JPS5924099B2 - 焼結結晶セラミツク物品のクリストバライト相発生を阻止する方法 - Google Patents
焼結結晶セラミツク物品のクリストバライト相発生を阻止する方法Info
- Publication number
- JPS5924099B2 JPS5924099B2 JP51012149A JP1214976A JPS5924099B2 JP S5924099 B2 JPS5924099 B2 JP S5924099B2 JP 51012149 A JP51012149 A JP 51012149A JP 1214976 A JP1214976 A JP 1214976A JP S5924099 B2 JPS5924099 B2 JP S5924099B2
- Authority
- JP
- Japan
- Prior art keywords
- glass
- frit
- oxide
- article
- cristobalite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims description 61
- 229910052906 cristobalite Inorganic materials 0.000 title claims description 34
- 238000000034 method Methods 0.000 title claims description 12
- 239000011222 crystalline ceramic Substances 0.000 title claims description 6
- 229910002106 crystalline ceramic Inorganic materials 0.000 title claims description 6
- 239000011521 glass Substances 0.000 claims description 39
- 239000003112 inhibitor Substances 0.000 claims description 29
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 17
- 238000010304 firing Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 9
- 238000002844 melting Methods 0.000 claims description 9
- 230000008018 melting Effects 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 6
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 claims description 4
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 claims description 3
- 238000011065 in-situ storage Methods 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 230000002401 inhibitory effect Effects 0.000 claims 2
- 229910017583 La2O Inorganic materials 0.000 claims 1
- 238000010298 pulverizing process Methods 0.000 claims 1
- 238000010791 quenching Methods 0.000 claims 1
- 230000000171 quenching effect Effects 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 26
- 239000000377 silicon dioxide Substances 0.000 description 15
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical compound [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 description 11
- 229910052644 β-spodumene Inorganic materials 0.000 description 9
- 150000001768 cations Chemical class 0.000 description 7
- 238000005245 sintering Methods 0.000 description 7
- 229910000502 Li-aluminosilicate Inorganic materials 0.000 description 6
- 229910052681 coesite Inorganic materials 0.000 description 5
- 239000002241 glass-ceramic Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000006104 solid solution Substances 0.000 description 5
- 229910052682 stishovite Inorganic materials 0.000 description 5
- 229910052905 tridymite Inorganic materials 0.000 description 5
- 238000007792 addition Methods 0.000 description 4
- 239000006121 base glass Substances 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 4
- 235000012239 silicon dioxide Nutrition 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000002019 doping agent Substances 0.000 description 3
- 238000010587 phase diagram Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000002202 Polyethylene glycol Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 2
- 239000006066 glass batch Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 229910052863 mullite Inorganic materials 0.000 description 2
- 229920001223 polyethylene glycol Polymers 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 101100481408 Danio rerio tie2 gene Proteins 0.000 description 1
- 101100481410 Mus musculus Tek gene Proteins 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- HEHRHMRHPUNLIR-UHFFFAOYSA-N aluminum;hydroxy-[hydroxy(oxo)silyl]oxy-oxosilane;lithium Chemical compound [Li].[Al].O[Si](=O)O[Si](O)=O.O[Si](=O)O[Si](O)=O HEHRHMRHPUNLIR-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 238000000462 isostatic pressing Methods 0.000 description 1
- 229910052746 lanthanum Inorganic materials 0.000 description 1
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 239000010955 niobium Substances 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 229910052670 petalite Inorganic materials 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 238000007569 slipcasting Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910052642 spodumene Inorganic materials 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052643 α-spodumene Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0018—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents
