JPS61103962A - ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法 - Google Patents
ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法Info
- Publication number
- JPS61103962A JPS61103962A JP60236549A JP23654985A JPS61103962A JP S61103962 A JPS61103962 A JP S61103962A JP 60236549 A JP60236549 A JP 60236549A JP 23654985 A JP23654985 A JP 23654985A JP S61103962 A JPS61103962 A JP S61103962A
- Authority
- JP
- Japan
- Prior art keywords
- ammonium polyphosphate
- water
- resin
- weight
- melamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003063 flame retardant Substances 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 229920000388 Polyphosphate Polymers 0.000 title 1
- 230000007062 hydrolysis Effects 0.000 title 1
- 238000006460 hydrolysis reaction Methods 0.000 title 1
- 239000001205 polyphosphate Substances 0.000 title 1
- 235000011176 polyphosphates Nutrition 0.000 title 1
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims description 57
- 229920001276 ammonium polyphosphate Polymers 0.000 claims description 57
- 239000004114 Ammonium polyphosphate Substances 0.000 claims description 53
- 229920005989 resin Polymers 0.000 claims description 42
- 239000011347 resin Substances 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 239000000725 suspension Substances 0.000 claims description 18
- 239000000375 suspending agent Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 13
- 230000035484 reaction time Effects 0.000 claims description 12
- JMHCCAYJTTWMCX-QWPJCUCISA-M sodium;(2s)-2-amino-3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoate;pentahydrate Chemical compound O.O.O.O.O.[Na+].IC1=CC(C[C@H](N)C([O-])=O)=CC(I)=C1OC1=CC(I)=C(O)C(I)=C1 JMHCCAYJTTWMCX-QWPJCUCISA-M 0.000 claims description 12
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- -1 at room temperature Substances 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 229920003002 synthetic resin Polymers 0.000 claims description 3
- 239000000057 synthetic resin Substances 0.000 claims description 3
- 229920001187 thermosetting polymer Polymers 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 2
- 239000011541 reaction mixture Substances 0.000 claims description 2
- 230000009969 flowable effect Effects 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 33
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 22
- 239000000047 product Substances 0.000 description 22
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000004848 polyfunctional curative Substances 0.000 description 12
- 238000005259 measurement Methods 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000012065 filter cake Substances 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000004254 Ammonium phosphate Substances 0.000 description 5
- 229920000877 Melamine resin Polymers 0.000 description 5
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 5
- 235000019289 ammonium phosphates Nutrition 0.000 description 5
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 5
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical compound O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000003301 hydrolyzing effect Effects 0.000 description 3
- GUSFEBGYPWJUSS-UHFFFAOYSA-N pentaazanium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [NH4+].[NH4+].[NH4+].[NH4+].[NH4+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O GUSFEBGYPWJUSS-UHFFFAOYSA-N 0.000 description 3
- 229920005830 Polyurethane Foam Polymers 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 229920002635 polyurethane Polymers 0.000 description 2
- 239000011496 polyurethane foam Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000005029 sieve analysis Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000283690 Bos taurus Species 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- VKFFEYLSKIYTSJ-UHFFFAOYSA-N tetraazanium;phosphonato phosphate Chemical compound [NH4+].[NH4+].[NH4+].[NH4+].[O-]P([O-])(=O)OP([O-])([O-])=O VKFFEYLSKIYTSJ-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229920006186 water-soluble synthetic resin Polymers 0.000 description 1
- 239000012866 water-soluble synthetic resin Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Fireproofing Substances (AREA)
- Polyurethanes Or Polyureas (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3439233.5 | 1984-10-26 | ||
| DE3439233 | 1984-10-26 | ||
| DE3531500.8 | 1985-09-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61103962A true JPS61103962A (ja) | 1986-05-22 |
| JPH0455625B2 JPH0455625B2 (enExample) | 1992-09-03 |
Family
ID=6248821
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60236549A Granted JPS61103962A (ja) | 1984-10-26 | 1985-10-24 | ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法 |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JPS61103962A (enExample) |
| DD (1) | DD239215A5 (enExample) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01198685A (ja) * | 1987-10-28 | 1989-08-10 | Dainippon Ink & Chem Inc | 木材用難燃剤及び難燃木材 |
| WO1995018177A1 (en) | 1993-12-28 | 1995-07-06 | Chisso Corporation | Flame-retardant thermoplastic polymer composition, water-insoluble ammonium polyphosphate powder as the component thereof, and process for producing the same |
| EP0659819B1 (en) * | 1993-12-27 | 1999-08-11 | Chisso Corporation | Flame-retardant thermosetting resin composition |
| JP2009001435A (ja) * | 2007-06-19 | 2009-01-08 | Shin Etsu Chem Co Ltd | ポリリン酸アンモニウムの改質方法 |
| US7695651B2 (en) | 2004-02-16 | 2010-04-13 | Shin-Etsu Chemical Co., Ltd. | Flame retardant additives, emulsion type coating compositions, and flame retardant compositions |
-
1985
- 1985-10-22 DD DD85281964A patent/DD239215A5/de not_active IP Right Cessation
- 1985-10-24 JP JP60236549A patent/JPS61103962A/ja active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01198685A (ja) * | 1987-10-28 | 1989-08-10 | Dainippon Ink & Chem Inc | 木材用難燃剤及び難燃木材 |
| EP0659819B1 (en) * | 1993-12-27 | 1999-08-11 | Chisso Corporation | Flame-retardant thermosetting resin composition |
| WO1995018177A1 (en) | 1993-12-28 | 1995-07-06 | Chisso Corporation | Flame-retardant thermoplastic polymer composition, water-insoluble ammonium polyphosphate powder as the component thereof, and process for producing the same |
| US7695651B2 (en) | 2004-02-16 | 2010-04-13 | Shin-Etsu Chemical Co., Ltd. | Flame retardant additives, emulsion type coating compositions, and flame retardant compositions |
| JP2009001435A (ja) * | 2007-06-19 | 2009-01-08 | Shin Etsu Chem Co Ltd | ポリリン酸アンモニウムの改質方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DD239215A5 (de) | 1986-09-17 |
| JPH0455625B2 (enExample) | 1992-09-03 |
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