JPS6046910A - 炭化硼素粉末の製造法 - Google Patents
炭化硼素粉末の製造法Info
- Publication number
- JPS6046910A JPS6046910A JP58154411A JP15441183A JPS6046910A JP S6046910 A JPS6046910 A JP S6046910A JP 58154411 A JP58154411 A JP 58154411A JP 15441183 A JP15441183 A JP 15441183A JP S6046910 A JPS6046910 A JP S6046910A
- Authority
- JP
- Japan
- Prior art keywords
- magnesium
- boron
- oxide
- reaction
- boron carbide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052580 B4C Inorganic materials 0.000 title claims abstract description 20
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 239000000843 powder Substances 0.000 title claims description 10
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 26
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 26
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims abstract description 24
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229910052796 boron Inorganic materials 0.000 claims abstract description 18
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000004327 boric acid Substances 0.000 claims abstract description 17
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 229910052810 boron oxide Inorganic materials 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims description 8
- NFMWFGXCDDYTEG-UHFFFAOYSA-N trimagnesium;diborate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]B([O-])[O-].[O-]B([O-])[O-] NFMWFGXCDDYTEG-UHFFFAOYSA-N 0.000 abstract description 20
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 16
- 229910052799 carbon Inorganic materials 0.000 abstract description 13
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 12
- 239000011777 magnesium Substances 0.000 abstract description 11
- 229910052749 magnesium Inorganic materials 0.000 abstract description 10
- 238000003763 carbonization Methods 0.000 abstract description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 4
- 238000010000 carbonizing Methods 0.000 abstract description 4
- 238000010438 heat treatment Methods 0.000 abstract description 4
- 239000007864 aqueous solution Substances 0.000 abstract description 2
- 229910021383 artificial graphite Inorganic materials 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- -1 artificial graphite Chemical compound 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 34
- 239000002994 raw material Substances 0.000 description 10
- 238000006722 reduction reaction Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- 239000007789 gas Substances 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000000028 HMX Substances 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 150000001638 boron Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- UZGLIIJVICEWHF-UHFFFAOYSA-N octogen Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UZGLIIJVICEWHF-UHFFFAOYSA-N 0.000 description 1
- YWCYJWYNSHTONE-UHFFFAOYSA-O oxido(oxonio)boron Chemical compound [OH2+][B][O-] YWCYJWYNSHTONE-UHFFFAOYSA-O 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002683 reaction inhibitor Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP58154411A JPS6046910A (ja) | 1983-08-24 | 1983-08-24 | 炭化硼素粉末の製造法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP58154411A JPS6046910A (ja) | 1983-08-24 | 1983-08-24 | 炭化硼素粉末の製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6046910A true JPS6046910A (ja) | 1985-03-14 |
JPH0372570B2 JPH0372570B2 (cs) | 1991-11-19 |
Family
ID=15583562
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP58154411A Granted JPS6046910A (ja) | 1983-08-24 | 1983-08-24 | 炭化硼素粉末の製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6046910A (cs) |
-
1983
- 1983-08-24 JP JP58154411A patent/JPS6046910A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPH0372570B2 (cs) | 1991-11-19 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US4459363A (en) | Synthesis of refractory materials | |
US4241037A (en) | Process for purifying silicon | |
JP5692950B2 (ja) | Zr金属粉末の製造方法 | |
US4605542A (en) | Process for producing silicon carbide whisker | |
EP1437326B1 (en) | Method for producing silicon | |
US3350166A (en) | Synthesis of aluminum borate whiskers | |
JPS606908B2 (ja) | 硼素成分を含有する活性な炭化珪素質粉末の製造方法 | |
JPS6046910A (ja) | 炭化硼素粉末の製造法 | |
JPH0353279B2 (cs) | ||
Sudoh et al. | Synthesis of boron carbide microcrystals from saccharides and boric acid | |
JP3647079B2 (ja) | 六方晶窒化ほう素粉末の製造方法 | |
JPH0575694B2 (cs) | ||
JPH0476356B2 (cs) | ||
JPS58115016A (ja) | 微粉末炭化珪素の製造方法 | |
JPH0372569B2 (cs) | ||
JPH0130766B2 (cs) | ||
JP3521173B2 (ja) | 六方晶窒化ほう素粉末の製造方法 | |
RU2130424C1 (ru) | Способ получения карбида титана | |
US2036221A (en) | Method of purifying zirconium silicates | |
JP3397503B2 (ja) | 低圧相窒化ほう素粉末の製造方法 | |
SU1181999A1 (ru) | Способ получени порошкообразных пирониобатов кальци и стронци | |
JP2000034116A (ja) | 炭化ケイ素およびシリコンの製造方法 | |
TW202212585A (zh) | 低氧AlSc合金粉末及其製造方法 | |
JPS59164613A (ja) | 高純度微粉末シリコンの製造方法 | |
JPS63203729A (ja) | 高純度金属リチウムの製造方法 |