- C03C10/0027—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents containing SiO2, Al2O3, Li2O as main constituents
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Compositions Of Oxide Ceramics (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/548,548 US3951670A (en) | 1975-02-10 | 1975-02-10 | Cristobalite suppression in high-silica Li2 O-Al2 O-SiO2 devitrified glass frits |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS51103913A JPS51103913A (enExample) | 1976-09-14 |
| JPS5924099B2 true JPS5924099B2 (ja) | 1984-06-07 |
Family
ID=24189338
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP51012149A Expired JPS5924099B2 (ja) | 1975-02-10 | 1976-02-06 | 焼結結晶セラミツク物品のクリストバライト相発生を阻止する方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3951670A (enExample) |
| JP (1) | JPS5924099B2 (enExample) |
| DE (1) | DE2602106C2 (enExample) |
| FR (1) | FR2300050A1 (enExample) |
| GB (1) | GB1493743A (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4042403A (en) * | 1975-05-19 | 1977-08-16 | Corning Glass Works | Thermally stable glass-ceramic articles |
| US4047960A (en) * | 1976-06-18 | 1977-09-13 | Corning Glass Works | Refractory partially crystalline materials with good visible transparency |
| US4162921A (en) * | 1977-01-05 | 1979-07-31 | Firsov Vitaly M | Glass-crystalline material and method of producing same |
| JPS544914A (en) * | 1977-06-14 | 1979-01-16 | Asahi Glass Co Ltd | Highhdense lowwexpandable sintered body |
| US4189325A (en) * | 1979-01-09 | 1980-02-19 | The Board of Regents, State of Florida, University of Florida | Glass-ceramic dental restorations |
| US4353966A (en) * | 1980-12-12 | 1982-10-12 | United Technologies Corporation | Composite bonding |
| JPS6345148A (ja) * | 1986-08-11 | 1988-02-26 | Natl Inst For Res In Inorg Mater | 機械加工性の針状結晶析出結晶化ガラスの製造方法 |
| US5096857A (en) * | 1990-10-22 | 1992-03-17 | E. I. Du Pont De Nemours And Company | Chemically stabilized cristobalite |
| US5084328A (en) * | 1990-12-24 | 1992-01-28 | Corning Incorporated | Strong, surface crystallized glass articles |
| US7229286B2 (en) * | 1998-07-10 | 2007-06-12 | Jones Derek W | Composite veneered cast glass-ceramic dental construct |
| JP2000086289A (ja) * | 1998-09-10 | 2000-03-28 | Ngk Insulators Ltd | 結晶化ガラスの核形成剤、結晶化ガラス、磁気ディスク基板および磁気ディスク |
| KR102595466B1 (ko) * | 2017-09-05 | 2023-10-30 | 니폰 덴키 가라스 가부시키가이샤 | Las계 결정성 유리, las계 결정화 유리, 및 그것들의 제조 방법 |
| CN110386811A (zh) * | 2018-04-16 | 2019-10-29 | 中国科学院上海硅酸盐研究所 | 一种具有零平均线热膨胀系数的复相陶瓷材料及其制备方法 |
| CN111018506B (zh) * | 2019-11-28 | 2022-08-26 | 浙江锦诚新材料股份有限公司 | 一种用于水泥窑预热器抗结皮喷涂料 |
| CN117682849B (zh) * | 2023-11-20 | 2025-12-05 | 深圳顺络电子股份有限公司 | 一种可低温烧结的陶瓷材料及其制备方法、层叠体 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL236367A (enExample) * | 1958-03-03 | |||
| US3112184A (en) * | 1958-09-08 | 1963-11-26 | Corning Glass Works | Method of making ceramic articles |
| NL252872A (enExample) * | 1959-07-01 | |||
| US3006775A (en) * | 1959-09-23 | 1961-10-31 | Gen Electric | Ceramic material and method of making the same |
| US3084053A (en) * | 1960-05-13 | 1963-04-02 | Robert H Arlett | Ceramic materials and method for making same |
| US3251403A (en) * | 1962-01-05 | 1966-05-17 | Corning Glass Works | Ceramic heat exchanger structures |
| US3279931A (en) * | 1963-02-13 | 1966-10-18 | Corning Glass Works | Glass-ceramic body and method of making it |
| US3600204A (en) * | 1968-05-31 | 1971-08-17 | Corning Glass Works | Glass-ceramic article prepared from low expansion thermally devitrifiable glass frit |
| US3839001A (en) * | 1973-07-20 | 1974-10-01 | Corning Glass Works | Manufacture of ceramic article |
-
1975
- 1975-02-10 US US05/548,548 patent/US3951670A/en not_active Expired - Lifetime
- 1975-10-31 GB GB45251/75A patent/GB1493743A/en not_active Expired
-
1976
- 1976-01-21 DE DE2602106A patent/DE2602106C2/de not_active Expired
- 1976-02-06 FR FR7603309A patent/FR2300050A1/fr active Granted
- 1976-02-06 JP JP51012149A patent/JPS5924099B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3951670A (en) | 1976-04-20 |
| GB1493743A (en) | 1977-11-30 |
| DE2602106A1 (de) | 1976-08-19 |
| FR2300050B1 (enExample) | 1982-04-23 |
| JPS51103913A (enExample) | 1976-09-14 |
| DE2602106C2 (de) | 1986-09-11 |
| FR2300050A1 (fr) | 1976-09-03 |
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