JPS5795977A - Preparation of piperidinophenylpropionic acid - Google Patents
Preparation of piperidinophenylpropionic acidInfo
- Publication number
- JPS5795977A JPS5795977A JP55170920A JP17092080A JPS5795977A JP S5795977 A JPS5795977 A JP S5795977A JP 55170920 A JP55170920 A JP 55170920A JP 17092080 A JP17092080 A JP 17092080A JP S5795977 A JPS5795977 A JP S5795977A
- Authority
- JP
- Japan
- Prior art keywords
- piperidinophenyl
- chloro
- formula
- raw material
- metal hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
PURPOSE: To obtain the titled substance useful as an antiphlogistic and analgesic agent by a simple operation in high yield, by using 2-(3-chloro-4-piperidinophenyl) propylidene azanol to be synthesized easily from an inexpensive industrial reagent as a raw material, treating it with an alkali metal hydroxide, etc.
CONSTITUTION: 2-(3-chloro-4-piperidinophenyl)propylidene azanol shown by the formula I as a raw material is treated with preferably 3W5 equivalents of an alkali metal hydroxide or an alkaline earth metal hydroxide in a high-boiling glycol type solvent, e.g., ethylene glycol, etc. at 80W250°C, to give the titled compound. The raw material compound shown by the formula I is easily obtained by treating 2-(3-chloro-4-piperidinophenyl)-2-methyloxysilane shown by the formula II with an acid to give 2-(3-chloro-4-piperidinophenyl)propanal shown by the formula III, which is reacted with hydroxylamine.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55170920A JPS5795977A (en) | 1980-12-05 | 1980-12-05 | Preparation of piperidinophenylpropionic acid |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55170920A JPS5795977A (en) | 1980-12-05 | 1980-12-05 | Preparation of piperidinophenylpropionic acid |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5795977A true JPS5795977A (en) | 1982-06-15 |
Family
ID=15913796
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55170920A Pending JPS5795977A (en) | 1980-12-05 | 1980-12-05 | Preparation of piperidinophenylpropionic acid |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5795977A (en) |
-
1980
- 1980-12-05 JP JP55170920A patent/JPS5795977A/en active Pending
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