JPS6045641B2 - 重合体を単離する方法 - Google Patents
重合体を単離する方法Info
- Publication number
- JPS6045641B2 JPS6045641B2 JP53061760A JP6176078A JPS6045641B2 JP S6045641 B2 JPS6045641 B2 JP S6045641B2 JP 53061760 A JP53061760 A JP 53061760A JP 6176078 A JP6176078 A JP 6176078A JP S6045641 B2 JPS6045641 B2 JP S6045641B2
- Authority
- JP
- Japan
- Prior art keywords
- water
- zone
- polymer
- separator
- settling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920000642 polymer Polymers 0.000 title claims description 66
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 91
- 238000000034 method Methods 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 18
- 230000006835 compression Effects 0.000 claims description 15
- 238000007906 compression Methods 0.000 claims description 15
- 238000000926 separation method Methods 0.000 claims description 12
- 229920001973 fluoroelastomer Polymers 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 7
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 5
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 claims description 5
- 238000002955 isolation Methods 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000000178 monomer Substances 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims description 3
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- 239000003039 volatile agent Substances 0.000 claims 2
- 238000010348 incorporation Methods 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 claims 1
- 239000002002 slurry Substances 0.000 description 18
- 239000012071 phase Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 238000013461 design Methods 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 230000001276 controlling effect Effects 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 238000001125 extrusion Methods 0.000 description 3
- 230000005484 gravity Effects 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 238000004062 sedimentation Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000009471 action Effects 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 239000000701 coagulant Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 229930185605 Bisphenol Natural products 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- USFRYJRPHFMVBZ-UHFFFAOYSA-M benzyl(triphenyl)phosphanium;chloride Chemical compound [Cl-].C=1C=CC=CC=1[P+](C=1C=CC=CC=1)(C=1C=CC=CC=1)CC1=CC=CC=C1 USFRYJRPHFMVBZ-UHFFFAOYSA-M 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- GRLPQNLYRHEGIJ-UHFFFAOYSA-J potassium aluminium sulfate Chemical compound [Al+3].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GRLPQNLYRHEGIJ-UHFFFAOYSA-J 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/24—Treatment of polymer suspensions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/009—Heating or cooling mechanisms specially adapted for settling tanks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/02—Settling tanks with single outlets for the separated liquid
- B01D21/04—Settling tanks with single outlets for the separated liquid with moving scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/2427—The feed or discharge opening located at a distant position from the side walls
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/245—Discharge mechanisms for the sediments
- B01D21/2461—Positive-displacement pumps; Screw feeders; Trough conveyors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/30—Control equipment
- B01D21/34—Controlling the feed distribution; Controlling the liquid level ; Control of process parameters
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
- Extrusion Moulding Of Plastics Or The Like (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/801,370 US4132845A (en) | 1977-05-27 | 1977-05-27 | Mechanical dewatering process for elastomer slurries |
| US801370 | 1985-11-25 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS53147787A JPS53147787A (en) | 1978-12-22 |
| JPS6045641B2 true JPS6045641B2 (ja) | 1985-10-11 |
