JPS5913171B2 - 脱カチオン化乳およびその製法 - Google Patents
脱カチオン化乳およびその製法Info
- Publication number
- JPS5913171B2 JPS5913171B2 JP5908181A JP5908181A JPS5913171B2 JP S5913171 B2 JPS5913171 B2 JP S5913171B2 JP 5908181 A JP5908181 A JP 5908181A JP 5908181 A JP5908181 A JP 5908181A JP S5913171 B2 JPS5913171 B2 JP S5913171B2
- Authority
- JP
- Japan
- Prior art keywords
- milk
- cation exchange
- exchange resin
- casein
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 235000013336 milk Nutrition 0.000 title claims description 112
- 210000004080 milk Anatomy 0.000 title claims description 112
- 239000008267 milk Substances 0.000 title claims description 110
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- 239000003729 cation exchange resin Substances 0.000 claims description 36
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 33
- 239000002253 acid Substances 0.000 claims description 25
- 239000011347 resin Substances 0.000 claims description 24
- 229920005989 resin Polymers 0.000 claims description 24
- 239000011148 porous material Substances 0.000 claims description 18
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- 239000011707 mineral Substances 0.000 claims description 17
- 230000002378 acidificating effect Effects 0.000 claims description 15
- 125000000542 sulfonic acid group Chemical group 0.000 claims description 8
- 235000020183 skimmed milk Nutrition 0.000 claims description 7
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 6
- 239000008101 lactose Substances 0.000 claims description 6
- 102000004169 proteins and genes Human genes 0.000 claims description 6
- 108090000623 proteins and genes Proteins 0.000 claims description 6
- 239000004793 Polystyrene Substances 0.000 claims description 5
- 229920002223 polystyrene Polymers 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 4
- 102000011632 Caseins Human genes 0.000 description 57
- 108010076119 Caseins Proteins 0.000 description 57
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 56
- 235000021240 caseins Nutrition 0.000 description 56
- 239000005018 casein Substances 0.000 description 55
- 239000005862 Whey Substances 0.000 description 39
- 102000007544 Whey Proteins Human genes 0.000 description 39
- 108010046377 Whey Proteins Proteins 0.000 description 39
- 239000000203 mixture Substances 0.000 description 28
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 22
- 235000013351 cheese Nutrition 0.000 description 17
- 239000002245 particle Substances 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 239000012141 concentrate Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 9
- 235000020185 raw untreated milk Nutrition 0.000 description 8
- 239000000126 substance Substances 0.000 description 6
- 229940071162 caseinate Drugs 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000005345 coagulation Methods 0.000 description 5
- 230000015271 coagulation Effects 0.000 description 5
- 229920001577 copolymer Polymers 0.000 description 5
- 238000005115 demineralization Methods 0.000 description 5
- 230000002328 demineralizing effect Effects 0.000 description 5
- 108010058314 rennet Proteins 0.000 description 5
- 229940108461 rennet Drugs 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 238000000108 ultra-filtration Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 229920002125 Sokalan® Polymers 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 229940023913 cation exchange resins Drugs 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 4
- 230000020477 pH reduction Effects 0.000 description 4
- 235000018102 proteins Nutrition 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- 229920001429 chelating resin Polymers 0.000 description 3
- 230000001112 coagulating effect Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 239000004310 lactic acid Substances 0.000 description 2
- 235000014655 lactic acid Nutrition 0.000 description 2
- 150000007522 mineralic acids Chemical class 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 2
- 229910001414 potassium ion Inorganic materials 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910001415 sodium ion Inorganic materials 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- CHRJZRDFSQHIFI-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;styrene Chemical class C=CC1=CC=CC=C1.C=CC1=CC=CC=C1C=C CHRJZRDFSQHIFI-UHFFFAOYSA-N 0.000 description 1
- HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical group C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 235000006770 Malva sylvestris Nutrition 0.000 description 1
- 102000014171 Milk Proteins Human genes 0.000 description 1
- 108010011756 Milk Proteins Proteins 0.000 description 1
- 244000038561 Modiola caroliniana Species 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229940021722 caseins Drugs 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- MYRTYDVEIRVNKP-UHFFFAOYSA-N divinylbenzene Substances C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 1
