JPS61103962A - ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法 - Google Patents
ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法Info
- Publication number
- JPS61103962A JPS61103962A JP60236549A JP23654985A JPS61103962A JP S61103962 A JPS61103962 A JP S61103962A JP 60236549 A JP60236549 A JP 60236549A JP 23654985 A JP23654985 A JP 23654985A JP S61103962 A JPS61103962 A JP S61103962A
- Authority
- JP
- Japan
- Prior art keywords
- ammonium polyphosphate
- water
- resin
- weight
- melamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003063 flame retardant Substances 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 229920000388 Polyphosphate Polymers 0.000 title 1
- 230000007062 hydrolysis Effects 0.000 title 1
- 238000006460 hydrolysis reaction Methods 0.000 title 1
- 239000001205 polyphosphate Substances 0.000 title 1
- 235000011176 polyphosphates Nutrition 0.000 title 1
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims description 57
- 229920001276 ammonium polyphosphate Polymers 0.000 claims description 57
- 239000004114 Ammonium polyphosphate Substances 0.000 claims description 53
- 229920005989 resin Polymers 0.000 claims description 42
- 239000011347 resin Substances 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 239000000725 suspension Substances 0.000 claims description 18
- 239000000375 suspending agent Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 13
- 230000035484 reaction time Effects 0.000 claims description 12
- JMHCCAYJTTWMCX-QWPJCUCISA-M sodium;(2s)-2-amino-3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoate;pentahydrate Chemical compound O.O.O.O.O.[Na+].IC1=CC(C[C@H](N)C([O-])=O)=CC(I)=C1OC1=CC(I)=C(O)C(I)=C1 JMHCCAYJTTWMCX-QWPJCUCISA-M 0.000 claims description 12
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- -1 at room temperature Substances 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 229920003002 synthetic resin Polymers 0.000 claims description 3
- 239000000057 synthetic resin Substances 0.000 claims description 3
- 229920001187 thermosetting polymer Polymers 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 2
- 239000011541 reaction mixture Substances 0.000 claims description 2
- 230000009969 flowable effect Effects 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 33
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 22
- 239000000047 product Substances 0.000 description 22
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000004848 polyfunctional curative Substances 0.000 description 12
- 238000005259 measurement Methods 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000012065 filter cake Substances 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000004254 Ammonium phosphate Substances 0.000 description 5
- 229920000877 Melamine resin Polymers 0.000 description 5
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 5
- 235000019289 ammonium phosphates Nutrition 0.000 description 5
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 5
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical compound O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000003301 hydrolyzing effect Effects 0.000 description 3
- GUSFEBGYPWJUSS-UHFFFAOYSA-N pentaazanium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [NH4+].[NH4+].[NH4+].[NH4+].[NH4+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O GUSFEBGYPWJUSS-UHFFFAOYSA-N 0.000 description 3
- 229920005830 Polyurethane Foam Polymers 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 229920002635 polyurethane Polymers 0.000 description 2
- 239000011496 polyurethane foam Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000005029 sieve analysis Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000283690 Bos taurus Species 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- VKFFEYLSKIYTSJ-UHFFFAOYSA-N tetraazanium;phosphonato phosphate Chemical compound [NH4+].[NH4+].[NH4+].[NH4+].[O-]P([O-])(=O)OP([O-])([O-])=O VKFFEYLSKIYTSJ-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229920006186 water-soluble synthetic resin Polymers 0.000 description 1
- 239000012866 water-soluble synthetic resin Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Fireproofing Substances (AREA)