Family
ID=25180923
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP53061760A Expired JPS6045641B2 (ja) | 1977-05-27 | 1978-05-25 | 重合体を単離する方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4132845A (Direct) |
| JP (1) | JPS6045641B2 (Direct) |
| CA (1) | CA1118368A (Direct) |
| DE (1) | DE2822635A1 (Direct) |
| FR (1) | FR2392039A1 (Direct) |
| GB (2) | GB1601055A (Direct) |
| IT (1) | IT1094841B (Direct) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4408038A (en) * | 1982-03-29 | 1983-10-04 | E. I. Du Pont De Nemours & Co. | In-line coagulation process for fluoroelastomer emulsions |
| US4954303A (en) * | 1989-02-10 | 1990-09-04 | The Dow Chemical Company | Apparatus and process for devolatilization of high viscosity polymers |
| US4944657A (en) * | 1989-03-01 | 1990-07-31 | Mowli John C | Two-stage pumping apparatus with low shear first stage |
| US4968236A (en) * | 1989-07-06 | 1990-11-06 | Ultra Span - A Division Of Alphair Ventilating Systems Inc. | Auxiliary auger assembly for hollow core slab production |
| US5041249A (en) * | 1989-12-26 | 1991-08-20 | Exxon Chemical Patent Inc. | Process for low-temperature elastomer finishing |
| DE4110943C1 (Direct) * | 1991-04-05 | 1992-10-15 | Adalbert Dr.-Ing. 4280 Borken De Nagy | |
| US5267837A (en) * | 1992-09-23 | 1993-12-07 | Mowli John C | Two-stage pumping apparatus with non-meshing first stage augers |
| US5628560A (en) * | 1995-05-24 | 1997-05-13 | American Maplan Corporation | Double-screw extruder |
| US6239223B1 (en) | 1997-09-05 | 2001-05-29 | Chemfab Corporation | Fluoropolymeric composition |
| JP4779280B2 (ja) * | 1999-09-01 | 2011-09-28 | ダイキン工業株式会社 | 含フッ素弾性状共重合体組成物の製造方法 |
| US6720360B1 (en) * | 2000-02-01 | 2004-04-13 | 3M Innovative Properties Company | Ultra-clean fluoropolymers |
| US6593416B2 (en) | 2000-02-01 | 2003-07-15 | 3M Innovative Properties Company | Fluoropolymers |
| EP1889855B1 (en) * | 2005-05-02 | 2010-04-14 | Daikin Industries, Ltd. | Method for producing fluorine-containing polymer |
| DE202010001758U1 (de) * | 2010-02-02 | 2011-06-09 | UTS Biogastechnik GmbH, 85399 | Schneckenseparator |
| DE202010001759U1 (de) * | 2010-02-02 | 2011-06-09 | UTS Biogastechnik GmbH, 85399 | Schneckenseparator |
| DE202010001765U1 (de) * | 2010-02-02 | 2011-06-09 | UTS Biogastechnik GmbH, 85399 | Schneckenseparator |
| DE202017005336U1 (de) * | 2017-10-17 | 2019-01-21 | Leybold Gmbh | Schraubenrotor |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL258615A (Direct) * | 1959-12-01 | 1900-01-01 | ||
| DE1779922A1 (de) * | 1961-02-17 | 1972-01-13 | Internat Basic Economy Corp | Vorrichtung zum Entfernen von Fluessigkeit aus Elastomeren |
| US3687288A (en) * | 1970-09-03 | 1972-08-29 | Marco Dev Co Inc | Separator and method |
| FR2321456A1 (fr) * | 1975-08-19 | 1977-03-18 | Alsthom Cgee | Procede pour le compactage et l'essorage des boues fluides chargees de matieres fibreuses |
-
1977
- 1977-05-27 US US05/801,370 patent/US4132845A/en not_active Expired - Lifetime
-
1978
- 1978-05-24 CA CA000303931A patent/CA1118368A/en not_active Expired
- 1978-05-24 DE DE19782822635 patent/DE2822635A1/de active Granted
- 1978-05-25 JP JP53061760A patent/JPS6045641B2/ja not_active Expired
- 1978-05-25 GB GB21556/79A patent/GB1601055A/en not_active Expired
- 1978-05-25 GB GB22386/78A patent/GB1601054A/en not_active Expired
- 1978-05-26 IT IT23901/78A patent/IT1094841B/it active
- 1978-05-26 FR FR7815748A patent/FR2392039A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IT7823901A0 (it) | 1978-05-26 |
| US4132845A (en) | 1979-01-02 |
| CA1118368A (en) | 1982-02-16 |
| FR2392039B1 (Direct) | 1984-12-28 |
| JPS53147787A (en) | 1978-12-22 |
| GB1601055A (en) | 1981-10-21 |
| GB1601054A (en) | 1981-10-21 |
| DE2822635A1 (de) | 1978-11-30 |
| IT1094841B (it) | 1985-08-10 |
| FR2392039A1 (fr) | 1978-12-22 |
| DE2822635C2 (Direct) | 1988-10-06 |
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