JPS5891103A - コロイド銀粒子分散物の製造方法 - Google Patents
コロイド銀粒子分散物の製造方法Info
- Publication number
- JPS5891103A JPS5891103A JP18978681A JP18978681A JPS5891103A JP S5891103 A JPS5891103 A JP S5891103A JP 18978681 A JP18978681 A JP 18978681A JP 18978681 A JP18978681 A JP 18978681A JP S5891103 A JPS5891103 A JP S5891103A
- Authority
- JP
- Japan
- Prior art keywords
- soln
- dispersion
- colloidal silver
- silver particles
- reducing agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000006185 dispersion Substances 0.000 title claims abstract description 13
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 9
- 239000002245 particle Substances 0.000 title claims abstract description 9
- 238000004519 manufacturing process Methods 0.000 title description 7
- 238000003756 stirring Methods 0.000 claims abstract description 16
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 12
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000012266 salt solution Substances 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 abstract description 7
- 108010010803 Gelatin Proteins 0.000 abstract description 4
- 239000000084 colloidal system Substances 0.000 abstract description 4
- 229920000159 gelatin Polymers 0.000 abstract description 4
- 239000008273 gelatin Substances 0.000 abstract description 4
- 235000019322 gelatine Nutrition 0.000 abstract description 4
- 235000011852 gelatine desserts Nutrition 0.000 abstract description 4
- 229920001353 Dextrin Polymers 0.000 abstract description 3
- 239000004375 Dextrin Substances 0.000 abstract description 3
- 235000019425 dextrin Nutrition 0.000 abstract description 2
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 abstract 2
- 230000001681 protective effect Effects 0.000 abstract 1
- 229910001961 silver nitrate Inorganic materials 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 12
- 239000010410 layer Substances 0.000 description 6
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 4
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 4
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 4
- -1 gill iron Chemical class 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910021607 Silver chloride Inorganic materials 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 238000000862 absorption spectrum Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 235000012149 noodles Nutrition 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 229940079877 pyrogallol Drugs 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 2
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- FUPIVZHYVSCYLX-UHFFFAOYSA-N 1,4-dihydronaphthalene Chemical compound C1=CC=C2CC=CCC2=C1 FUPIVZHYVSCYLX-UHFFFAOYSA-N 0.000 description 1
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 1
- JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 1
- OXZGHXNVWYYFQU-UHFFFAOYSA-N B.[AlH3] Chemical compound B.[AlH3] OXZGHXNVWYYFQU-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 229920002284 Cellulose triacetate Polymers 0.000 description 1
- 229920002307 Dextran Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 229910021612 Silver iodide Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 description 1
- 125000003289 ascorbyl group Chemical class [H]O[C@@]([H])(C([H])([H])O*)[C@@]1([H])OC(=O)C(O*)=C1O* 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 150000003378 silver Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 1
- 229940045105 silver iodide Drugs 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0004—Preparation of sols
- B01J13/0043—Preparation of sols containing elemental metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Colloid Chemistry (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18978681A JPS5891103A (ja) | 1981-11-25 | 1981-11-25 | コロイド銀粒子分散物の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18978681A JPS5891103A (ja) | 1981-11-25 | 1981-11-25 | コロイド銀粒子分散物の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5891103A true JPS5891103A (ja) | 1983-05-31 |
| JPH0128084B2 JPH0128084B2 (enrdf_load_stackoverflow) | 1989-06-01 |
Family
ID=16247177
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18978681A Granted JPS5891103A (ja) | 1981-11-25 | 1981-11-25 | コロイド銀粒子分散物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5891103A (enrdf_load_stackoverflow) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63100439A (ja) * | 1986-05-02 | 1988-05-02 | Fuji Photo Film Co Ltd | ゲル状物質を連続熔融する方法及び装置 |
| JPS6415309A (en) * | 1987-07-08 | 1989-01-19 | Agency Ind Science Techn | Production of metal fine powder |
| EP1666177A4 (en) * | 2003-08-28 | 2009-09-16 | Tama Tlo Ltd | PRECIOUS METAL COLLOID, PRECIOUS METAL MICROPARTICLE, COMPOSITION AND PROCESS FOR PRODUCING PRECIOUS METAL MICROPARTICLE |
| JP2009242875A (ja) * | 2008-03-31 | 2009-10-22 | Mitsubishi Paper Mills Ltd | 銀超微粒子の製造方法 |
| JP2009242874A (ja) * | 2008-03-31 | 2009-10-22 | Mitsubishi Paper Mills Ltd | 銀超微粒子の製造方法 |
| JP2009299162A (ja) * | 2008-06-16 | 2009-12-24 | Fujifilm Corp | 銀ナノワイヤー及びその製造方法、並びに水性分散物及び透明導電体 |
| JP2010110720A (ja) * | 2008-11-07 | 2010-05-20 | Toyota Central R&D Labs Inc | 金属化合物のコロイド溶液およびその製造方法 |
| JP2011219328A (ja) * | 2010-04-13 | 2011-11-04 | Toyota Motor Corp | 水酸化コバルトのコロイド溶液及びその製造方法 |
| CN105665748A (zh) * | 2016-04-25 | 2016-06-15 | 辽宁石化职业技术学院 | 一种高纯超细银粉的制备方法 |
-
1981
- 1981-11-25 JP JP18978681A patent/JPS5891103A/ja active Granted
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63100439A (ja) * | 1986-05-02 | 1988-05-02 | Fuji Photo Film Co Ltd | ゲル状物質を連続熔融する方法及び装置 |
| JPS6415309A (en) * | 1987-07-08 | 1989-01-19 | Agency Ind Science Techn | Production of metal fine powder |
| EP1666177A4 (en) * | 2003-08-28 | 2009-09-16 | Tama Tlo Ltd | PRECIOUS METAL COLLOID, PRECIOUS METAL MICROPARTICLE, COMPOSITION AND PROCESS FOR PRODUCING PRECIOUS METAL MICROPARTICLE |
| US7928149B2 (en) | 2003-08-28 | 2011-04-19 | Tama-Tlo, Ltd. | Precious metal colloid, precious metal fine-particle, composition, and method for producing precious metal fine-particle |
| JP2009242875A (ja) * | 2008-03-31 | 2009-10-22 | Mitsubishi Paper Mills Ltd | 銀超微粒子の製造方法 |
| JP2009242874A (ja) * | 2008-03-31 | 2009-10-22 | Mitsubishi Paper Mills Ltd | 銀超微粒子の製造方法 |
| JP2009299162A (ja) * | 2008-06-16 | 2009-12-24 | Fujifilm Corp | 銀ナノワイヤー及びその製造方法、並びに水性分散物及び透明導電体 |
| JP2010110720A (ja) * | 2008-11-07 | 2010-05-20 | Toyota Central R&D Labs Inc | 金属化合物のコロイド溶液およびその製造方法 |
| JP2011219328A (ja) * | 2010-04-13 | 2011-11-04 | Toyota Motor Corp | 水酸化コバルトのコロイド溶液及びその製造方法 |
| CN105665748A (zh) * | 2016-04-25 | 2016-06-15 | 辽宁石化职业技术学院 | 一种高纯超细银粉的制备方法 |
| CN105665748B (zh) * | 2016-04-25 | 2018-01-19 | 辽宁石化职业技术学院 | 一种高纯超细银粉的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0128084B2 (enrdf_load_stackoverflow) | 1989-06-01 |
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