- 238000000909 electrodialysis Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- -1 hydrogen ions Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 235000021239 milk protein Nutrition 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000010494 opalescence Effects 0.000 description 1
- 235000013550 pizza Nutrition 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000009919 sequestration Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 229940080237 sodium caseinate Drugs 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/14—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment
- A23C9/146—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment by ion-exchange
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C19/00—Cheese; Cheese preparations; Making thereof
- A23C19/02—Making cheese curd
- A23C19/045—Coagulation of milk without rennet or rennet substitutes
- A23C19/0455—Coagulation by direct acidification without fermentation of the milk, e.g. by chemical or physical means
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C21/00—Whey; Whey preparations
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/20—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from milk, e.g. casein; from whey
- A23J1/202—Casein or caseinates
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biotechnology (AREA)
- Biochemistry (AREA)
- Dairy Products (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8008644A FR2480568A1 (fr) | 1980-04-17 | 1980-04-17 | Procede de traitement du lait par une resine echangeuse de cations en vue de la fabrication de la caseine et du lactoserum |
| FR8008644 | 1980-04-17 | ||
| FR8106470 | 1981-03-31 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5718943A JPS5718943A (en) | 1982-01-30 |
| JPS5913171B2 true JPS5913171B2 (ja) | 1984-03-28 |
Family
ID=9241018
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5908181A Expired JPS5913171B2 (ja) | 1980-04-17 | 1981-04-17 | 脱カチオン化乳およびその製法 |
| JP18295683A Granted JPS59102351A (ja) | 1980-04-17 | 1983-09-29 | 脱カチオン化乳を用いる乳加工法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18295683A Granted JPS59102351A (ja) | 1980-04-17 | 1983-09-29 | 脱カチオン化乳を用いる乳加工法 |
Country Status (2)
| Country | Link |
|---|---|
| JP (2) | JPS5913171B2 (enrdf_load_stackoverflow) |
| FR (1) | FR2480568A1 (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60176667U (ja) * | 1984-05-01 | 1985-11-22 | 山口 正人 | 掛けぶとんカバ− |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2514615B1 (fr) * | 1981-10-21 | 1985-10-18 | Bridel Laiteries | Procede de traitement du lait par electrodialyse sur membranes cationiques, lait decationise acide ainsi obtenu et utilisation de ce dernier pour la fabrication de la caseine, du caille de lait pour fromages et du lactoserum |
| FR2534455B1 (fr) * | 1982-10-14 | 1985-08-23 | Bridel Laiteries | Procede de preparation des boissons aromatisees de longue conservation, a base de lactoserum acidifie |
| FR2552631B1 (fr) * | 1983-10-03 | 1990-10-19 | Meram Sa Laboratoires | Lait et produits laitiers appauvris ou non en calcium et enrichis en magnesium |
| AU580619B2 (en) * | 1984-09-11 | 1989-01-19 | Kraft Inc. | Manufacture of high-solids pre-cheese and cheeses |
| JPS61257140A (ja) * | 1985-05-11 | 1986-11-14 | Yamasa Shoyu Co Ltd | カルシウム強化牛乳の製造法 |
| DE3842980C2 (de) * | 1988-12-21 | 1995-06-29 | Westfalia Separator Ag | Verfahren zur zentrifugalen Behandlung von Käsereimilch und Zentrifuge zur Durchführung des Verfahrens |
| JP2631155B2 (ja) * | 1990-07-27 | 1997-07-16 | 明治乳業 株式会社 | 低ナトリウム粉乳の製造法 |
| JPH0751045B2 (ja) * | 1990-07-27 | 1995-06-05 | 明治乳業株式会社 | 低ナトリウムチーズ及びその製造法 |
| JPH04179440A (ja) * | 1990-07-27 | 1992-06-26 | Meiji Milk Prod Co Ltd | 低ナトリウム乳製品及びその製造法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH288707A (fr) * | 1946-09-11 | 1953-02-15 | M & R Dietetic Lab Inc | Procédé pour l'obtention d'un produit lacté non solide et produit obtenu par ce procédé. |
| FR1469793A (fr) * | 1966-02-22 | 1967-02-17 | Procédé de séparation de la caséine du lait en vue de la production de petit-lait pour la fabrication de lactose et de produits alimentaires | |
| FR2331963A1 (fr) * | 1975-11-20 | 1977-06-17 | Zuid Nl Melkindustrie | Procede de fabrication de petit-lait ou de produits de petit-lait a partir de lait ecreme ou de ses melanges |
| FR2418626A1 (fr) * | 1978-03-02 | 1979-09-28 | Triballat Laiteries | Procede et installations pour la preparation de la caseine a partir du lait et produits ainsi obtenus |
-
1980
- 1980-04-17 FR FR8008644A patent/FR2480568A1/fr active Granted
-
1981
- 1981-04-17 JP JP5908181A patent/JPS5913171B2/ja not_active Expired
-
1983
- 1983-09-29 JP JP18295683A patent/JPS59102351A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60176667U (ja) * | 1984-05-01 | 1985-11-22 | 山口 正人 | 掛けぶとんカバ− |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6121053B2 (enrdf_load_stackoverflow) | 1986-05-24 |
| JPS5718943A (en) | 1982-01-30 |
| FR2480568B1 (enrdf_load_stackoverflow) | 1984-09-14 |
| JPS59102351A (ja) | 1984-06-13 |
| FR2480568A1 (fr) | 1981-10-23 |
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