JPS59199683A - 酸無水物の簡易精製法 - Google Patents
酸無水物の簡易精製法Info
- Publication number
- JPS59199683A JPS59199683A JP7333783A JP7333783A JPS59199683A JP S59199683 A JPS59199683 A JP S59199683A JP 7333783 A JP7333783 A JP 7333783A JP 7333783 A JP7333783 A JP 7333783A JP S59199683 A JPS59199683 A JP S59199683A
- Authority
- JP
- Japan
- Prior art keywords
- anhydride
- acid anhydride
- dianhydride
- acid
- bis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000008065 acid anhydrides Chemical class 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 title description 2
- 238000000746 purification Methods 0.000 title 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims abstract 4
- GTDPSWPPOUPBNX-UHFFFAOYSA-N ac1mqpva Chemical compound CC12C(=O)OC(=O)C1(C)C1(C)C2(C)C(=O)OC1=O GTDPSWPPOUPBNX-UHFFFAOYSA-N 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000000052 vinegar Substances 0.000 claims description 8
- 235000021419 vinegar Nutrition 0.000 claims description 8
- 125000004018 acid anhydride group Chemical group 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract description 24
- 150000008064 anhydrides Chemical group 0.000 abstract description 10
- VLDPXPPHXDGHEW-UHFFFAOYSA-N 1-chloro-2-dichlorophosphoryloxybenzene Chemical compound ClC1=CC=CC=C1OP(Cl)(Cl)=O VLDPXPPHXDGHEW-UHFFFAOYSA-N 0.000 abstract description 2
- ROFZMKDROVBLNY-UHFFFAOYSA-N 4-nitro-2-benzofuran-1,3-dione Chemical compound [O-][N+](=O)C1=CC=CC2=C1C(=O)OC2=O ROFZMKDROVBLNY-UHFFFAOYSA-N 0.000 abstract 1
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 abstract 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 abstract 1
- 238000010908 decantation Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- DOBFTMLCEYUAQC-UHFFFAOYSA-N naphthalene-2,3,6,7-tetracarboxylic acid Chemical compound OC(=O)C1=C(C(O)=O)C=C2C=C(C(O)=O)C(C(=O)O)=CC2=C1 DOBFTMLCEYUAQC-UHFFFAOYSA-N 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- -1 2,3- dicarboxyphenyl Chemical group 0.000 description 9
- 241001474791 Proboscis Species 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 241000251468 Actinopterygii Species 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 241001070941 Castanea Species 0.000 description 2
- 235000014036 Castanea Nutrition 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000007983 Tris buffer Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- UFMBOFGKHIXOTA-UHFFFAOYSA-N 2-methylterephthalic acid Chemical compound CC1=CC(C(O)=O)=CC=C1C(O)=O UFMBOFGKHIXOTA-UHFFFAOYSA-N 0.000 description 1
- 101100043731 Caenorhabditis elegans syx-3 gene Proteins 0.000 description 1
- 101100535673 Drosophila melanogaster Syn gene Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 101100368134 Mus musculus Syn1 gene Proteins 0.000 description 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- VHCQVGQULWFQTM-UHFFFAOYSA-N Rubone Natural products COC1=CC(OC)=CC(O)=C1C(=O)C=CC1=CC(OC)=C(OC)C=C1OC VHCQVGQULWFQTM-UHFFFAOYSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000001467 acupuncture Methods 0.000 description 1
- 239000010866 blackwater Substances 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- UIUXUFNYAYAMOE-UHFFFAOYSA-N methylsilane Chemical compound [SiH3]C UIUXUFNYAYAMOE-UHFFFAOYSA-N 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 239000008239 natural water Substances 0.000 description 1
- XPEFOHCUPVNIAG-UHFFFAOYSA-N perylene-2,3,9,10-tetracarboxylic acid Chemical compound C1=CC2=C(C(O)=O)C(C(=O)O)=CC(C=3C4=C5C=CC(=C4C(C(O)=O)=CC=3)C(O)=O)=C2C5=C1 XPEFOHCUPVNIAG-UHFFFAOYSA-N 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 210000004894 snout Anatomy 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 150000000000 tetracarboxylic acids Chemical class 0.000 description 1
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Furan Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7333783A JPS59199683A (ja) | 1983-04-26 | 1983-04-26 | 酸無水物の簡易精製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7333783A JPS59199683A (ja) | 1983-04-26 | 1983-04-26 | 酸無水物の簡易精製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59199683A true JPS59199683A (ja) | 1984-11-12 |
| JPH0337551B2 JPH0337551B2 (enrdf_load_stackoverflow) | 1991-06-05 |
Family
ID=13515243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7333783A Granted JPS59199683A (ja) | 1983-04-26 | 1983-04-26 | 酸無水物の簡易精製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59199683A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT395975B (de) * | 1985-12-25 | 1993-04-26 | Daicel Chem | Verfahren zur herstellung eines organischen carbonsaeureanhydrids |
| JP2007051131A (ja) * | 2005-07-21 | 2007-03-01 | Mitsubishi Gas Chem Co Inc | 高純度ピロメリット酸二無水物の製造法 |
| JP2008174485A (ja) * | 2007-01-18 | 2008-07-31 | Mitsubishi Gas Chem Co Inc | 晶析方法 |
| WO2015029457A1 (en) * | 2013-09-02 | 2015-03-05 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method for producing pyromellitic dianhydride, pyromellitic dianhydride produced by the method, and apparatus therefor |
-
1983
- 1983-04-26 JP JP7333783A patent/JPS59199683A/ja active Granted
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT395975B (de) * | 1985-12-25 | 1993-04-26 | Daicel Chem | Verfahren zur herstellung eines organischen carbonsaeureanhydrids |
| JP2007051131A (ja) * | 2005-07-21 | 2007-03-01 | Mitsubishi Gas Chem Co Inc | 高純度ピロメリット酸二無水物の製造法 |
| JP2008174485A (ja) * | 2007-01-18 | 2008-07-31 | Mitsubishi Gas Chem Co Inc | 晶析方法 |
| WO2015029457A1 (en) * | 2013-09-02 | 2015-03-05 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method for producing pyromellitic dianhydride, pyromellitic dianhydride produced by the method, and apparatus therefor |
| JP2016529281A (ja) * | 2013-09-02 | 2016-09-23 | 日本エア・リキード株式会社 | ピロメリット酸二無水物の製造方法、該方法により製造されたピロメリット酸二無水物、ピロメリット酸二無水物の供給方法および供給装置 |
| US9856269B2 (en) | 2013-09-02 | 2018-01-02 | L'Air Liquide, SociétéAnonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Method for producing pyromellitic dianhydride, pyromellitic dianhydride produced by the method, and apparatus therefor |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0337551B2 (enrdf_load_stackoverflow) | 1991-06-05 |
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