JPS5770879A - Preparation of mercaptothiazoline compound - Google Patents
Preparation of mercaptothiazoline compoundInfo
- Publication number
- JPS5770879A JPS5770879A JP14628280A JP14628280A JPS5770879A JP S5770879 A JPS5770879 A JP S5770879A JP 14628280 A JP14628280 A JP 14628280A JP 14628280 A JP14628280 A JP 14628280A JP S5770879 A JPS5770879 A JP S5770879A
- Authority
- JP
- Japan
- Prior art keywords
- carbon disulfide
- alkaline hydroxide
- aminoalkyl sulfuric
- ester
- sulfuric ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Abstract
PURPOSE: To obtain the titled substance in high yield without side reactions, by reacting an aminoalkyl sulfuric easter with carbon disulfide in the presence of an alkaline hydroxide at a ratio of the alkaline hydroxide and carbon disulfide to the ester in a given range.
CONSTITUTION: An aminoalkyl sulfuric ester is reacted with carbon disulfide in the presence of an alkaline hydroxide. In the process, the carbon disulfide and alkaline hydroxide are used in an amount in the range of equimolar to 2mol% excess based on the aminoalkyl sulfuric ester, and the reaction is carried out in an aqueous solvent at 45W70°C to give the aimed compound in high yield. 2-Aminoethyl sulfate, 2-amino-1-propyl sulfate, etc. may be cited as the aminoalkyl sulfuric ester.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14628280A JPS5770879A (en) | 1980-10-21 | 1980-10-21 | Preparation of mercaptothiazoline compound |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14628280A JPS5770879A (en) | 1980-10-21 | 1980-10-21 | Preparation of mercaptothiazoline compound |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5770879A true JPS5770879A (en) | 1982-05-01 |
JPS639509B2 JPS639509B2 (en) | 1988-02-29 |
Family
ID=15404184
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14628280A Granted JPS5770879A (en) | 1980-10-21 | 1980-10-21 | Preparation of mercaptothiazoline compound |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5770879A (en) |
-
1980
- 1980-10-21 JP JP14628280A patent/JPS5770879A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS639509B2 (en) | 1988-02-29 |
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