- Polyurethanes Or Polyureas (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3439233 | 1984-10-26 | ||
| DE3439233.5 | 1984-10-26 | ||
| DE3531500.8 | 1985-09-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61103962A true JPS61103962A (ja) | 1986-05-22 |
| JPH0455625B2 JPH0455625B2 (enrdf_load_stackoverflow) | 1992-09-03 |
Family
ID=6248821
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60236549A Granted JPS61103962A (ja) | 1984-10-26 | 1985-10-24 | ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法 |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JPS61103962A (enrdf_load_stackoverflow) |
| DD (1) | DD239215A5 (enrdf_load_stackoverflow) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01198685A (ja) * | 1987-10-28 | 1989-08-10 | Dainippon Ink & Chem Inc | 木材用難燃剤及び難燃木材 |
| WO1995018177A1 (fr) | 1993-12-28 | 1995-07-06 | Chisso Corporation | Composition polymere thermoplastiques ignifuge, poudre de polyphosphate d'ammonium non hydrosoluble a constituant, et son procede de production |
| EP0659819B1 (en) * | 1993-12-27 | 1999-08-11 | Chisso Corporation | Flame-retardant thermosetting resin composition |
| JP2009001435A (ja) * | 2007-06-19 | 2009-01-08 | Shin Etsu Chem Co Ltd | ポリリン酸アンモニウムの改質方法 |
| US7695651B2 (en) | 2004-02-16 | 2010-04-13 | Shin-Etsu Chemical Co., Ltd. | Flame retardant additives, emulsion type coating compositions, and flame retardant compositions |
-
1985
- 1985-10-22 DD DD85281964A patent/DD239215A5/de not_active IP Right Cessation
- 1985-10-24 JP JP60236549A patent/JPS61103962A/ja active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01198685A (ja) * | 1987-10-28 | 1989-08-10 | Dainippon Ink & Chem Inc | 木材用難燃剤及び難燃木材 |
| EP0659819B1 (en) * | 1993-12-27 | 1999-08-11 | Chisso Corporation | Flame-retardant thermosetting resin composition |
| WO1995018177A1 (fr) | 1993-12-28 | 1995-07-06 | Chisso Corporation | Composition polymere thermoplastiques ignifuge, poudre de polyphosphate d'ammonium non hydrosoluble a constituant, et son procede de production |
| US7695651B2 (en) | 2004-02-16 | 2010-04-13 | Shin-Etsu Chemical Co., Ltd. | Flame retardant additives, emulsion type coating compositions, and flame retardant compositions |
| JP2009001435A (ja) * | 2007-06-19 | 2009-01-08 | Shin Etsu Chem Co Ltd | ポリリン酸アンモニウムの改質方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0455625B2 (enrdf_load_stackoverflow) | 1992-09-03 |
| DD239215A5 (de) | 1986-09-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH0453998B2 (enrdf_load_stackoverflow) | ||
| US4467056A (en) | Particulate agent for impeding the combustibility of combustible materials | |
| EP1373345A1 (en) | Stable liquid melamine urea formaldehyde resins | |
| US5085930A (en) | Particulate thermosetting adhesive compositions | |
| US3464854A (en) | Method of coating and composition therefor | |
| JPS61103962A (ja) | ポリ燐酸アンモニウムを基礎とする、加水分解安定な細分状耐燃剤の製法 | |
| US5552186A (en) | Process for coating a surface in contact with food using aqueous phenolic resin dispersions | |
| US4687651A (en) | Method for producing ammonium polyphosphate | |
| JPH10503746A (ja) | 化学的に結合した無機のポリマーコーティング及びそのための架橋用硬化剤 | |
| US3071492A (en) | Method of rendering starch hydrophobic and free flowing | |
| US2609360A (en) | Process of reacting polyvinylalcohol with urea phosphate | |
| US4945000A (en) | Particulate thermosetting adhesive compositions | |
| US3083185A (en) | Urea formaldehyde resin compositions containing adducts of sulfur oxides and aliphatic tertiary amines | |
| JPS5883023A (ja) | 硬化性組成物 | |
| KR920000627B1 (ko) | 폴리인산 암모늄을 기초물질로 한 가수분해되지 않는 방염제와 그 제조방법 | |
| JP2002529565A5 (enrdf_load_stackoverflow) | ||
| JPS581548A (ja) | 難燃性複合材料 | |
| JPS6198719A (ja) | 流動性粉末状ポリ燐酸アンモニウムを基剤とする防炎剤、その製造方法及び該防炎剤を含有する耐燃性に調整されたポリウレタン及びポリウレタンフオーム | |
| JP2001294412A (ja) | 被覆ポリリン酸アンモニウムおよびその製造方法 | |
| JPS5951582B2 (ja) | 発泡性防炎剤の製法 | |
| FI76108B (fi) | Foerfarande foer framstaellning av lim specieltt foer limning av cellulosahaltiga aemnen och textiler. | |
| US3816558A (en) | Filled aldehyde condensates having improved heat resistance | |
| US4180630A (en) | Phosphorus-nitrogen-silica composition as a flame retardant | |
| JPS61101514A (ja) | ポリ燐酸アンモニウムをベースとする加水分解安定性の耐燃剤、その製法及びこの耐燃剤を含む防火性ポリウレタン又はポリウレタンフオーム | |
| JPH08277102A (ja) | 不溶性ポリリン酸アンモニウム粒子及びその製造方法 |