 (ja) * | 2012-06-21 | 2013-12-27 | 東亞合成株式会社 | 非晶質無機陰イオン交換体、電子部品封止用樹脂組成物および非晶質ビスマス化合物の製造方法 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5327848B2 (ja) * | 2008-10-09 | 2013-10-30 | テイカ株式会社 | 紫外線遮蔽用分散体および紫外線遮蔽用コーティング組成物 |
| JP5205204B2 (ja) * | 2008-10-09 | 2013-06-05 | テイカ株式会社 | 単斜晶系微粒子酸化ビスマスの製造方法、紫外線遮蔽用分散体およびその製造方法、ならびに紫外線遮蔽用コーティング組成物 |
| CN103253704B (zh) * | 2013-04-12 | 2015-02-04 | 武汉理工大学 | 半导体多孔氧化铋纳米球及其制备方法和应用 |
-
1984
- 1984-11-30 JP JP25201484A patent/JPS61132519A/ja active Granted
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH111322A (ja) * | 1997-06-10 | 1999-01-06 | Dowa Mining Co Ltd | 酸化ビスマス粉およびその製造方法 |
| WO2013191075A1 (ja) * | 2012-06-21 | 2013-12-27 | 東亞合成株式会社 | 非晶質無機陰イオン交換体、電子部品封止用樹脂組成物および非晶質ビスマス化合物の製造方法 |
| JPWO2013191075A1 (ja) * | 2012-06-21 | 2016-05-26 | 東亞合成株式会社 | 非晶質無機陰イオン交換体、電子部品封止用樹脂組成物および非晶質ビスマス化合物の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0526725B2 (enrdf_load_stackoverflow) | 1993-04-19 |
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